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Assay Detail

CHEMBL3887327

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Kinase Glo Plus Assay: Human RSK2 protein, purchased from Invitrogen, is used to measure kinase activity utilizing Kinase Glo Plus (Promega) a homogeneous assay technology, which uses a luciferin-luciferase based ATP detection reagent to quantify residual ATP. The assay is performed using 0.75 nM His-RSK2, 0.75 .mu.M ATP and 1.0 uM S6 Kinase/RSK Substrate Peptide 1 (Upstate, catalog #12-124), in assay buffer consisting of 25 mM HEPES, pH 7.5, 10 mM MgCl2, 5 mM MnCl2, 50 mM KCl, 0.2% BSA, 0.01% CHAPS, 100 uM Na3VO4, 0.5 mM DTT, and 1% DMSO. Solutions of test compounds at various concentrations are prepared by 1:3 fold serial dilution of a 1 mM solution of compound in DMSO. The DMSO solutions are further diluted with assay buffer to a final concentration of DMSO of 5%. The assay is performed in a 384 well, white, non-binding plate (Corning, catalogue #3574). Solutions of test compounds (10 uL) are transferred to a dry assay plate, followed by addition of 20 uL kinase.
239
Total Activities
237
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

Ribosomal protein S6 kinase alpha-2 (CHEMBL3906)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Heterocyclic compounds containing an indole core
(2015)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 239 7.50 9.74

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3956539 1 9.74
CHEMBL3945993 1 9.60
CHEMBL3903528 1 9.42
CHEMBL3900064 1 9.38
CHEMBL3959915 1 9.23
CHEMBL4109143 1 9.22
CHEMBL3955947 1 9.22
CHEMBL3908561 1 9.21
CHEMBL3972132 1 9.20
CHEMBL4108521 1 9.19
CHEMBL4113357 1 9.15
CHEMBL4111661 1 9.15
CHEMBL3951802 1 9.11
CHEMBL3985027 1 9.05
CHEMBL1933288 1 8.96
CHEMBL1933280 1 8.96
CHEMBL3939884 1 8.89
CHEMBL3942136 1 8.89
CHEMBL4112559 1 8.85
CHEMBL3918100 1 8.80
CHEMBL3904474 1 8.74
CHEMBL3963988 1 8.74
CHEMBL3900130 1 8.74
CHEMBL3980724 1 8.72
CHEMBL4113926 2 8.72
CHEMBL4109800 1 8.72
CHEMBL1933278 1 8.72
CHEMBL3965519 1 8.70
CHEMBL3910099 1 8.70
CHEMBL4111985 2 8.68

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3956539 IC50 = 0.18 nM 9.74
CHEMBL3945993 IC50 = 0.25 nM 9.60
CHEMBL3903528 IC50 = 0.38 nM 9.42
CHEMBL3900064 IC50 = 0.42 nM 9.38
CHEMBL3959915 IC50 = 0.59 nM 9.23
CHEMBL4109143 IC50 = 0.6 nM 9.22
CHEMBL3955947 IC50 = 0.6 nM 9.22
CHEMBL3908561 IC50 = 0.62 nM 9.21
CHEMBL3972132 IC50 = 0.63 nM 9.20
CHEMBL4108521 IC50 = 0.64 nM 9.19
CHEMBL4113357 IC50 = 0.7 nM 9.15
CHEMBL4111661 IC50 = 0.71 nM 9.15
CHEMBL3951802 IC50 = 0.77 nM 9.11
CHEMBL3985027 IC50 = 0.89 nM 9.05
CHEMBL1933288 IC50 = 1.1 nM 8.96
CHEMBL1933280 IC50 = 1.1 nM 8.96
CHEMBL3942136 IC50 = 1.3 nM 8.89
CHEMBL3939884 IC50 = 1.3 nM 8.89
CHEMBL4112559 IC50 = 1.4 nM 8.85
CHEMBL3918100 IC50 = 1.6 nM 8.80
CHEMBL3900130 IC50 = 1.8 nM 8.74
CHEMBL3963988 IC50 = 1.8 nM 8.74
CHEMBL3904474 IC50 = 1.8 nM 8.74
CHEMBL4113926 IC50 = 1.9 nM 8.72
CHEMBL3980724 IC50 = 1.9 nM 8.72
CHEMBL4109800 IC50 = 1.9 nM 8.72
CHEMBL1933278 IC50 = 1.9 nM 8.72
CHEMBL3965519 IC50 = 2.0 nM 8.70
CHEMBL3910099 IC50 = 2.0 nM 8.70
CHEMBL3966733 IC50 = 2.1 nM 8.68
CHEMBL4111985 IC50 = 2.1 nM 8.68
CHEMBL3969149 IC50 = 2.2 nM 8.66
CHEMBL3946668 IC50 = 2.5 nM 8.60
CHEMBL3917125 IC50 = 2.6 nM 8.59
CHEMBL3916626 IC50 = 3.0 nM 8.52
CHEMBL4107750 IC50 = 3.4 nM 8.47
CHEMBL4110776 IC50 = 3.6 nM 8.44
CHEMBL1933142 IC50 = 3.7 nM 8.43
CHEMBL3936149 IC50 = 3.8 nM 8.42
CHEMBL3916789 IC50 = 4.0 nM 8.40
CHEMBL3921354 IC50 = 4.0 nM 8.40
CHEMBL4108963 IC50 = 4.3 nM 8.37
CHEMBL1938803 IC50 = 4.4 nM 8.36
CHEMBL1933287 IC50 = 4.4 nM 8.36
CHEMBL3941501 IC50 = 4.8 nM 8.32
CHEMBL3955733 IC50 = 4.8 nM 8.32
CHEMBL3912033 IC50 = 4.9 nM 8.31
CHEMBL3961025 IC50 = 5.0 nM 8.30
CHEMBL3981684 IC50 = 5.1 nM 8.29
CHEMBL3917267 IC50 = 5.2 nM 8.28