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Assay Detail

CHEMBL3705705

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Enzyme Assays: Compounds for testing were diluted in DMSO to 50 fold the final concentration and a ten point three fold dilution series was made. The compounds were diluted in assay buffer (50 mM HEPES, pH 7.4, 100 mM KCl, 0.001% Tween-20, 0.05% BSA, 20 uM TCEP) to 6 fold their final concentration. The HDAC enzymes (purchased from BPS Biosciences) were diluted to 1.5 fold their final concentration in assay buffer. The tripeptide substrate and trypsin at 0.05 uM final concentration were diluted in assay buffer at 6 fold their final concentration. The final enzyme concentrations used in these assays were 3.3 ng/ml (HDAC1), 0.2 ng/ml (HDAC2), 0.08 ng/ml (HDAC3) and 2 ng/ml (HDAC6). The final substrate concentrations used were 16 uM (HDAC1), 10 uM (HDAC2), 17 uM (HDAC3) and 14 uM (HDAC6).
365
Total Activities
176
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Histone deacetylase 6 (CHEMBL1865)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Reverse amide compounds as protein deacetylase inhibitors and methods of use thereof
(2013)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 365 7.39 8.70

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3693777 2 8.70
CHEMBL3640691 2 8.70
CHEMBL3693720 4 8.70
CHEMBL3693788 2 8.52
CHEMBL3640685 2 8.52
CHEMBL3640683 2 8.52
CHEMBL3640678 2 8.52
CHEMBL3640674 2 8.52
CHEMBL3640669 2 8.52
CHEMBL3640662 2 8.52
CHEMBL3640660 2 8.52
CHEMBL3693812 2 8.52
CHEMBL3693806 2 8.52
CHEMBL3693804 2 8.52
CHEMBL3693803 2 8.52
CHEMBL3693798 4 8.52
CHEMBL3693789 2 8.52
CHEMBL3693782 2 8.52
CHEMBL3693780 2 8.52
CHEMBL3693778 2 8.52
CHEMBL3693746 2 8.52
CHEMBL3693731 2 8.52
CHEMBL3693730 2 8.52
CHEMBL3693722 2 8.52
CHEMBL3693717 2 8.52
CHEMBL3693716 2 8.52
CHEMBL3693711 2 8.52
CHEMBL3693706 2 8.52
CHEMBL3693704 2 8.52
CHEMBL3693719 2 8.40

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3693777 IC50 = 2.0 nM 8.70
CHEMBL3640691 IC50 = 2.0 nM 8.70
CHEMBL3693720 IC50 = 2.0 nM 8.70
CHEMBL3693731 IC50 = 3.0 nM 8.52
CHEMBL3693746 IC50 = 3.0 nM 8.52
CHEMBL3693812 IC50 = 3.0 nM 8.52
CHEMBL3640660 IC50 = 3.0 nM 8.52
CHEMBL3640685 IC50 = 3.0 nM 8.52
CHEMBL3693730 IC50 = 3.0 nM 8.52
CHEMBL3640683 IC50 = 3.0 nM 8.52
CHEMBL3640678 IC50 = 3.0 nM 8.52
CHEMBL3640674 IC50 = 3.0 nM 8.52
CHEMBL3693722 IC50 = 3.0 nM 8.52
CHEMBL3693778 IC50 = 3.0 nM 8.52
CHEMBL3693780 IC50 = 3.0 nM 8.52
CHEMBL3640662 IC50 = 3.0 nM 8.52
CHEMBL3693716 IC50 = 3.0 nM 8.52
CHEMBL3693717 IC50 = 3.0 nM 8.52
CHEMBL3693798 IC50 = 3.0 nM 8.52
CHEMBL3693803 IC50 = 3.0 nM 8.52
CHEMBL3693704 IC50 = 3.0 nM 8.52
CHEMBL3693804 IC50 = 3.0 nM 8.52
CHEMBL3693706 IC50 = 3.0 nM 8.52
CHEMBL3693798 IC50 = 3.0 nM 8.52
CHEMBL3640669 IC50 = 3.0 nM 8.52
CHEMBL3693806 IC50 = 3.0 nM 8.52
CHEMBL3693789 IC50 = 3.0 nM 8.52
CHEMBL3693711 IC50 = 3.0 nM 8.52
CHEMBL3693788 IC50 = 3.0 nM 8.52
CHEMBL3693782 IC50 = 3.0 nM 8.52
CHEMBL3693719 IC50 = 4.0 nM 8.40
CHEMBL3640700 IC50 = 4.0 nM 8.40
CHEMBL3639395 IC50 = 4.0 nM 8.40
CHEMBL3640673 IC50 = 4.0 nM 8.40
CHEMBL3693740 IC50 = 4.0 nM 8.40
CHEMBL3640694 IC50 = 4.0 nM 8.40
CHEMBL3640693 IC50 = 4.0 nM 8.40
CHEMBL3693755 IC50 = 4.0 nM 8.40
CHEMBL3693765 IC50 = 4.0 nM 8.40
CHEMBL3693810 IC50 = 4.0 nM 8.40
CHEMBL3640677 IC50 = 4.0 nM 8.40
CHEMBL3693775 IC50 = 4.0 nM 8.40
CHEMBL3693783 IC50 = 4.0 nM 8.40
CHEMBL3693786 CITARINOSTAT IC50 = 4.0 nM 8.40
CHEMBL3640654 IC50 = 4.0 nM 8.40
CHEMBL3693795 IC50 = 5.0 nM 8.30
CHEMBL3693793 IC50 = 5.0 nM 8.30
CHEMBL3640650 IC50 = 5.0 nM 8.30
CHEMBL3640703 IC50 = 5.0 nM 8.30
CHEMBL3640681 IC50 = 5.0 nM 8.30