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Assay Detail

CHEMBL1037787

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Displacement of [125I]Tyr-o-CRF from CRF1 receptor in rat frontal cortex homogenate by binding titration assay
16
Total Activities
16
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Rattus norvegicus
Tissue Frontal cortex
Confidence 9 — Direct single protein target
Curated By Intermediate

Target

Corticotropin-releasing factor receptor 1 (CHEMBL4649)
Type SINGLE PROTEIN
Organism Rattus norvegicus

Publication

A strategy to minimize reactive metabolite formation: discovery of (S)-4-(1-cyclopropyl-2-methoxyethyl)-6-[6-(difluoromethoxy)-2,5-dimethylpyridin-3-ylamino]-5-oxo-4,5-dihydropyrazine-2-carbonitrile as a potent, orally bioavailable corticotropin-releasing factor-1 receptor antagonist.
Hartz RA, Ahuja VT, Zhuo X, Mattson RJ, Denhart DJ, Deskus JA, Vrudhula VM, Pan S, Ditta JL, Shu YZ, Grace JE, Lentz KA, Lelas S, Li YW, Molski TF, Krishnananthan S, Wong H, Qian-Cutrone J, Schartman R, Denton R, Lodge NJ, Zaczek R, Macor JE, Bronson JJ.
J Med Chem (2009) 52 : 7653 -7668
PubMed 19954247 · DOI

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 16 8.91 9.68

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL583153 1 9.68
CHEMBL574852 1 9.62
CHEMBL584343 1 9.55
CHEMBL583387 1 9.52
CHEMBL572589 1 9.30
CHEMBL574853 1 9.09
CHEMBL573978 1 9.07
CHEMBL575491 1 8.96
CHEMBL576589 1 8.85
CHEMBL574436 1 8.82
CHEMBL573748 1 8.82
CHEMBL572588 1 8.80
CHEMBL573976 1 8.77
CHEMBL573284 1 8.00
CHEMBL578838 1 7.92
CHEMBL575510 1 7.85

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL583153 IC50 = 0.21 nM 9.68
CHEMBL574852 IC50 = 0.24 nM 9.62
CHEMBL584343 IC50 = 0.28 nM 9.55
CHEMBL583387 IC50 = 0.3 nM 9.52
CHEMBL572589 IC50 = 0.5 nM 9.30
CHEMBL574853 IC50 = 0.82 nM 9.09
CHEMBL573978 IC50 = 0.86 nM 9.07
CHEMBL575491 IC50 = 1.1 nM 8.96
CHEMBL576589 IC50 = 1.4 nM 8.85
CHEMBL574436 IC50 = 1.5 nM 8.82
CHEMBL573748 IC50 = 1.5 nM 8.82
CHEMBL572588 IC50 = 1.6 nM 8.80
CHEMBL573976 IC50 = 1.7 nM 8.77
CHEMBL573284 IC50 = 10.0 nM 8.00
CHEMBL578838 IC50 = 12.0 nM 7.92
CHEMBL575510 IC50 = 14.0 nM 7.85