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Assay Detail

CHEMBL3707937

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
In Vitro Assay: The in vitro affinity of the compounds of the present invention for the CXCR1 and CXCR2 receptors was determined on a functional test of the .beta.-arrestin recruitment type after receptor activation.It was demonstrated that the activation by CXCL8 of the CXCR2 receptor in cells of the PathHunter HEK293-CXCR2 line or of the CXCR1 receptor in cells of the U2OS h CXCR1 .beta.-arrestin line results in the recruitment of .beta.-arrestin (Richardson et al. 2003 Role of the cytoplasmic tails of CXCR1 and CXCR2 in mediating leukocyte migration, activation, and regulation. J. Immunol. 170: 2904-2911.)In order to evaluate the direct interaction of the CXCR2 or CXCR1 receptor with .beta.-arrestin 2, a .beta.-arrestin 2 recruitment test for CXCR2 or CXCR1 based on of .beta.-galactosidase enzyme complementation (Olson K R, Eglen R M. Beta galactosidase complementation: a cell-based luminescent assay platform for drug discovery. Assay Drug Dev Technol. 2007 February; 5(1); 137-44).
37
Total Activities
36
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

C-X-C chemokine receptor type 2 (CHEMBL2434)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Disubstituted 3,4-diamino-3-cyclobutene-1,2-dione compounds for use in the treatment of chemokine-mediated pathologies
(2015)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 37 6.72 7.60

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3704565 1 7.60
CHEMBL3704569 1 7.58
CHEMBL3704573 1 7.52
CHEMBL3701196 1 7.51
CHEMBL3704564 2 7.50
CHEMBL3701188 1 7.43
CHEMBL3640000 1 7.22
CHEMBL3704571 1 7.14
CHEMBL3704570 1 7.14
CHEMBL3640034 1 7.02
CHEMBL3701190 1 7.00
CHEMBL3701187 1 7.00
CHEMBL3701184 1 6.97
CHEMBL3704561 1 6.97
CHEMBL3704562 1 6.84
CHEMBL3704563 1 6.70
CHEMBL3704555 1 6.61
CHEMBL3701195 1 6.59
CHEMBL3701191 1 6.58
CHEMBL3701183 1 6.57
CHEMBL3704568 1 6.51
CHEMBL3701194 1 6.47
CHEMBL3701185 1 6.47
CHEMBL3704558 1 6.46
CHEMBL3704572 1 6.43
CHEMBL3701193 1 6.41
CHEMBL3704557 1 6.36
CHEMBL3704556 1 6.32
CHEMBL3704567 1 6.30
CHEMBL3701189 1 6.26

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3704565 IC50 = 25.0 nM 7.60
CHEMBL3704569 IC50 = 26.0 nM 7.58
CHEMBL3704573 IC50 = 30.0 nM 7.52
CHEMBL3701196 IC50 = 31.0 nM 7.51
CHEMBL3704564 IC50 = 32.0 nM 7.50
CHEMBL3701188 IC50 = 37.0 nM 7.43
CHEMBL3640000 IC50 = 60.0 nM 7.22
CHEMBL3704571 IC50 = 72.0 nM 7.14
CHEMBL3704570 IC50 = 72.0 nM 7.14
CHEMBL3640034 IC50 = 96.0 nM 7.02
CHEMBL3701190 IC50 = 100.0 nM 7.00
CHEMBL3701187 IC50 = 100.0 nM 7.00
CHEMBL3701184 IC50 = 106.0 nM 6.97
CHEMBL3704561 IC50 = 106.0 nM 6.97
CHEMBL3704562 IC50 = 146.0 nM 6.84
CHEMBL3704563 IC50 = 198.0 nM 6.70
CHEMBL3704564 IC50 = 207.0 nM 6.68
CHEMBL3704555 IC50 = 244.0 nM 6.61
CHEMBL3701195 IC50 = 257.0 nM 6.59
CHEMBL3701191 IC50 = 262.0 nM 6.58
CHEMBL3701183 IC50 = 272.0 nM 6.57
CHEMBL3704568 IC50 = 311.0 nM 6.51
CHEMBL3701194 IC50 = 335.0 nM 6.47
CHEMBL3701185 IC50 = 341.0 nM 6.47
CHEMBL3704558 IC50 = 349.0 nM 6.46
CHEMBL3704572 IC50 = 373.0 nM 6.43
CHEMBL3701193 IC50 = 394.0 nM 6.41
CHEMBL3704557 IC50 = 433.0 nM 6.36
CHEMBL3704556 IC50 = 475.0 nM 6.32
CHEMBL3704567 IC50 = 502.0 nM 6.30
CHEMBL3701189 IC50 = 549.0 nM 6.26
CHEMBL3701192 IC50 = 626.0 nM 6.20
CHEMBL3704559 IC50 = 716.0 nM 6.14
CHEMBL3704574 IC50 = 733.0 nM 6.13
CHEMBL3704560 IC50 = 962.0 nM 6.02
CHEMBL3704566 IC50 = 1035.0 nM 5.99
CHEMBL3701186 IC50 = 1088.0 nM 5.96