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Assay Detail

CHEMBL3887550

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
High-Throughput Screening Assay: To identify novel inhibitors of hepsin, the Chembridge DIVERSet 10,000 compound high-diversity library was screened using an assay based on the cleavage of the chromogenic peptide. In addition, the NINDS II library of 1040 compounds (MicroSource Discovery) was screened to identify hepsin inhibitors among established drugs and known bioactive molecules. Screens were performed in a 96-well format at a final compound concentration of 2 uM. To minimize false positives, positions 1 and 12 of each row contained DMSO/buffer controls. As a measure of reproducibility, the Z' score for this assay was 0.78 (Zhang et al., 1999 J Biomol Screen 4:67).
16
Total Activities
16
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

Serine protease hepsin (CHEMBL2079849)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Hepsin inhibitors
(2015)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 16 6.13 6.64

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL46469 ANTHRALIN 2.0 1 6.64
CHEMBL3188992 1 6.55
CHEMBL3933764 1 6.48
CHEMBL1449583 1 6.46
CHEMBL608 PROBUCOL 4.0 1 6.37
CHEMBL3963713 1 6.24
CHEMBL3983642 1 6.14
CHEMBL3937216 1 6.12
CHEMBL291278 N-METHYL-D-ASPARTIC ACID (NMDA) 2.0 1 6.12
CHEMBL3891244 1 6.03
CHEMBL3912774 1 6.01
CHEMBL3922811 1 6.01
CHEMBL3933172 1 5.88
CHEMBL3928230 1 5.71
CHEMBL1623 MECLIZINE 4.0 1 5.70
CHEMBL3913828 1 5.64

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL46469 ANTHRALIN IC50 = 230.0 nM 6.64
CHEMBL3188992 IC50 = 280.0 nM 6.55
CHEMBL3933764 IC50 = 330.0 nM 6.48
CHEMBL1449583 IC50 = 350.0 nM 6.46
CHEMBL608 PROBUCOL IC50 = 430.0 nM 6.37
CHEMBL3963713 IC50 = 570.0 nM 6.24
CHEMBL3983642 IC50 = 720.0 nM 6.14
CHEMBL3937216 IC50 = 760.0 nM 6.12
CHEMBL291278 N-METHYL-D-ASPARTIC ACID (NMDA) IC50 = 750.0 nM 6.12
CHEMBL3891244 IC50 = 930.0 nM 6.03
CHEMBL3912774 IC50 = 980.0 nM 6.01
CHEMBL3922811 IC50 = 980.0 nM 6.01
CHEMBL3933172 IC50 = 1310.0 nM 5.88
CHEMBL3928230 IC50 = 1930.0 nM 5.71
CHEMBL1623 MECLIZINE IC50 = 2020.0 nM 5.70
CHEMBL3913828 IC50 = 2310.0 nM 5.64