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Assay Detail

CHEMBL3705877

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Inhibition Assay: A similar assay procedure as described in Test 2 was used for HDAC6. Human recombinant full length HDAC6 expressed in a baculovirus expression system was purchased from BPS BioSciences (San Diego, Calif., U.S.A.). The substrate used in the HDAC1 assay was 5 uM of acetyl-Gly-Ala-Lys(acetyl)-AMC. TEST 2: Human recombinant HDAC4 was expressed in full length form (aa 2-1084) in Sf9 insect cells (obtained from ATCC) using baculovirus generated with Bac-to-Bac system (Invitrogen). Test compounds were serially diluted to reach final test concentrations from 0.000128 uM to 10 uM. HDAC4 and test compounds were incubated in 25 mM Tris buffer pH 8.0 containing 137 mM NaCl, 2.7 mM KCl, 1 mM MgCl2, 0.05% (w/v) bovine serum albumine and 0.005% (v/v) Triton-X-100 for 2 hours at room temperature in presence of 5 uM of acetyl-Gly-Ala-Lys(E-trifluoroacetyl)-AMC (AMC=7-amino-4-methyl coumarin) in a final volume of 9 ul. Control wells with HDAC4 only (positive control).
151
Total Activities
148
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Cell Type Sf9
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Histone deacetylase 6 (CHEMBL1865)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Trifluoromethyl-oxadiazole derivatives and their use in the treatment of disease
(2015)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 151 5.41 6.40

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3692630 1 6.40
CHEMBL3692643 1 6.36
CHEMBL3692641 1 6.34
CHEMBL3692639 1 6.33
CHEMBL3692645 1 6.24
CHEMBL3692637 1 6.16
CHEMBL3692642 1 6.13
CHEMBL3692638 1 6.11
CHEMBL3639915 1 5.85
CHEMBL3692651 1 5.82
CHEMBL3692691 1 5.75
CHEMBL3692644 1 5.70
CHEMBL3692583 1 5.68
CHEMBL3692596 1 5.66
CHEMBL3692689 1 5.64
CHEMBL3692598 1 5.64
CHEMBL3692656 1 5.62
CHEMBL3692679 1 5.62
CHEMBL3692685 1 5.62
CHEMBL3692624 1 5.60
CHEMBL3692684 1 5.58
CHEMBL3692688 1 5.58
CHEMBL3692663 1 5.52
CHEMBL3692671 1 5.52
CHEMBL3692686 1 5.52
CHEMBL3688144 1 5.51
CHEMBL3692650 1 5.51
CHEMBL3692683 1 5.51
CHEMBL3688141 1 5.50
CHEMBL3688145 1 5.50

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3692630 IC50 = 400.0 nM 6.40
CHEMBL3692643 IC50 = 440.0 nM 6.36
CHEMBL3692641 IC50 = 460.0 nM 6.34
CHEMBL3692639 IC50 = 470.0 nM 6.33
CHEMBL3692645 IC50 = 580.0 nM 6.24
CHEMBL3692637 IC50 = 700.0 nM 6.16
CHEMBL3692642 IC50 = 740.0 nM 6.13
CHEMBL3692638 IC50 = 770.0 nM 6.11
CHEMBL3639915 IC50 = 1400.0 nM 5.85
CHEMBL3692651 IC50 = 1500.0 nM 5.82
CHEMBL3692691 IC50 = 1800.0 nM 5.75
CHEMBL3692644 IC50 = 2000.0 nM 5.70
CHEMBL3692583 IC50 = 2100.0 nM 5.68
CHEMBL3692596 IC50 = 2200.0 nM 5.66
CHEMBL3692689 IC50 = 2300.0 nM 5.64
CHEMBL3692598 IC50 = 2300.0 nM 5.64
CHEMBL3692685 IC50 = 2400.0 nM 5.62
CHEMBL3692679 IC50 = 2400.0 nM 5.62
CHEMBL3692656 IC50 = 2400.0 nM 5.62
CHEMBL3692624 IC50 = 2500.0 nM 5.60
CHEMBL3692688 IC50 = 2600.0 nM 5.58
CHEMBL3692684 IC50 = 2600.0 nM 5.58
CHEMBL3692686 IC50 = 3000.0 nM 5.52
CHEMBL3692671 IC50 = 3000.0 nM 5.52
CHEMBL3692663 IC50 = 3000.0 nM 5.52
CHEMBL3688144 IC50 = 3100.0 nM 5.51
CHEMBL3692650 IC50 = 3100.0 nM 5.51
CHEMBL3692683 IC50 = 3100.0 nM 5.51
CHEMBL3688141 IC50 = 3200.0 nM 5.50
CHEMBL3692681 IC50 = 3200.0 nM 5.50
CHEMBL3688145 IC50 = 3200.0 nM 5.50
CHEMBL3688164 IC50 = 3200.0 nM 5.50
CHEMBL3692582 IC50 = 3300.0 nM 5.48
CHEMBL3692676 IC50 = 3300.0 nM 5.48
CHEMBL3692690 IC50 = 3400.0 nM 5.47
CHEMBL3692678 IC50 = 3700.0 nM 5.43
CHEMBL3692660 IC50 = 3900.0 nM 5.41
CHEMBL3692575 IC50 = 3900.0 nM 5.41
CHEMBL3692612 IC50 = 3900.0 nM 5.41
CHEMBL3692626 IC50 = 4000.0 nM 5.40
CHEMBL3688151 IC50 = 4100.0 nM 5.39
CHEMBL3692631 IC50 = 4400.0 nM 5.36
CHEMBL3692655 IC50 = 4400.0 nM 5.36
CHEMBL3692662 IC50 = 4500.0 nM 5.35
CHEMBL3692576 IC50 = 4600.0 nM 5.34
CHEMBL3692601 IC50 = 4600.0 nM 5.34
CHEMBL3692622 IC50 = 4700.0 nM 5.33
CHEMBL3692652 IC50 = 4700.0 nM 5.33
CHEMBL3688160 IC50 = 4800.0 nM 5.32
CHEMBL3692584 IC50 = 4800.0 nM 5.32