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Assay Detail

CHEMBL3887360

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Functional
cAMP GloSensor Assay: HEK293T cells co-expressing the cAMP biosensor GloSensor-22F (Promega) and hD2 receptors were seeded (10,000 cells/20 ul/well) into white, clear-bottom, tissue culture plates in HBSS, 10% FBS, 20 mM HEPES, pH 7.4. After a one- to two-hour recovery, cells were treated with 10 ul of 3x test or reference drug prepared in HBSS, 10% FBS, 20 mM HEPES, pH 7.4. After 30 minutes, cells were challenged with 10 ul of 1,200 nM (4x) isoproterenol in 8% (4x) GloSensor reagent. Luminescence per well per second was read on a Wallac TriLux microbeta plate counter. Data were normalized to the isoproterenol response (100%) and the maximal quinpirole-induced inhibition thereof (0%) and regressed using the sigmoidal dose-response function built into GraphPad Prism 4.0. Notably, HEK293T cells expressing the GloSensor-22F alone (no hD2) were assayed in parallel and displayed no inhibition of isoproterenol-stimulated cAMP.
25
Total Activities
25
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Functional
Organism Homo sapiens
Cell Type HEK-293T
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

D(2) dopamine receptor (CHEMBL217)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Functionally selective ligands of dopamine D2 receptors
(2015)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
EC50 25 7.45 10.00

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3921903 1 10.00
CHEMBL3978288 1 9.70
CHEMBL3912435 1 9.40
CHEMBL3983588 1 8.74
CHEMBL2165118 1 8.25
CHEMBL2165132 1 8.24
CHEMBL2165134 1 8.24
CHEMBL3918805 1 8.21
CHEMBL2165139 1 8.01
CHEMBL2165116 1 8.01
CHEMBL3937643 1 7.96
CHEMBL2165119 1 7.89
CHEMBL3916047 1 7.89
CHEMBL2165137 1 7.68
CHEMBL3944009 1 7.57
CHEMBL2165126 1 6.90
CHEMBL3973357 1 6.79
CHEMBL3929710 1 6.65
CHEMBL3957278 1 6.51
CHEMBL2165140 1 6.46
CHEMBL3934712 1 6.29
CHEMBL2165129 1 6.00
CHEMBL2165133 1 5.43
CHEMBL3943838 1 5.01
CHEMBL3903542 1 4.34

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3921903 EC50 = 0.1 nM 10.00
CHEMBL3978288 EC50 = 0.2 nM 9.70
CHEMBL3912435 EC50 = 0.4 nM 9.40
CHEMBL3983588 EC50 = 1.8 nM 8.74
CHEMBL2165118 EC50 = 5.6 nM 8.25
CHEMBL2165132 EC50 = 5.7 nM 8.24
CHEMBL2165134 EC50 = 5.7 nM 8.24
CHEMBL3918805 EC50 = 6.1 nM 8.21
CHEMBL2165139 EC50 = 9.8 nM 8.01
CHEMBL2165116 EC50 = 9.7 nM 8.01
CHEMBL3937643 EC50 = 11.0 nM 7.96
CHEMBL2165119 EC50 = 13.0 nM 7.89
CHEMBL3916047 EC50 = 13.0 nM 7.89
CHEMBL2165137 EC50 = 21.0 nM 7.68
CHEMBL3944009 EC50 = 27.0 nM 7.57
CHEMBL2165126 EC50 = 126.0 nM 6.90
CHEMBL3973357 EC50 = 163.0 nM 6.79
CHEMBL3929710 EC50 = 222.0 nM 6.65
CHEMBL3957278 EC50 = 306.0 nM 6.51
CHEMBL2165140 EC50 = 348.0 nM 6.46
CHEMBL3934712 EC50 = 512.0 nM 6.29
CHEMBL2165129 EC50 = 1000.0 nM 6.00
CHEMBL2165133 EC50 = 3700.0 nM 5.43
CHEMBL3943838 EC50 = 9870.0 nM 5.01
CHEMBL3903542 EC50 = 46000.0 nM 4.34