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Assay Detail

CHEMBL3887296

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
P70S6K Enzyme Assay: P70S6K inhibitor compounds are diluted and plated in 96 well plates. A reaction mixture including the following components is then added to the compound plate to initiate the enzyme reaction; P70S6K (3 nM, T412E mutant, Millipore) is mixed with 24 uM ATP in an assay buffer containing 100 mM Hepes (pH 7.5), 5 mM MgCl2, 1 mM DTT, 0.015% Brij and 1 uM of the substrate peptide FITC-AHA-AKRRRLSSLRA-OH (derived from the S6 ribosomal protein sequence, FITC=fluorescein isothiocyanate, AHA=6-aminohexanoic acid). The reaction is incubated for 90 min at 25.degree. C., before the addition of 10 mM EDTA to stop the reaction. The proportion of substrate and product (phosphorylated) peptide is analysed on a Caliper Life Sciences Lab Chip 3000, using a pressure of -1.4 psi, and upstream and downstream voltages of -3000 and -700 respectively. Product peaks are resolved before substrate peaks on the resulting chromatograms.
400
Total Activities
399
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

Ribosomal protein S6 kinase beta-1 (CHEMBL4501)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Imidazole amines as modulators of kinase activity
(2015)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 400 8.33 10.22

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3936990 1 10.22
CHEMBL3899716 1 10.00
CHEMBL3966806 1 9.96
CHEMBL3906990 1 9.70
CHEMBL3980521 1 9.70
CHEMBL3981085 1 9.59
CHEMBL3894849 1 9.40
CHEMBL3943127 1 9.36
CHEMBL3977147 1 9.30
CHEMBL3971598 1 9.30
CHEMBL3978595 1 9.30
CHEMBL3904322 1 9.22
CHEMBL3910789 1 9.22
CHEMBL3919089 1 9.22
CHEMBL3941283 1 9.22
CHEMBL3965271 1 9.15
CHEMBL3891980 1 9.15
CHEMBL3961056 1 9.15
CHEMBL3957657 1 9.14
CHEMBL3966203 1 9.10
CHEMBL3912632 1 9.10
CHEMBL3928772 1 9.10
CHEMBL3967010 1 9.10
CHEMBL3949201 1 9.10
CHEMBL3913464 1 9.10
CHEMBL3972479 1 9.10
CHEMBL3963056 1 9.10
CHEMBL3962020 1 9.05
CHEMBL3941451 1 9.05
CHEMBL3906695 1 9.05

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3936990 IC50 = 0.06 nM 10.22
CHEMBL3899716 IC50 = 0.1 nM 10.00
CHEMBL3966806 IC50 = 0.11 nM 9.96
CHEMBL3980521 IC50 = 0.2 nM 9.70
CHEMBL3906990 IC50 = 0.2 nM 9.70
CHEMBL3981085 IC50 = 0.26 nM 9.59
CHEMBL3894849 IC50 = 0.4 nM 9.40
CHEMBL3943127 IC50 = 0.44 nM 9.36
CHEMBL3971598 IC50 = 0.5 nM 9.30
CHEMBL3977147 IC50 = 0.5 nM 9.30
CHEMBL3978595 IC50 = 0.5 nM 9.30
CHEMBL3910789 IC50 = 0.6 nM 9.22
CHEMBL3941283 IC50 = 0.6 nM 9.22
CHEMBL3919089 IC50 = 0.6 nM 9.22
CHEMBL3904322 IC50 = 0.6 nM 9.22
CHEMBL3891980 IC50 = 0.7 nM 9.15
CHEMBL3961056 IC50 = 0.7 nM 9.15
CHEMBL3965271 IC50 = 0.7 nM 9.15
CHEMBL3957657 IC50 = 0.73 nM 9.14
CHEMBL3928772 IC50 = 0.8 nM 9.10
CHEMBL3913464 IC50 = 0.8 nM 9.10
CHEMBL3912632 IC50 = 0.8 nM 9.10
CHEMBL3967010 IC50 = 0.8 nM 9.10
CHEMBL3949201 IC50 = 0.8 nM 9.10
CHEMBL3963056 IC50 = 0.8 nM 9.10
CHEMBL3972479 IC50 = 0.8 nM 9.10
CHEMBL3966203 IC50 = 0.8 nM 9.10
CHEMBL3906695 IC50 = 0.9 nM 9.05
CHEMBL3919834 IC50 = 0.9 nM 9.05
CHEMBL3969016 IC50 = 0.9 nM 9.05
CHEMBL3941451 IC50 = 0.9 nM 9.05
CHEMBL3940627 IC50 = 0.9 nM 9.05
CHEMBL3928074 IC50 = 0.9 nM 9.05
CHEMBL3962020 IC50 = 0.9 nM 9.05
CHEMBL3927358 IC50 = 0.9 nM 9.05
CHEMBL3933597 IC50 = 1.0 nM 9.00
CHEMBL3948085 IC50 = 1.0 nM 9.00
CHEMBL3890352 IC50 = 1.0 nM 9.00
CHEMBL3940867 IC50 = 1.0 nM 9.00
CHEMBL3938454 IC50 = 1.0 nM 9.00
CHEMBL3951747 IC50 = 1.0 nM 9.00
CHEMBL3983282 IC50 = 1.1 nM 8.96
CHEMBL3912769 IC50 = 1.1 nM 8.96
CHEMBL3980922 IC50 = 1.1 nM 8.96
CHEMBL3968744 IC50 = 1.1 nM 8.96
CHEMBL3974201 IC50 = 1.1 nM 8.96
CHEMBL3960355 IC50 = 1.1 nM 8.96
CHEMBL3954781 IC50 = 1.1 nM 8.96
CHEMBL3962807 IC50 = 1.2 nM 8.92
CHEMBL3916178 IC50 = 1.2 nM 8.92