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Assay Detail

CHEMBL3705758

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Binding
Homogeneous Time-Resolve Fluorescence (HTRF) Assay: One potential limitation of the above FP assay is the risk of selection of compounds that may interfere with the FP assays and produce so called false-positives. Therefore, during development of embodiments of the present invention, a time-resolved fluorescence resonance energy transfer (TR-FRET) assay was utilized as a secondary, assay (e.g. for confirmation of results), commercialized by CIS-BIO as homogeneous time-resolve fluorescence (HTRF) assay. In some embodiments, the HTRF assay may be the primary assay and the FP assay is used as a secondary assay to confirm results. HTRF is based on the non-radiative energy transfer of the long-lived emission from the Europium cryptate (Eu3+-cryptate) donor to the allophycocyanin (XL665) acceptor, combined with time-resolved detection. When these two fluorophores are brought together by a biomolecular interaction, a portion of the energy captured by the Eu3+-cryptate during excitation at 337 nm is released through fluorescence emission.
7
Total Activities
7
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

Menin (CHEMBL1615381)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Compositions and methods for treatment of leukemia
(2015)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 7 4.77 5.92

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL1401388 1 5.92
CHEMBL3696195 1 5.16
CHEMBL3696196 1 4.55
CHEMBL3696206 1 4.48
CHEMBL3696166 1 4.46
CHEMBL3696165 1 4.07
CHEMBL1703614 1 -

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL1401388 IC50 = 1200.0 nM 5.92
CHEMBL3696195 IC50 = 7000.0 nM 5.16
CHEMBL3696196 IC50 = 28000.0 nM 4.55
CHEMBL3696206 IC50 = 33000.0 nM 4.48
CHEMBL3696166 IC50 = 35000.0 nM 4.46
CHEMBL3696165 IC50 = 85000.0 nM 4.07
CHEMBL1703614 IC50 = 200000.0 nM -