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Assay Detail

CHEMBL3705870

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Fluorometric Plate Assay: To determine the efficacy of various synthesized PAI-1 inhibitor compounds, a fluorometric plate assay was carried out to measure the half maximal inhibitory concentration (IC50) of these compounds on recombinant active human PAI-1 in vitro. An IC50 is a measure of the effectiveness of a compound in inhibiting biological or biochemical function. Stated another way, IC50 represents the concentration of a drug that is required for 50% inhibition in vitro. The IC50 of various compounds was measured using a fluorometric plate assay as set out below, and the results are shown in Table 3.Recombinant active human PAI-1 (Molecular Innovations) (final 1 nM) was incubated for 15 min at 23 C. with increasing concentrations of each compound in 100 mM NaCl, 40 mM HEPES, 0.005% Tween-20, 10% DMSO, pH 7.8. Alternately, the assay has been carried out using low concentrations of DMSO (about 0.1% DMSO or less) in the buffer. In various aspects, the invention does not require a solvent, like DMSO.
37
Total Activities
37
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Plasminogen activator inhibitor 1 (CHEMBL3475)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Plasminogen activator inhibitor-1 inhibitors and methods of use thereof to modulate lipid metabolism
(2015)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 37 6.17 8.00

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL425946 1 8.00
CHEMBL3669202 1 8.00
CHEMBL1224764 1 8.00
CHEMBL207014 1 8.00
CHEMBL377052 1 8.00
CHEMBL3669191 1 7.30
CHEMBL3669189 1 7.30
CHEMBL3669200 1 7.16
CHEMBL3669193 1 7.05
CHEMBL2087115 1 6.55
CHEMBL2087114 1 6.43
CHEMBL2087116 1 5.93
CHEMBL3669196 1 5.77
CHEMBL1090448 1 5.53
CHEMBL3669181 1 5.11
CHEMBL599742 1 4.99
CHEMBL3669187 1 4.56
CHEMBL3669183 1 4.54
CHEMBL3669194 1 4.49
CHEMBL3669199 1 4.32
CHEMBL3669197 1 4.32
CHEMBL3669178 1 4.31
CHEMBL3669185 1 -
CHEMBL292067 1 -
CHEMBL3669186 1 -
CHEMBL606451 1 -
CHEMBL3669188 1 -
CHEMBL3669182 1 -
CHEMBL3669180 1 -
CHEMBL3669192 1 -

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL425946 IC50 = 10.0 nM 8.00
CHEMBL377052 IC50 = 10.0 nM 8.00
CHEMBL207014 IC50 = 10.0 nM 8.00
CHEMBL1224764 IC50 = 10.0 nM 8.00
CHEMBL3669202 IC50 = 10.0 nM 8.00
CHEMBL3669191 IC50 = 50.0 nM 7.30
CHEMBL3669189 IC50 = 50.0 nM 7.30
CHEMBL3669200 IC50 = 70.0 nM 7.16
CHEMBL3669193 IC50 = 90.0 nM 7.05
CHEMBL2087115 IC50 = 280.0 nM 6.55
CHEMBL2087114 IC50 = 370.0 nM 6.43
CHEMBL2087116 IC50 = 1170.0 nM 5.93
CHEMBL3669196 IC50 = 1710.0 nM 5.77
CHEMBL1090448 IC50 = 2960.0 nM 5.53
CHEMBL3669181 IC50 = 7850.0 nM 5.11
CHEMBL599742 IC50 = 10200.0 nM 4.99
CHEMBL3669187 IC50 = 27500.0 nM 4.56
CHEMBL3669183 IC50 = 28700.0 nM 4.54
CHEMBL3669194 IC50 = 32700.0 nM 4.49
CHEMBL3669197 IC50 = 47900.0 nM 4.32
CHEMBL3669199 IC50 = 48300.0 nM 4.32
CHEMBL3669178 IC50 = 49300.0 nM 4.31
CHEMBL3669195 IC50 = 104000.0 nM -
CHEMBL3669198 IC50 = 146000.0 nM -
CHEMBL3669190 IC50 = 195000.0 nM -
CHEMBL3669179 IC50 = 196000.0 nM -
CHEMBL3669184 IC50 = 236000.0 nM -
CHEMBL3669201 IC50 = 246000.0 nM -
CHEMBL302625 IC50 = 269000.0 nM -
CHEMBL3669192 IC50 = 332000.0 nM -
CHEMBL3669180 IC50 = 338000.0 nM -
CHEMBL3669182 IC50 = 386000.0 nM -
CHEMBL3669188 IC50 = 423000.0 nM -
CHEMBL606451 IC50 = 450000.0 nM -
CHEMBL3669186 IC50 = 562000.0 nM -
CHEMBL292067 IC50 = 900000.0 nM -
CHEMBL3669185 IC50 = 2204000.0 nM -