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Assay Detail

CHEMBL3705499

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Binding
Inhibition Assay: A test for MGAT2 inhibitory action of test compounds was conducted in accordance with a partially modified version of the method described in John F. Lockwood et al., Am. J. Physiol. Endocrinol. Metab., 2003, 285, E927.Bac-to-Bac Baculovirus Expression System (Life Technologies Japan) was used to express human MGAT2 in insect cells (Sf9) (Life Technologies Japan). These cells were sonicated and centrifuged at 100,000 g.times.1 hr to give a precipitate. The precipitate was used as a human MGAT2 enzyme fraction in this assay.This test was conducted using a black flat-bottom 96-well plate (Corning). A buffer solution with final concentrations of 5 mM magnesium chloride, 100 mM sucrose and 100 mM Tris-HCl (pH=7.5) was prepared and test compounds prepared in various concentrations using dimethyl sulfoxide were added thereto to give a final dimethyl sulfoxide concentration of 1%. The MGAT2 enzyme fraction was added thereto to give a final concentration of 0.5 .mu.g/ml.
103
Total Activities
96
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Cell Type Sf9
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

2-acylglycerol O-acyltransferase 2 (CHEMBL2439944)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Nitrogen-containing condensed heterocyclic compound
(2015)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 103 7.13 8.70

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3655055 1 8.70
CHEMBL3639539 1 8.40
CHEMBL3655036 1 8.15
CHEMBL3655042 1 8.00
CHEMBL3655064 1 7.89
CHEMBL3655065 1 7.85
CHEMBL3655059 1 7.64
CHEMBL3655032 1 7.62
CHEMBL3654970 1 7.62
CHEMBL3655016 2 7.60
CHEMBL3655039 1 7.58
CHEMBL3655015 2 7.58
CHEMBL3654958 1 7.58
CHEMBL3654950 1 7.55
CHEMBL3655057 1 7.55
CHEMBL3655038 1 7.54
CHEMBL3655054 1 7.52
CHEMBL3654957 1 7.51
CHEMBL3655017 2 7.51
CHEMBL3654956 1 7.51
CHEMBL3655049 1 7.48
CHEMBL3654951 1 7.46
CHEMBL3654959 1 7.44
CHEMBL3655033 1 7.41
CHEMBL3654967 1 7.40
CHEMBL3655030 1 7.40
CHEMBL3655019 2 7.38
CHEMBL3654980 1 7.38
CHEMBL3655035 1 7.37
CHEMBL3655021 2 7.36

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3655055 IC50 = 2.0 nM 8.70
CHEMBL3639539 IC50 = 4.0 nM 8.40
CHEMBL3655036 IC50 = 7.0 nM 8.15
CHEMBL3655042 IC50 = 10.0 nM 8.00
CHEMBL3655064 IC50 = 13.0 nM 7.89
CHEMBL3655065 IC50 = 14.0 nM 7.85
CHEMBL3655059 IC50 = 23.0 nM 7.64
CHEMBL3655032 IC50 = 24.0 nM 7.62
CHEMBL3654970 IC50 = 24.0 nM 7.62
CHEMBL3655016 IC50 = 25.0 nM 7.60
CHEMBL3655039 IC50 = 26.0 nM 7.58
CHEMBL3654958 IC50 = 26.0 nM 7.58
CHEMBL3655015 IC50 = 26.0 nM 7.58
CHEMBL3655057 IC50 = 28.0 nM 7.55
CHEMBL3654950 IC50 = 28.0 nM 7.55
CHEMBL3655038 IC50 = 29.0 nM 7.54
CHEMBL3655054 IC50 = 30.0 nM 7.52
CHEMBL3654956 IC50 = 31.0 nM 7.51
CHEMBL3654957 IC50 = 31.0 nM 7.51
CHEMBL3655017 IC50 = 31.0 nM 7.51
CHEMBL3655049 IC50 = 33.0 nM 7.48
CHEMBL3654951 IC50 = 35.0 nM 7.46
CHEMBL3654959 IC50 = 36.0 nM 7.44
CHEMBL3655033 IC50 = 39.0 nM 7.41
CHEMBL3655015 IC50 = 39.0 nM 7.41
CHEMBL3655030 IC50 = 40.0 nM 7.40
CHEMBL3654967 IC50 = 40.0 nM 7.40
CHEMBL3655019 IC50 = 42.0 nM 7.38
CHEMBL3654980 IC50 = 42.0 nM 7.38
CHEMBL3655035 IC50 = 43.0 nM 7.37
CHEMBL3655021 IC50 = 44.0 nM 7.36
CHEMBL3655016 IC50 = 44.0 nM 7.36
CHEMBL3655031 IC50 = 45.0 nM 7.35
CHEMBL3654964 IC50 = 49.0 nM 7.31
CHEMBL3654968 IC50 = 51.0 nM 7.29
CHEMBL3654955 IC50 = 53.0 nM 7.28
CHEMBL3654985 IC50 = 52.0 nM 7.28
CHEMBL3655041 IC50 = 56.0 nM 7.25
CHEMBL3655053 IC50 = 58.0 nM 7.24
CHEMBL3655045 IC50 = 59.0 nM 7.23
CHEMBL3655017 IC50 = 62.0 nM 7.21
CHEMBL3654952 IC50 = 62.0 nM 7.21
CHEMBL3654966 IC50 = 62.0 nM 7.21
CHEMBL3655048 IC50 = 62.0 nM 7.21
CHEMBL3654960 IC50 = 65.0 nM 7.19
CHEMBL3655020 IC50 = 66.0 nM 7.18
CHEMBL3655021 IC50 = 68.0 nM 7.17
CHEMBL3655029 IC50 = 69.0 nM 7.16
CHEMBL3654997 IC50 = 70.0 nM 7.16
CHEMBL3654949 IC50 = 76.0 nM 7.12