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Assay Detail

CHEMBL3707812

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Fluorescent-Based (Inhibitor) Screening Assay: Human recombinant monoamine oxidase proteins MAO-A and MAO-B were purchased from Sigma Aldrich. MAOs catalyze the oxidative deamination of 1, 2 and 3 amines. In order to monitor MAO enzymatic activities and/or their inhibition rate by inhibitor(s) of interest, a fluorescent-based (inhibitor)-screening assay was set up. 3-(2-Aminophenyl)-3-oxopropamamine (kynuramine dihydrobromide, Sigma Aldrich), a non fluorescent compound was chosen as a substrate. Kynuramine is a non-specific substrate for both MAOs activities. While undergoing oxidative deamination by MAO activities, kynuramine is converted into 4-hydroxyquinoline (4-HQ), a resulting fluorescent product.The monoamine oxidase activity was estimated by measuring the conversion of kynuramine into 4-hydroxyquinoline. Assays were conducted in 96-well black plates with clear bottom (Corning) in a final volume of 100 uL. The assay buffer was 100 mM HEPES, pH 7.5. Each experiment was performed in triplicate within the same experiment.
58
Total Activities
58
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Amine oxidase [flavin-containing] B (CHEMBL2039)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Phenylcyclopropylamine derivatives and their medical use
(2015)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 58 5.14 6.22

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3989843 TRANYLCYPROMINE 4.0 1 6.22
CHEMBL3651093 1 6.00
CHEMBL3651140 1 5.82
CHEMBL3651113 1 5.72
CHEMBL3651102 1 5.70
CHEMBL3651147 1 5.68
CHEMBL3651124 1 5.66
CHEMBL3651105 1 5.64
CHEMBL3651148 1 5.64
CHEMBL3651123 1 5.62
CHEMBL3651139 1 5.60
CHEMBL3651108 1 5.52
CHEMBL3651110 1 5.52
CHEMBL3651114 1 5.48
CHEMBL3651125 1 5.46
CHEMBL3651101 1 5.40
CHEMBL3651118 1 5.27
CHEMBL3651107 1 5.27
CHEMBL3651103 1 5.22
CHEMBL3651109 1 5.22
CHEMBL3651111 1 5.21
CHEMBL3651092 1 5.16
CHEMBL3651151 1 5.13
CHEMBL3651112 1 5.10
CHEMBL3651104 1 5.10
CHEMBL3651145 1 5.10
CHEMBL3651120 1 5.09
CHEMBL3651136 1 5.07
CHEMBL3651128 1 5.02
CHEMBL3651138 1 5.02

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3989843 TRANYLCYPROMINE IC50 = 600.0 nM 6.22
CHEMBL3651093 IC50 = 1000.0 nM 6.00
CHEMBL3651140 IC50 = 1500.0 nM 5.82
CHEMBL3651113 IC50 = 1900.0 nM 5.72
CHEMBL3651102 IC50 = 2000.0 nM 5.70
CHEMBL3651147 IC50 = 2100.0 nM 5.68
CHEMBL3651124 IC50 = 2200.0 nM 5.66
CHEMBL3651105 IC50 = 2300.0 nM 5.64
CHEMBL3651148 IC50 = 2300.0 nM 5.64
CHEMBL3651123 IC50 = 2400.0 nM 5.62
CHEMBL3651139 IC50 = 2500.0 nM 5.60
CHEMBL3651108 IC50 = 3000.0 nM 5.52
CHEMBL3651110 IC50 = 3000.0 nM 5.52
CHEMBL3651114 IC50 = 3300.0 nM 5.48
CHEMBL3651125 IC50 = 3500.0 nM 5.46
CHEMBL3651101 IC50 = 4000.0 nM 5.40
CHEMBL3651118 IC50 = 5400.0 nM 5.27
CHEMBL3651107 IC50 = 5330.0 nM 5.27
CHEMBL3651103 IC50 = 6000.0 nM 5.22
CHEMBL3651109 IC50 = 6000.0 nM 5.22
CHEMBL3651111 IC50 = 6100.0 nM 5.21
CHEMBL3651092 IC50 = 7000.0 nM 5.16
CHEMBL3651151 IC50 = 7400.0 nM 5.13
CHEMBL3651145 IC50 = 7900.0 nM 5.10
CHEMBL3651112 IC50 = 8000.0 nM 5.10
CHEMBL3651104 IC50 = 8000.0 nM 5.10
CHEMBL3651120 IC50 = 8100.0 nM 5.09
CHEMBL3651136 IC50 = 8600.0 nM 5.07
CHEMBL3651128 IC50 = 9600.0 nM 5.02
CHEMBL3651138 IC50 = 9500.0 nM 5.02
CHEMBL3651146 IC50 = 9800.0 nM 5.01
CHEMBL3651135 IC50 = 9800.0 nM 5.01
CHEMBL3651091 IC50 = 10000.0 nM 5.00
CHEMBL3651100 IC50 = 10000.0 nM 5.00
CHEMBL3651129 IC50 = 10400.0 nM 4.98
CHEMBL3651094 IC50 = 11000.0 nM 4.96
CHEMBL3639499 IC50 = 13000.0 nM 4.89
CHEMBL3651137 IC50 = 13800.0 nM 4.86
CHEMBL3651096 IC50 = 14000.0 nM 4.85
CHEMBL3651126 IC50 = 14000.0 nM 4.85
CHEMBL3651119 IC50 = 15500.0 nM 4.81
CHEMBL3651099 IC50 = 16000.0 nM 4.80
CHEMBL3651095 IC50 = 17000.0 nM 4.77
CHEMBL3651117 IC50 = 18200.0 nM 4.74
CHEMBL3651134 IC50 = 21600.0 nM 4.67
CHEMBL3651122 IC50 = 24000.0 nM 4.62
CHEMBL3651142 IC50 = 23800.0 nM 4.62
CHEMBL3651141 IC50 = 25300.0 nM 4.60
CHEMBL3651097 IC50 = 28000.0 nM 4.55
CHEMBL3651121 IC50 = 34300.0 nM 4.46