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Assay Detail

CHEMBL3762511

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Inhibition of recombinant human HDAC6 using Boc-Lys(Ac)-AMC as substrate preincubated for 15 mins followed by substrate addition measured after 60 mins by fluorescence-based assay
18
Total Activities
18
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Histone deacetylase 6 (CHEMBL1865)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Identification of N-(6-mercaptohexyl)-3-(4-pyridyl)-1H-pyrazole-5-carboxamide and its disulfide prodrug as potent histone deacetylase inhibitors with in vitro and in vivo anti-tumor efficacy.
Wen J, Bao Y, Niu Q, Yang J, Fan Y, Li J, Jing Y, Zhao L, Liu D.
Eur J Med Chem (2016) 109 : 350 -359
PubMed 26814680 · DOI

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 18 7.11 7.75

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3759562 1 7.75
CHEMBL3760013 1 7.66
CHEMBL3758882 1 7.58
CHEMBL3758261 1 7.57
CHEMBL3759791 1 7.52
CHEMBL3759322 1 7.48
CHEMBL3760115 1 7.25
CHEMBL325676 1 7.13
CHEMBL98 VORINOSTAT 4.0 1 7.09
CHEMBL3759998 1 7.08
CHEMBL3759941 1 7.04
CHEMBL3758334 1 6.97
CHEMBL3760046 1 6.78
CHEMBL3759836 1 6.63
CHEMBL3758451 1 6.62
CHEMBL3758595 1 6.61
CHEMBL3758444 1 6.12
CHEMBL3758409 1 -

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3759562 IC50 = 18.0 nM 7.75
CHEMBL3760013 IC50 = 22.0 nM 7.66
CHEMBL3758882 IC50 = 26.0 nM 7.58
CHEMBL3758261 IC50 = 27.0 nM 7.57
CHEMBL3759791 IC50 = 30.0 nM 7.52
CHEMBL3759322 IC50 = 33.0 nM 7.48
CHEMBL3760115 IC50 = 56.0 nM 7.25
CHEMBL325676 IC50 = 74.0 nM 7.13
CHEMBL98 VORINOSTAT IC50 = 82.0 nM 7.09
CHEMBL3759998 IC50 = 84.0 nM 7.08
CHEMBL3759941 IC50 = 92.0 nM 7.04
CHEMBL3758334 IC50 = 106.0 nM 6.97
CHEMBL3760046 IC50 = 167.0 nM 6.78
CHEMBL3759836 IC50 = 235.0 nM 6.63
CHEMBL3758451 IC50 = 241.0 nM 6.62
CHEMBL3758595 IC50 = 244.0 nM 6.61
CHEMBL3758444 IC50 = 758.0 nM 6.12
CHEMBL3758409 IC50 - -