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Assay Detail

CHEMBL3887218

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Scintillation Proximity Assay (SPA) Assay: SPA membrane binding assay was used to identify inhibitors of [33P] 2MeS-ADP binding to cloned human P2Yi receptors (The P2Yi receptor membranes were provided by Biology and the cloning of the receptor and P2Yi receptor membrane preparation is same as described by Biology). Binding reactions were performed in 384- well OptiPlates (PerkinElmer Life Sciences, Cat # 6007299) in a volume of 50 ui containing -15 fmol of P2Y1 receptor (1.7 ug of total protein), 0.3 nM [33P] 2MeS-ADP(PerkinElmer; 2,000 Ci/mmol), various concentrations of the test compound (usually between 10 uM and 160 pM) in Buffer B containing 1% DMSO in assay buffer (15 mM, HEPES, 145 mM potassium chloride, 5 mM sodium Chloride, 5 mM EDTA, 0.1 mM MgCl2, pH 7.4) and 100 ug of SPA bead (WGA polystyrene Image beads, #RPNQ 0260V, Amersham). Reactions were allowed to proceed to completion at room temperature for 1 hour followed by centrifugation of the plate for 5 min.
40
Total Activities
40
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

P2Y purinoceptor 1 (CHEMBL4315)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Amino-heteroaryl 7-hydroxy-spiropiperidine indolinyl antagonists of P2Y1 receptor
(2015)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 40 7.77 8.52

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3920135 1 8.52
CHEMBL3263070 1 8.30
CHEMBL3263058 1 8.22
CHEMBL3903953 1 8.22
CHEMBL3932713 1 8.17
CHEMBL3896467 1 8.15
CHEMBL3967844 1 8.10
CHEMBL3263069 1 8.10
CHEMBL3926419 1 8.10
CHEMBL3973199 1 8.05
CHEMBL3263068 1 8.00
CHEMBL3263057 1 8.00
CHEMBL3900332 1 7.96
CHEMBL3928274 1 7.92
CHEMBL3263071 1 7.89
CHEMBL3263074 1 7.89
CHEMBL3893716 1 7.82
CHEMBL3263073 1 7.80
CHEMBL3263066 1 7.80
CHEMBL3263062 1 7.80
CHEMBL3927367 1 7.72
CHEMBL3905619 1 7.72
CHEMBL3918409 1 7.72
CHEMBL3981201 1 7.68
CHEMBL3911187 1 7.66
CHEMBL3929983 1 7.66
CHEMBL3979693 1 7.64
CHEMBL3893862 1 7.64
CHEMBL3890364 1 7.62
CHEMBL3263067 1 7.58

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3920135 IC50 = 3.0 nM 8.52
CHEMBL3263070 IC50 = 5.0 nM 8.30
CHEMBL3263058 IC50 = 6.0 nM 8.22
CHEMBL3903953 IC50 = 6.0 nM 8.22
CHEMBL3932713 IC50 = 6.8 nM 8.17
CHEMBL3896467 IC50 = 7.0 nM 8.15
CHEMBL3967844 IC50 = 8.0 nM 8.10
CHEMBL3263069 IC50 = 8.0 nM 8.10
CHEMBL3926419 IC50 = 8.0 nM 8.10
CHEMBL3973199 IC50 = 9.0 nM 8.05
CHEMBL3263057 IC50 = 10.0 nM 8.00
CHEMBL3263068 IC50 = 10.0 nM 8.00
CHEMBL3900332 IC50 = 11.0 nM 7.96
CHEMBL3928274 IC50 = 12.0 nM 7.92
CHEMBL3263074 IC50 = 13.0 nM 7.89
CHEMBL3263071 IC50 = 13.0 nM 7.89
CHEMBL3893716 IC50 = 15.0 nM 7.82
CHEMBL3263073 IC50 = 16.0 nM 7.80
CHEMBL3263066 IC50 = 16.0 nM 7.80
CHEMBL3263062 IC50 = 16.0 nM 7.80
CHEMBL3927367 IC50 = 19.0 nM 7.72
CHEMBL3918409 IC50 = 19.0 nM 7.72
CHEMBL3905619 IC50 = 19.0 nM 7.72
CHEMBL3981201 IC50 = 21.0 nM 7.68
CHEMBL3911187 IC50 = 22.0 nM 7.66
CHEMBL3929983 IC50 = 22.0 nM 7.66
CHEMBL3979693 IC50 = 23.0 nM 7.64
CHEMBL3893862 IC50 = 23.0 nM 7.64
CHEMBL3890364 IC50 = 24.0 nM 7.62
CHEMBL3263067 IC50 = 26.0 nM 7.58
CHEMBL3263072 IC50 = 28.0 nM 7.55
CHEMBL3902900 IC50 = 28.0 nM 7.55
CHEMBL3898478 IC50 = 33.0 nM 7.48
CHEMBL3968470 IC50 = 37.0 nM 7.43
CHEMBL3956460 IC50 = 40.2 nM 7.40
CHEMBL3901946 IC50 = 48.0 nM 7.32
CHEMBL3932841 IC50 = 60.0 nM 7.22
CHEMBL3263060 IC50 = 66.0 nM 7.18
CHEMBL3972991 IC50 = 66.0 nM 7.18
CHEMBL3974841 IC50 = 69.0 nM 7.16