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Assay Detail

CHEMBL3887675

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Kinase Assay: For the assay, 50 nl of each stock solution of the test compound in DMSO was pipetted into a black, low-volume 384-well microtiter plate (Greiner Bio-One, Frickenhausen, Germany) 2 ul of a solution of the above FGFR-3 fusion protein in aqueous assay buffer [8 mM MOPS pH 7.0, 10 mM magnesium acetate, 1.0 mM dithiothreitol, 0.05% (w/v) bovine serum albumin (BSA), 0.07% (v/v) Tween-20, 0.2 mM EDTA] was added, and the mixture was incubated for 15 min at 22° C. to allow pre-binding of the test compound to the enzyme. Then, the kinase reaction was started by the addition of 3 ul of a solution of adenosine triphosphate (ATP, 16.7 uM; final concentration in the 5 ul assay volume=10 uM) and substrate (0.8 uM; final concentration in the 5 ul assay volume=0.5 uM) in assay buffer, and the resulting mixture was incubated for a reaction time of 60 min at 22° C. The concentration of FGFR-3 fusion protein was adjusted depending on the activity of the enzyme lot.
96
Total Activities
88
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

Fibroblast growth factor receptor 3 (CHEMBL2742)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Disubstituted benzothienyl-pyrrolotriazines and uses thereof
(2015)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 96 8.05 9.70

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3937124 1 9.70
CHEMBL3911335 2 9.30
CHEMBL3929322 1 9.15
CHEMBL3951786 1 9.05
CHEMBL3985178 1 9.00
CHEMBL3943773 1 8.85
CHEMBL3920417 1 8.85
CHEMBL3949626 1 8.74
CHEMBL3906839 2 8.70
CHEMBL4108692 1 8.70
CHEMBL3916756 1 8.68
CHEMBL3944881 1 8.60
CHEMBL3938823 1 8.60
CHEMBL3889953 1 8.60
CHEMBL3924399 2 8.57
CHEMBL3934668 1 8.54
CHEMBL3968059 1 8.51
CHEMBL3892887 1 8.48
CHEMBL3952635 1 8.47
CHEMBL3938513 1 8.43
CHEMBL3905636 1 8.41
CHEMBL3977038 1 8.35
CHEMBL3895503 1 8.33
CHEMBL3979384 1 8.31
CHEMBL3905236 1 8.31
CHEMBL3934358 1 8.28
CHEMBL3909132 1 8.28
CHEMBL3897839 1 8.27
CHEMBL3907995 1 8.24
CHEMBL3969060 1 8.21

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3937124 IC50 = 0.2 nM 9.70
CHEMBL3911335 IC50 = 0.5 nM 9.30
CHEMBL3929322 IC50 = 0.7 nM 9.15
CHEMBL3951786 IC50 = 0.9 nM 9.05
CHEMBL3985178 IC50 = 1.0 nM 9.00
CHEMBL3943773 IC50 = 1.4 nM 8.85
CHEMBL3920417 IC50 = 1.4 nM 8.85
CHEMBL3949626 IC50 = 1.8 nM 8.74
CHEMBL3906839 IC50 = 2.0 nM 8.70
CHEMBL4108692 IC50 = 2.0 nM 8.70
CHEMBL3916756 IC50 = 2.1 nM 8.68
CHEMBL3938823 IC50 = 2.5 nM 8.60
CHEMBL3889953 IC50 = 2.5 nM 8.60
CHEMBL3944881 IC50 = 2.5 nM 8.60
CHEMBL3924399 IC50 = 2.7 nM 8.57
CHEMBL3924399 IC50 = 2.8 nM 8.55
CHEMBL3934668 IC50 = 2.9 nM 8.54
CHEMBL3968059 IC50 = 3.1 nM 8.51
CHEMBL3892887 IC50 = 3.3 nM 8.48
CHEMBL3952635 IC50 = 3.4 nM 8.47
CHEMBL3938513 IC50 = 3.7 nM 8.43
CHEMBL3906839 IC50 = 3.8 nM 8.42
CHEMBL3905636 IC50 = 3.9 nM 8.41
CHEMBL3977038 IC50 = 4.5 nM 8.35
CHEMBL3895503 IC50 = 4.7 nM 8.33
CHEMBL3979384 IC50 = 4.9 nM 8.31
CHEMBL3905236 IC50 = 4.9 nM 8.31
CHEMBL3909132 IC50 = 5.2 nM 8.28
CHEMBL3934358 IC50 = 5.3 nM 8.28
CHEMBL3897839 IC50 = 5.4 nM 8.27
CHEMBL3907995 IC50 = 5.7 nM 8.24
CHEMBL3969060 IC50 = 6.1 nM 8.21
CHEMBL3958993 IC50 = 6.4 nM 8.19
CHEMBL3954561 IC50 = 6.8 nM 8.17
CHEMBL3957859 IC50 = 6.8 nM 8.17
CHEMBL3953385 IC50 = 6.8 nM 8.17
CHEMBL3921263 IC50 = 7.0 nM 8.15
CHEMBL4112606 IC50 = 7.1 nM 8.15
CHEMBL3906882 IC50 = 7.2 nM 8.14
CHEMBL3926373 IC50 = 7.2 nM 8.14
CHEMBL3949665 IC50 = 7.7 nM 8.11
CHEMBL3929725 IC50 = 7.9 nM 8.10
CHEMBL3930377 IC50 = 8.1 nM 8.09
CHEMBL3969781 IC50 = 8.3 nM 8.08
CHEMBL3938754 IC50 = 8.7 nM 8.06
CHEMBL3976573 IC50 = 9.4 nM 8.03
CHEMBL3915403 IC50 = 9.4 nM 8.03
CHEMBL3969794 IC50 = 9.6 nM 8.02
CHEMBL3974164 IC50 = 9.8 nM 8.01
CHEMBL3948716 IC50 = 9.8 nM 8.01