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Assay Detail

CHEMBL3129555

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Inhibition of BRAF V600E mutant in human HT-29 cells assessed as phosphorylation of MEK
14
Total Activities
14
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Cell Type HT-29
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Serine/threonine-protein kinase B-raf (CHEMBL5145)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Discovery of a selective kinase inhibitor (TAK-632) targeting pan-RAF inhibition: design, synthesis, and biological evaluation of C-7-substituted 1,3-benzothiazole derivatives.
Okaniwa M, Hirose M, Arita T, Yabuki M, Nakamura A, Takagi T, Kawamoto T, Uchiyama N, Sumita A, Tsutsumi S, Tottori T, Inui Y, Sang BC, Yano J, Aertgeerts K, Yoshida S, Ishikawa T.
J Med Chem (2013) 56 : 6478 -6494
PubMed 23906342 · DOI

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 14 7.12 7.66

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3125885 1 7.66
CHEMBL3125893 1 7.62
CHEMBL3125892 1 7.54
CHEMBL3125891 1 7.47
CHEMBL3125890 1 7.12
CHEMBL3125883 1 7.12
CHEMBL3125886 1 7.09
CHEMBL3125884 1 6.96
CHEMBL3125881 1 6.77
CHEMBL3125889 1 6.50
CHEMBL3125888 1 6.44
CHEMBL3125887 1 -
CHEMBL3125882 1 -
CHEMBL3124950 1 -

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3125885 IC50 = 22.0 nM 7.66
CHEMBL3125893 IC50 = 24.0 nM 7.62
CHEMBL3125892 IC50 = 29.0 nM 7.54
CHEMBL3125891 IC50 = 34.0 nM 7.47
CHEMBL3125890 IC50 = 75.0 nM 7.12
CHEMBL3125883 IC50 = 75.0 nM 7.12
CHEMBL3125886 IC50 = 81.0 nM 7.09
CHEMBL3125884 IC50 = 110.0 nM 6.96
CHEMBL3125881 IC50 = 170.0 nM 6.77
CHEMBL3125889 IC50 = 320.0 nM 6.50
CHEMBL3125888 IC50 = 360.0 nM 6.44
CHEMBL3125887 IC50 > 500.0 nM -
CHEMBL3125882 IC50 > 500.0 nM -
CHEMBL3124950 IC50 - -