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Assay Detail

CHEMBL3887883

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
In Vitro Enzyme Assay: Final assay conditions were 4 pM cRaf, 3 uM ATP, 10 nM biotin tagged MEK1 kinase dead protein substrate. Reactions were performed in Greiner384 well plates, catalog #784075. Reaction buffer was 50 mM Tris, pH 7.5, 50 mM NaCl, 10 mM MgCl2, 0.01% Tween-20, 0.05% BSA and 1 mM DTT. 5 ul of 2×cRaf plus MEK1 were dispensed into plates containing 0.25 ul of compound in 100% DMSO and incubated at room temperature for 30 minutes. Reactions were started by addition of 5 ul of 2×ATP. Reactions were run for two hours and terminated by addition of 10 ul of 2× antibody and Alphascreen bead mixture in Stop Buffer. Stop Buffer was 50 mM Tris, pH 7.5, 0.005% Tween-20, 25 mM EDTA.
197
Total Activities
196
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

Serine/threonine-protein kinase B-raf (CHEMBL5145)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Biaryl amide compounds as kinase inhibitors
(2016)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 197 8.46 9.82

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3933272 1 9.82
CHEMBL3967893 1 9.48
CHEMBL3951474 1 9.41
CHEMBL3905257 1 9.41
CHEMBL3956654 1 9.39
CHEMBL3959581 1 9.38
CHEMBL3976881 1 9.34
CHEMBL3928030 1 9.34
CHEMBL3962812 1 9.32
CHEMBL3984282 1 9.29
CHEMBL3946003 1 9.23
CHEMBL3987177 1 9.22
CHEMBL3942721 1 9.20
CHEMBL3960775 1 9.19
CHEMBL3907015 1 9.19
CHEMBL3914464 1 9.15
CHEMBL3955743 1 9.13
CHEMBL3966766 1 9.12
CHEMBL3966243 1 9.11
CHEMBL3930929 1 9.11
CHEMBL3919205 1 9.10
CHEMBL3963090 1 9.09
CHEMBL3969121 2 9.08
CHEMBL3969555 1 9.08
CHEMBL3972141 1 9.07
CHEMBL3945935 1 9.06
CHEMBL3955103 1 9.05
CHEMBL3909119 1 9.04
CHEMBL3927963 1 9.03
CHEMBL3906652 1 9.00

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3933272 IC50 = 0.152 nM 9.82
CHEMBL3967893 IC50 = 0.33 nM 9.48
CHEMBL3905257 IC50 = 0.389 nM 9.41
CHEMBL3951474 IC50 = 0.385 nM 9.41
CHEMBL3956654 IC50 = 0.408 nM 9.39
CHEMBL3959581 IC50 = 0.422 nM 9.38
CHEMBL3976881 IC50 = 0.456 nM 9.34
CHEMBL3928030 IC50 = 0.455 nM 9.34
CHEMBL3962812 IC50 = 0.483 nM 9.32
CHEMBL3984282 IC50 = 0.51 nM 9.29
CHEMBL3946003 IC50 = 0.585 nM 9.23
CHEMBL3987177 IC50 = 0.601 nM 9.22
CHEMBL3942721 IC50 = 0.632 nM 9.20
CHEMBL3960775 IC50 = 0.652 nM 9.19
CHEMBL3907015 IC50 = 0.64 nM 9.19
CHEMBL3914464 IC50 = 0.706 nM 9.15
CHEMBL3955743 IC50 = 0.737 nM 9.13
CHEMBL3966766 IC50 = 0.756 nM 9.12
CHEMBL3930929 IC50 = 0.775 nM 9.11
CHEMBL3966243 IC50 = 0.773 nM 9.11
CHEMBL3919205 IC50 = 0.802 nM 9.10
CHEMBL3963090 IC50 = 0.816 nM 9.09
CHEMBL3969121 IC50 = 0.837 nM 9.08
CHEMBL3969555 IC50 = 0.83 nM 9.08
CHEMBL3972141 IC50 = 0.86 nM 9.07
CHEMBL3945935 IC50 = 0.862 nM 9.06
CHEMBL3955103 IC50 = 0.884 nM 9.05
CHEMBL3909119 IC50 = 0.905 nM 9.04
CHEMBL3927963 IC50 = 0.941 nM 9.03
CHEMBL3903274 IC50 = 0.994 nM 9.00
CHEMBL3889721 IC50 = 1.003 nM 9.00
CHEMBL3906652 IC50 = 1.001 nM 9.00
CHEMBL4111816 IC50 = 1.023 nM 8.99
CHEMBL3912148 IC50 = 1.08 nM 8.97
CHEMBL3956383 IC50 = 1.07 nM 8.97
CHEMBL3924576 IC50 = 1.067 nM 8.97
CHEMBL3959652 IC50 = 1.131 nM 8.95
CHEMBL3905047 IC50 = 1.137 nM 8.94
CHEMBL3960436 IC50 = 1.142 nM 8.94
CHEMBL3960515 IC50 = 1.17 nM 8.93
CHEMBL3971301 IC50 = 1.214 nM 8.92
CHEMBL3932011 IC50 = 1.197 nM 8.92
CHEMBL3928581 IC50 = 1.241 nM 8.91
CHEMBL3894542 IC50 = 1.254 nM 8.90
CHEMBL4108504 IC50 = 1.286 nM 8.89
CHEMBL3946071 IC50 = 1.278 nM 8.89
CHEMBL3903846 IC50 = 1.277 nM 8.89
CHEMBL3947016 IC50 = 1.306 nM 8.88
CHEMBL3889893 IC50 = 1.332 nM 8.88
CHEMBL3975759 IC50 = 1.356 nM 8.87