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Assay Detail

CHEMBL3705828

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Homogeneous Time Resolved Fluorescence Assay: The assay below is used to test the modulatory activity of compounds against FLAP. Human and mouse FLAP-encoding DNA was amplified by polymerase chain reaction and cloned into pFastBac1 (Invitrogen) with a NH2-terminal 6-His tag for expression in Spodoptera frugiperda (Sf-9) cells. FLAP-containing membranes were prepared as was a FITC-labeled FLAP modulator (3-(3-(tert-butylthio)-1-(4-chlorobenzyl)-5-(quinolin-2-ylmethoxy)-1H-indol-2-yl)-2,2-dimethylpropanoic acid). The FLAP binding assay is performed in HTRF format (homogeneous time resolved fluorescence). FLAP-containing membranes (1 ug/well final for human) are incubated in the presence of the HTRF ligand, [5-[({[2-(2-{3-[3-(tert-butylsulfanyl)-1-(4-chlorobenzyl)-5-(quinolin-2-ylmethoxy)-1H-indol-2-yl]-2,2-dimethylpropanoyl}hydrazino)-2-oxoethyl]sulfanyl}acetyl)amino]-2-(6-hydroxy-3-oxo-3H-xanthen-9-yl)benzoic acid] (25 nM final), a terbium labeled anti-His tag antibody (0.5 ng/well final, from Cisbio) and compounds.
335
Total Activities
332
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Arachidonate 5-lipoxygenase-activating protein (CHEMBL4550)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Flap modulators
(2015)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
Ki 335 7.33 9.40

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3704300 1 9.40
CHEMBL3659304 1 9.30
CHEMBL3659301 1 9.05
CHEMBL3704245 1 9.00
CHEMBL3704248 1 9.00
CHEMBL3704256 1 9.00
CHEMBL3704298 1 8.96
CHEMBL3659272 1 8.92
CHEMBL3704289 1 8.89
CHEMBL3704294 1 8.89
CHEMBL3704303 1 8.89
CHEMBL3659293 1 8.89
CHEMBL3659257 1 8.85
CHEMBL3704296 1 8.77
CHEMBL3704266 1 8.72
CHEMBL3704181 1 8.70
CHEMBL3640031 1 8.70
CHEMBL3704351 1 8.66
CHEMBL3659267 1 8.66
CHEMBL3704307 1 8.64
CHEMBL3704265 1 8.62
CHEMBL3659340 1 8.62
CHEMBL3659256 1 8.60
CHEMBL3659261 1 8.60
CHEMBL3704323 1 8.55
CHEMBL3704297 1 8.54
CHEMBL3704350 1 8.54
CHEMBL3704249 1 8.52
CHEMBL3704278 1 8.52
CHEMBL3659266 1 8.48

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3704300 Ki = 0.4 nM 9.40
CHEMBL3659304 Ki = 0.5 nM 9.30
CHEMBL3659301 Ki = 0.9 nM 9.05
CHEMBL3704256 Ki = 1.0 nM 9.00
CHEMBL3704248 Ki = 1.0 nM 9.00
CHEMBL3704245 Ki = 1.0 nM 9.00
CHEMBL3704298 Ki = 1.1 nM 8.96
CHEMBL3659272 Ki = 1.2 nM 8.92
CHEMBL3704303 Ki = 1.3 nM 8.89
CHEMBL3704294 Ki = 1.3 nM 8.89
CHEMBL3704289 Ki = 1.3 nM 8.89
CHEMBL3659293 Ki = 1.3 nM 8.89
CHEMBL3659257 Ki = 1.4 nM 8.85
CHEMBL3704296 Ki = 1.7 nM 8.77
CHEMBL3704266 Ki = 1.9 nM 8.72
CHEMBL3640031 Ki = 2.0 nM 8.70
CHEMBL3704181 Ki = 2.0 nM 8.70
CHEMBL3704351 Ki = 2.2 nM 8.66
CHEMBL3659267 Ki = 2.2 nM 8.66
CHEMBL3704307 Ki = 2.3 nM 8.64
CHEMBL3659340 Ki = 2.4 nM 8.62
CHEMBL3704265 Ki = 2.4 nM 8.62
CHEMBL3659256 Ki = 2.5 nM 8.60
CHEMBL3659261 Ki = 2.5 nM 8.60
CHEMBL3704323 Ki = 2.8 nM 8.55
CHEMBL3704297 Ki = 2.9 nM 8.54
CHEMBL3704350 Ki = 2.9 nM 8.54
CHEMBL3704278 Ki = 3.0 nM 8.52
CHEMBL3704249 Ki = 3.0 nM 8.52
CHEMBL3659266 Ki = 3.3 nM 8.48
CHEMBL3659268 Ki = 3.3 nM 8.48
CHEMBL3704290 Ki = 3.5 nM 8.46
CHEMBL3659273 Ki = 3.6 nM 8.44
CHEMBL3659358 Ki = 3.7 nM 8.43
CHEMBL3704291 Ki = 3.7 nM 8.43
CHEMBL3704284 Ki = 3.7 nM 8.43
CHEMBL3704349 Ki = 3.7 nM 8.43
CHEMBL3659290 Ki = 3.8 nM 8.42
CHEMBL3704293 Ki = 3.9 nM 8.41
CHEMBL3704276 Ki = 4.0 nM 8.40
CHEMBL3704246 Ki = 4.0 nM 8.40
CHEMBL3704247 Ki = 4.0 nM 8.40
CHEMBL3704162 Ki = 4.0 nM 8.40
CHEMBL3704309 Ki = 4.1 nM 8.39
CHEMBL3704342 Ki = 4.1 nM 8.39
CHEMBL3659322 Ki = 4.2 nM 8.38
CHEMBL3704251 Ki = 5.0 nM 8.30
CHEMBL3704178 Ki = 5.0 nM 8.30
CHEMBL3704244 Ki = 5.0 nM 8.30
CHEMBL3704295 Ki = 5.0 nM 8.30