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Assay Detail

CHEMBL3706037

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Binding
IMAP-FP Assay: Activated ERK2 activity was determined in an IMAP-FP assay (Molecular Devices). Using this assay format, the potency (IC50) of each compound was determined from a 10 point (1:3 serial dilution, 3 uM starting compound concentration) titration curve using the following outlined procedure. To each well of a black Corning 384-well plate (Corning Catalog #3575), 7.5 mL of compound (3333 fold dilution in final assay volume of 25 uL) was dispensed, followed by the addition of 15 uL of kinase buffer (tween containing kinase buffer, Molecular Devices) containing 0.0364 ng/mL (0.833 nM) of phosphorylated active hERK2 enzyme. Following a 15 minute compound & enzyme incubation, each reaction was initiated by the addition of 10 uL kinase buffer containing 2.45 uM ERK2 IMAP substrate peptides (2.25 uM-unlabeled IPTTPITTTYFFFK-COOH and 200 nM-labeled IPTTPITTTYFFFK-5FAM (5-carboxyfluorescein)-COOH), and 75 uM ATP.
663
Total Activities
641
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Mitogen-activated protein kinase 1 (CHEMBL4040)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Compounds that are ERK inhibitors
(2015)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 663 8.33 9.82

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3658845 1 9.82
CHEMBL3654722 1 9.80
CHEMBL3663068 1 9.80
CHEMBL3654812 1 9.77
CHEMBL3663002 1 9.74
CHEMBL3663034 1 9.71
CHEMBL2408789 1 9.69
CHEMBL3654809 2 9.66
CHEMBL3658692 1 9.65
CHEMBL3663093 1 9.65
CHEMBL3663134 1 9.65
CHEMBL3654746 1 9.63
CHEMBL3658725 1 9.63
CHEMBL3663000 1 9.63
CHEMBL3663035 1 9.63
CHEMBL3654704 1 9.61
CHEMBL3654711 1 9.60
CHEMBL3663084 1 9.60
CHEMBL3663008 1 9.59
CHEMBL3663025 1 9.59
CHEMBL3663009 1 9.58
CHEMBL3662997 1 9.57
CHEMBL3662998 1 9.56
CHEMBL2408790 1 9.54
CHEMBL3654682 1 9.54
CHEMBL3658726 1 9.54
CHEMBL3658844 1 9.54
CHEMBL3662984 1 9.53
CHEMBL3662993 1 9.53
CHEMBL3663062 1 9.53

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3658845 IC50 = 0.1524 nM 9.82
CHEMBL3663068 IC50 = 0.1591 nM 9.80
CHEMBL3654722 IC50 = 0.1588 nM 9.80
CHEMBL3654812 IC50 = 0.1709 nM 9.77
CHEMBL3663002 IC50 = 0.1837 nM 9.74
CHEMBL3663034 IC50 = 0.1934 nM 9.71
CHEMBL2408789 IC50 = 0.2045 nM 9.69
CHEMBL3654809 IC50 = 0.2171 nM 9.66
CHEMBL3663134 IC50 = 0.2213 nM 9.65
CHEMBL3658692 IC50 = 0.223 nM 9.65
CHEMBL3663093 IC50 = 0.2233 nM 9.65
CHEMBL3654809 IC50 = 0.2339 nM 9.63
CHEMBL3654746 IC50 = 0.2351 nM 9.63
CHEMBL3663035 IC50 = 0.233 nM 9.63
CHEMBL3663000 IC50 = 0.2357 nM 9.63
CHEMBL3658725 IC50 = 0.2316 nM 9.63
CHEMBL3654704 IC50 = 0.2452 nM 9.61
CHEMBL3663084 IC50 = 0.2508 nM 9.60
CHEMBL3654711 IC50 = 0.2512 nM 9.60
CHEMBL3663008 IC50 = 0.2599 nM 9.59
CHEMBL3663025 IC50 = 0.2569 nM 9.59
CHEMBL3663009 IC50 = 0.2616 nM 9.58
CHEMBL3662997 IC50 = 0.2688 nM 9.57
CHEMBL3662998 IC50 = 0.2724 nM 9.56
CHEMBL3658844 IC50 = 0.2904 nM 9.54
CHEMBL3654682 IC50 = 0.2904 nM 9.54
CHEMBL3658726 IC50 = 0.288 nM 9.54
CHEMBL2408790 IC50 = 0.2857 nM 9.54
CHEMBL3662984 IC50 = 0.2928 nM 9.53
CHEMBL3662993 IC50 = 0.2983 nM 9.53
CHEMBL3663062 IC50 = 0.2974 nM 9.53
CHEMBL3662990 IC50 = 0.3036 nM 9.52
CHEMBL3658652 IC50 = 0.3037 nM 9.52
CHEMBL3658776 IC50 = 0.3033 nM 9.52
CHEMBL3658804 IC50 = 0.3088 nM 9.51
CHEMBL3658847 IC50 = 0.3067 nM 9.51
CHEMBL3654886 IC50 = 0.309 nM 9.51
CHEMBL3663092 IC50 = 0.3175 nM 9.50
CHEMBL3663003 IC50 = 0.3151 nM 9.50
CHEMBL3663021 IC50 = 0.3132 nM 9.50
CHEMBL3663055 IC50 = 0.326 nM 9.49
CHEMBL3658788 IC50 = 0.3229 nM 9.49
CHEMBL3654680 IC50 = 0.3336 nM 9.48
CHEMBL3658701 IC50 = 0.3329 nM 9.48
CHEMBL3703711 IC50 = 0.342 nM 9.47
CHEMBL3663057 IC50 = 0.3352 nM 9.47
CHEMBL3658730 IC50 = 0.3398 nM 9.47
CHEMBL3663001 IC50 = 0.3577 nM 9.45
CHEMBL3662980 IC50 = 0.3584 nM 9.45
CHEMBL3662977 IC50 = 0.357 nM 9.45