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Assay Detail

CHEMBL3431450

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Functional
GSK_TCAKS: pIC50 Leishmania donovani viability assay using fluorescence intensity. Assay plates (1536-well) were prepared by adding 30nL per well of compound. For single shot assay, the final compound concentration was 5uM. For potency determinations, eleven-point one in three dilution curves were generated with a top concentration of 50uM. Briefly, eGFP LdBOB axenic amastigotes were harvested, fixed and counted in a CASY cell counter (Roche-Applied Science). A final concentration of 1.5 * 10^5 cells per well were prepared in amastigote media containing 500 U/mL penicillin/streptomycin (Invitrogen) and 6uL was dispensed to each experimental well using a Multidrop Combi dispenser (Thermo Scientific). 6uL of assay media was dispensed to control columns used as reference for 100% compound response. Following incubation for 72 h at 37C, 5% CO2, 2 uL of resazurin was added to each well at a final concentration of 0.5 mM in phosphate buffered saline (PBS) with IGEPAL (Sigma-Aldrich), 0.05% (v/v). The plates were incubated for 4 h at room temperature and resorufin fluorescence was detected using a PerkinElmer EnVision plate reader with excitation at 528 nm and emission at 590 nm.
590
Total Activities
590
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Functional
Organism Leishmania donovani
Cell Type CASY
Confidence 1 — Organism
Curated By Autocuration

Target

Leishmania donovani (CHEMBL367)
Type ORGANISM
Organism Leishmania donovani

Publication

GSK Tres Cantos Anti-Kinetoplastid Screening (TCAKS) Data.
Imanol Pena, M. Pilar Manzano, Juan Cantizani, Albane Kessler, Julio Alonso-Padilla, Ana I. Bardera, Emilio Alvarez, Gonzalo Colmenarejo, Ignacio Cotillo, Irene Roquero, Francisco de Dios-Anton, Vanessa Barroso, Ana Rodriguez, David W. Gray, Miguel Navarro, Vinod Kumar, Alexander Sherstnev, David Drewry, James R. Brown, Jose M. Fiandor & J. Julio Martin.

· DOI

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 590 5.34 7.50

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3431298 1 7.50
CHEMBL3431297 1 7.40
CHEMBL3431127 1 7.40
CHEMBL3431435 1 7.20
CHEMBL3431295 1 7.10
CHEMBL3431194 1 7.00
CHEMBL3431025 1 6.90
CHEMBL2098124 1 6.90
CHEMBL522630 1 6.90
CHEMBL3431397 1 6.90
CHEMBL3431400 1 6.80
CHEMBL3431230 1 6.70
CHEMBL3431433 1 6.70
CHEMBL3431229 1 6.60
CHEMBL523303 1 6.60
CHEMBL3431258 1 6.50
CHEMBL3431188 1 6.50
CHEMBL491149 1 6.50
CHEMBL523468 1 6.50
CHEMBL3431381 1 6.50
CHEMBL3431326 1 6.40
CHEMBL1232777 FORMYCIN B 1 6.40
CHEMBL3430988 1 6.40
CHEMBL3431004 1 6.40
CHEMBL3431011 1 6.40
CHEMBL3431106 1 6.40
CHEMBL3431139 1 6.40
CHEMBL3431187 1 6.40
CHEMBL3431363 1 6.30
CHEMBL3431371 1 6.30

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3431298 IC50 = 31.62 nM 7.50
CHEMBL3431297 IC50 = 39.81 nM 7.40
CHEMBL3431127 IC50 = 39.81 nM 7.40
CHEMBL3431435 IC50 = 63.1 nM 7.20
CHEMBL3431295 IC50 = 79.43 nM 7.10
CHEMBL3431194 IC50 = 100.0 nM 7.00
CHEMBL3431397 IC50 = 125.89 nM 6.90
CHEMBL3431025 IC50 = 125.89 nM 6.90
CHEMBL2098124 IC50 = 125.89 nM 6.90
CHEMBL522630 IC50 = 125.89 nM 6.90
CHEMBL3431400 IC50 = 158.49 nM 6.80
CHEMBL3431230 IC50 = 199.53 nM 6.70
CHEMBL3431433 IC50 = 199.53 nM 6.70
CHEMBL523303 IC50 = 251.19 nM 6.60
CHEMBL3431229 IC50 = 251.19 nM 6.60
CHEMBL491149 IC50 = 316.23 nM 6.50
CHEMBL3431258 IC50 = 316.23 nM 6.50
CHEMBL523468 IC50 = 316.23 nM 6.50
CHEMBL3431381 IC50 = 316.23 nM 6.50
CHEMBL3431188 IC50 = 316.23 nM 6.50
CHEMBL3431187 IC50 = 398.11 nM 6.40
CHEMBL3431326 IC50 = 398.11 nM 6.40
CHEMBL3430988 IC50 = 398.11 nM 6.40
CHEMBL3431004 IC50 = 398.11 nM 6.40
CHEMBL3431011 IC50 = 398.11 nM 6.40
CHEMBL3431106 IC50 = 398.11 nM 6.40
CHEMBL1232777 FORMYCIN B IC50 = 398.11 nM 6.40
CHEMBL3431139 IC50 = 398.11 nM 6.40
CHEMBL3431363 IC50 = 501.19 nM 6.30
CHEMBL3431371 IC50 = 501.19 nM 6.30
CHEMBL3431033 IC50 = 501.19 nM 6.30
CHEMBL3431003 IC50 = 501.19 nM 6.30
CHEMBL3431105 IC50 = 501.19 nM 6.30
CHEMBL1489081 IC50 = 630.96 nM 6.20
CHEMBL3430947 IC50 = 630.96 nM 6.20
CHEMBL3431082 IC50 = 630.96 nM 6.20
CHEMBL3431357 IC50 = 630.96 nM 6.20
CHEMBL3431193 IC50 = 630.96 nM 6.20
CHEMBL3431170 IC50 = 630.96 nM 6.20
CHEMBL3431345 IC50 = 630.96 nM 6.20
CHEMBL3431209 IC50 = 794.33 nM 6.10
CHEMBL3431129 IC50 = 794.33 nM 6.10
CHEMBL1731664 IC50 = 794.33 nM 6.10
CHEMBL2441267 IC50 = 794.33 nM 6.10
CHEMBL3431352 IC50 = 794.33 nM 6.10
CHEMBL3431376 IC50 = 794.33 nM 6.10
CHEMBL530275 IC50 = 794.33 nM 6.10
CHEMBL3431432 IC50 = 794.33 nM 6.10
CHEMBL3431431 IC50 = 794.33 nM 6.10
CHEMBL526199 IC50 = 794.33 nM 6.10