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Assay Detail

CHEMBL3887514

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Functional
GPR6 In Vitro Assay (A.1): This cell based assay measures the ability of compounds to inhibit the constitutive cAMP activity of GPR6 receptor expressed in CHO-K1 cells. CHO cells were stably expressed with GPR6 receptor, whose expression is controlled by a tetracycline inducable element. The cells were cultured in medium containing F12K, 10% FBS, 1% PennStrep, 200 ug/mL Hygromycin. GPR6 receptor expression was induced for 20 hrs with 1 ug/ml doxycycline (sigma D9891) in growth media. After addition of doxycycline cells were plated at a density of 250-500 cells per well in half-volume black clear bottom plates (Costar) and place in an incubator (37° C, 5% C(O)2) for 20 hours prior to cAMP assays.Culture media was removed from cells and they were washed with 50 uL of Ringer's Buffer (MgCl2 0.047 mg/mL, NaH2PO4 0.18 mg/mL, Na2HPO4 0.1 mg/mL, KCl 0.34 mg/mL, NaHC(O)3 1.26 mg/mL, D-glucose 1.8 mg/mL, NaCl 7 mg/mL; pH=7.4). Compounds suspended in DMSO were diluted in Ringer's Buffer.
69
Total Activities
69
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Functional
Cell Type CHO
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

G-protein coupled receptor 6 (CHEMBL3714130)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Substituted pyrido[3,4-b]pyrazines as GPR6 modulators
(2015)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 69 10.42 10.98

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3892898 1 10.98
CHEMBL3909497 1 10.98
CHEMBL3931736 1 10.94
CHEMBL3905204 1 10.92
CHEMBL3962092 1 10.87
CHEMBL3955078 1 10.86
CHEMBL3915516 1 10.86
CHEMBL3982858 1 10.86
CHEMBL3971468 1 10.86
CHEMBL3957710 1 10.83
CHEMBL3935897 1 10.82
CHEMBL3976386 1 10.78
CHEMBL3943282 1 10.77
CHEMBL3967591 1 10.76
CHEMBL3908467 1 10.75
CHEMBL3963072 1 10.74
CHEMBL4113017 1 10.73
CHEMBL3986433 1 10.71
CHEMBL3925720 1 10.71
CHEMBL3943478 1 10.70
CHEMBL3949818 1 10.68
CHEMBL3905140 1 10.66
CHEMBL3923125 1 10.64
CHEMBL3985327 1 10.63
CHEMBL3921525 1 10.63
CHEMBL3967336 1 10.62
CHEMBL3945233 1 10.60
CHEMBL3948026 1 10.60
CHEMBL4111582 1 10.58
CHEMBL3911615 1 10.58

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3892898 IC50 = 0.0104 nM 10.98
CHEMBL3909497 IC50 = 0.0104 nM 10.98
CHEMBL3931736 IC50 = 0.0115 nM 10.94
CHEMBL3905204 IC50 = 0.012 nM 10.92
CHEMBL3962092 IC50 = 0.0134 nM 10.87
CHEMBL3955078 IC50 = 0.0138 nM 10.86
CHEMBL3915516 IC50 = 0.0138 nM 10.86
CHEMBL3982858 IC50 = 0.0137 nM 10.86
CHEMBL3971468 IC50 = 0.0138 nM 10.86
CHEMBL3957710 IC50 = 0.0149 nM 10.83
CHEMBL3935897 IC50 = 0.0152 nM 10.82
CHEMBL3976386 IC50 = 0.0166 nM 10.78
CHEMBL3943282 IC50 = 0.0168 nM 10.77
CHEMBL3967591 IC50 = 0.0173 nM 10.76
CHEMBL3908467 IC50 = 0.0179 nM 10.75
CHEMBL3963072 IC50 = 0.018 nM 10.74
CHEMBL4113017 IC50 = 0.0185 nM 10.73
CHEMBL3986433 IC50 = 0.0195 nM 10.71
CHEMBL3925720 IC50 = 0.0197 nM 10.71
CHEMBL3943478 IC50 = 0.0199 nM 10.70
CHEMBL3949818 IC50 = 0.0209 nM 10.68
CHEMBL3905140 IC50 = 0.0221 nM 10.66
CHEMBL3923125 IC50 = 0.023 nM 10.64
CHEMBL3985327 IC50 = 0.0232 nM 10.63
CHEMBL3921525 IC50 = 0.0237 nM 10.63
CHEMBL3967336 IC50 = 0.0239 nM 10.62
CHEMBL3948026 IC50 = 0.0249 nM 10.60
CHEMBL3945233 IC50 = 0.0249 nM 10.60
CHEMBL4111582 IC50 = 0.0265 nM 10.58
CHEMBL3911615 IC50 = 0.0266 nM 10.58
CHEMBL3924362 IC50 = 0.0269 nM 10.57
CHEMBL3945303 IC50 = 0.0298 nM 10.53
CHEMBL3975976 IC50 = 0.0314 nM 10.50
CHEMBL3927473 IC50 = 0.0327 nM 10.49
CHEMBL3951645 IC50 = 0.0325 nM 10.49
CHEMBL3935030 IC50 = 0.035 nM 10.46
CHEMBL3902681 IC50 = 0.0387 nM 10.41
CHEMBL3909048 IC50 = 0.052 nM 10.28
CHEMBL3939970 IC50 = 0.0552 nM 10.26
CHEMBL3987027 IC50 = 0.0572 nM 10.24
CHEMBL3912262 IC50 = 0.0626 nM 10.20
CHEMBL4113797 IC50 = 0.064 nM 10.19
CHEMBL3980074 IC50 = 0.068 nM 10.17
CHEMBL3961475 IC50 = 0.076 nM 10.12
CHEMBL3923277 IC50 = 0.0788 nM 10.10
CHEMBL3965124 IC50 = 0.085 nM 10.07
CHEMBL3980789 IC50 = 0.087 nM 10.06
CHEMBL3940326 IC50 = 0.088 nM 10.06
CHEMBL3902976 IC50 = 0.0866 nM 10.06
CHEMBL3927786 IC50 = 0.091 nM 10.04