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Assay Detail

CHEMBL3706047

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
FLIPR Assay: Ca.sup.2+flux: 1321N1 cells expressing the recombinant human, rat or mouse P2X7 channel was cultured in HyQ DME/(HyClone/Dulbecco's Modified Eagle Medium) high glucose supplemented with 10% Fetal Bovine Serum (FBS) and appropriate selection marker. Cells were seeded at a density of 25000 cells/well (96-well clear bottom black walled plates) in 100 .mu.l volume/well. On the day of the experiment, cell plates were washed with assay buffer, containing (in mM): 130 NaCl, 2 KCl, 1 CaCl.sub.2, 1 MgCl.sub.2, 10 HEPES, 5 glucose; pH 7.40 and 300 mOs. After the wash, cells were loaded with the Calcium-4 dye (Molecular Device) and incubated in the dark for 60 minutes. Test compounds were prepared at 250.times. the test concentration in neat DMSO. Intermediate 96-well compound plates were prepared by transferring 1.2 .mu.L of the compound into 300 .mu.L of assay buffer. A further 3.times. dilution occurred when transferring 50 .mu.L/well of the compound plate to 100 .mu.L/well in the cell plate.
45
Total Activities
45
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Cell Type 1321-N1
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

P2X purinoceptor 7 (CHEMBL4805)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

5,6,7,8,9,10-hexahydro-6,10-epimino[1,2,4]triazolo[4,3-a]azocines as P2X7 modulators
(2015)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 45 7.59 8.96

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3697521 1 8.96
CHEMBL3697548 1 8.77
CHEMBL3697551 1 8.59
CHEMBL3697543 1 8.51
CHEMBL3697509 1 8.42
CHEMBL3697539 1 8.30
CHEMBL3697544 1 8.21
CHEMBL3697531 1 8.20
CHEMBL3697534 1 8.11
CHEMBL3697515 1 8.11
CHEMBL3697511 1 8.02
CHEMBL3697516 1 8.01
CHEMBL6067665 1 8.00
CHEMBL3697520 1 8.00
CHEMBL3697542 1 7.99
CHEMBL3697540 1 7.98
CHEMBL3697530 1 7.90
CHEMBL3697535 1 7.88
CHEMBL3697538 1 7.88
CHEMBL3697519 1 7.88
CHEMBL3697527 1 7.87
CHEMBL3697541 1 7.84
CHEMBL3697550 1 7.83
CHEMBL3697536 1 7.82
CHEMBL3697545 1 7.77
CHEMBL3697552 1 7.71
CHEMBL3697533 1 7.70
CHEMBL3697532 1 7.70
CHEMBL3697537 1 7.69
CHEMBL3697546 1 7.51

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3697521 IC50 = 1.1 nM 8.96
CHEMBL3697548 IC50 = 1.7 nM 8.77
CHEMBL3697551 IC50 = 2.6 nM 8.59
CHEMBL3697543 IC50 = 3.1 nM 8.51
CHEMBL3697509 IC50 = 3.8 nM 8.42
CHEMBL3697539 IC50 = 5.0 nM 8.30
CHEMBL3697544 IC50 = 6.1 nM 8.21
CHEMBL3697531 IC50 = 6.3 nM 8.20
CHEMBL3697534 IC50 = 7.7 nM 8.11
CHEMBL3697515 IC50 = 7.7 nM 8.11
CHEMBL3697511 IC50 = 9.6 nM 8.02
CHEMBL3697516 IC50 = 9.7 nM 8.01
CHEMBL6067665 IC50 = 10.0 nM 8.00
CHEMBL3697520 IC50 = 10.0 nM 8.00
CHEMBL3697542 IC50 = 10.2 nM 7.99
CHEMBL3697540 IC50 = 10.4 nM 7.98
CHEMBL3697530 IC50 = 12.6 nM 7.90
CHEMBL3697535 IC50 = 13.1 nM 7.88
CHEMBL3697538 IC50 = 13.2 nM 7.88
CHEMBL3697519 IC50 = 13.3 nM 7.88
CHEMBL3697527 IC50 = 13.4 nM 7.87
CHEMBL3697541 IC50 = 14.4 nM 7.84
CHEMBL3697550 IC50 = 14.9 nM 7.83
CHEMBL3697536 IC50 = 15.2 nM 7.82
CHEMBL3697545 IC50 = 17.1 nM 7.77
CHEMBL3697552 IC50 = 19.6 nM 7.71
CHEMBL3697533 IC50 = 20.0 nM 7.70
CHEMBL3697532 IC50 = 20.0 nM 7.70
CHEMBL3697537 IC50 = 20.3 nM 7.69
CHEMBL3697546 IC50 = 30.8 nM 7.51
CHEMBL3697528 IC50 = 36.5 nM 7.44
CHEMBL3697523 IC50 = 40.4 nM 7.39
CHEMBL3697529 IC50 = 51.1 nM 7.29
CHEMBL3697513 IC50 = 63.4 nM 7.20
CHEMBL3697512 IC50 = 95.3 nM 7.02
CHEMBL3697522 IC50 = 94.8 nM 7.02
CHEMBL3697547 IC50 = 97.7 nM 7.01
CHEMBL3697549 IC50 = 100.5 nM 7.00
CHEMBL3697526 IC50 = 118.3 nM 6.93
CHEMBL3697517 IC50 = 481.9 nM 6.32
CHEMBL3639963 IC50 = 1905.5 nM 5.72
CHEMBL3697514 IC50 = 2296.2 nM 5.64
CHEMBL3697524 IC50 = 3698.3 nM 5.43
CHEMBL3697518 IC50 = 5688.5 nM 5.25
CHEMBL3697510 IC50 > 10000.0 nM -