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Assay Detail

CHEMBL3887536

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
HotSpot kinase assay: IC50s were determined using the in vitro HotSpot kinase assay (purified enzymes, 33P-ATP, an appropriate substrate and 1 μM ATP.). For enzyme inhibition assays, compounds were tested in range of ten concentrations from 10 uM to 0.0005 uM using purified enzymes and the Hotspot kinase assay. Reaction conditions were 1 uM ATP, one hour incubation with inhibitor, and kinase activity detected using 33-ATP phosphorylation of an appropriately selected peptide substrate.
21
Total Activities
19
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

Tyrosine-protein kinase Lck (CHEMBL258)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Inhibitors of bruton's tyrosine kinase
(2015)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 21 8.13 9.12

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3893004 1 9.12
CHEMBL3912266 1 9.06
CHEMBL3647967 2 9.00
CHEMBL4109796 1 8.81
CHEMBL1873475 IBRUTINIB 4.0 2 8.70
CHEMBL4106607 1 8.68
CHEMBL3903870 1 8.61
CHEMBL3917698 1 8.59
CHEMBL3905432 1 8.42
CHEMBL4107879 1 8.23
CHEMBL3903249 1 8.22
CHEMBL3921017 1 8.18
CHEMBL3910496 1 8.03
CHEMBL3921655 1 7.66
CHEMBL3894102 1 7.59
CHEMBL3982014 1 7.01
CHEMBL3894938 1 6.68
CHEMBL4110614 1 6.63
CHEMBL3915538 1 5.87

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3893004 IC50 = 0.76 nM 9.12
CHEMBL3912266 IC50 = 0.88 nM 9.06
CHEMBL3647967 IC50 = 1.0 nM 9.00
CHEMBL3647967 IC50 = 1.0 nM 9.00
CHEMBL4109796 IC50 = 1.56 nM 8.81
CHEMBL1873475 IBRUTINIB IC50 = 2.0 nM 8.70
CHEMBL1873475 IBRUTINIB IC50 = 2.0 nM 8.70
CHEMBL4106607 IC50 = 2.07 nM 8.68
CHEMBL3903870 IC50 = 2.43 nM 8.61
CHEMBL3917698 IC50 = 2.6 nM 8.59
CHEMBL3905432 IC50 = 3.82 nM 8.42
CHEMBL4107879 IC50 = 5.9 nM 8.23
CHEMBL3903249 IC50 = 5.97 nM 8.22
CHEMBL3921017 IC50 = 6.62 nM 8.18
CHEMBL3910496 IC50 = 9.24 nM 8.03
CHEMBL3921655 IC50 = 22.12 nM 7.66
CHEMBL3894102 IC50 = 25.81 nM 7.59
CHEMBL3982014 IC50 = 98.59 nM 7.01
CHEMBL3894938 IC50 = 208.0 nM 6.68
CHEMBL4110614 IC50 = 235.4 nM 6.63
CHEMBL3915538 IC50 = 1346.0 nM 5.87