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Assay Detail

CHEMBL3888022

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Binding
ELISA-Based Assay: Measurement of inhibition by compounds was performed using the HCV replicon system. Several different replicons encoding different HCV genotypes or mutations were used. In addition, potency measurements were made using different formats of the replicon assay, including different ways of measurements and different plating formats. See Jan M. Vrolijk et al., A replicons-based bioassay for the measurement of interferons in patients with chronic hepatitis C, 110 J. VIROLOGICAL METHODS 201 (2003); Steven S. Carroll et al., Inhibition of Hepatitis C Virus RNA Replication by 2'-Modified Nucleoside Analogs, 278(14) J. BIOLOGICAL CHEMISTRY 11979 (2003). However, the underlying principles are common to all of these determinations, and are outlined below.Stable neomycin phosphotransferase encoding replicons-harboring cell lines were used, so all cell lines were maintained under G418 selection prior to the assay. Potency was determined using a cell ELISA assay with an antibody to the replicons encoded NS3/4a protease. See Caterina Trozzi et al., In Vitro Selection and Characterization of Hepatitis C Virus Serine Protease Variants Resistant to an Active-Site Peptide Inhibitor, 77(6) J. Virol. 3669 (2003).
211
Total Activities
195
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

Genome polyprotein (CHEMBL3988603)
Type SINGLE PROTEIN
Organism Hepatitis C virus genotype 1b (isolate Japanese) (HCV)

Publication

Tetracyclic heterocycle compounds and methods of use thereof for the treatment of viral diseases
(2016)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 211 8.23 9.15

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3947223 2 9.15
CHEMBL3905713 2 9.05
CHEMBL3892379 2 9.05
CHEMBL3935713 1 9.05
CHEMBL3933586 1 9.00
CHEMBL3915462 1 8.92
CHEMBL3940812 1 8.92
CHEMBL3909191 1 8.92
CHEMBL3939023 1 8.89
CHEMBL3921348 2 8.85
CHEMBL3891479 1 8.80
CHEMBL3949178 2 8.80
CHEMBL3943078 1 8.77
CHEMBL3971537 1 8.77
CHEMBL3906025 1 8.77
CHEMBL3899309 1 8.74
CHEMBL3956983 1 8.74
CHEMBL3918127 1 8.74
CHEMBL3898617 1 8.74
CHEMBL3980692 1 8.72
CHEMBL3928375 1 8.72
CHEMBL3943320 1 8.72
CHEMBL3897404 2 8.72
CHEMBL3896939 1 8.70
CHEMBL3957086 1 8.68
CHEMBL3892828 1 8.68
CHEMBL3980606 1 8.68
CHEMBL3906781 2 8.68
CHEMBL3899764 1 8.68
CHEMBL3944919 2 8.68

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3947223 IC50 = 0.7 nM 9.15
CHEMBL3892379 IC50 = 0.9 nM 9.05
CHEMBL3905713 IC50 = 0.9 nM 9.05
CHEMBL3935713 IC50 = 0.9 nM 9.05
CHEMBL3933586 IC50 = 1.0 nM 9.00
CHEMBL3915462 IC50 = 1.2 nM 8.92
CHEMBL3940812 IC50 = 1.2 nM 8.92
CHEMBL3909191 IC50 = 1.2 nM 8.92
CHEMBL3939023 IC50 = 1.3 nM 8.89
CHEMBL3921348 IC50 = 1.4 nM 8.85
CHEMBL3891479 IC50 = 1.6 nM 8.80
CHEMBL3949178 IC50 = 1.6 nM 8.80
CHEMBL3971537 IC50 = 1.7 nM 8.77
CHEMBL3906025 IC50 = 1.7 nM 8.77
CHEMBL3943078 IC50 = 1.7 nM 8.77
CHEMBL3899309 IC50 = 1.8 nM 8.74
CHEMBL3898617 IC50 = 1.8 nM 8.74
CHEMBL3956983 IC50 = 1.8 nM 8.74
CHEMBL3918127 IC50 = 1.8 nM 8.74
CHEMBL3980692 IC50 = 1.9 nM 8.72
CHEMBL3928375 IC50 = 1.9 nM 8.72
CHEMBL3897404 IC50 = 1.9 nM 8.72
CHEMBL3943320 IC50 = 1.9 nM 8.72
CHEMBL3896939 IC50 = 2.0 nM 8.70
CHEMBL3957086 IC50 = 2.1 nM 8.68
CHEMBL3980606 IC50 = 2.1 nM 8.68
CHEMBL3906781 IC50 = 2.1 nM 8.68
CHEMBL3899764 IC50 = 2.1 nM 8.68
CHEMBL3944919 IC50 = 2.1 nM 8.68
CHEMBL3971894 IC50 = 2.1 nM 8.68
CHEMBL3909804 IC50 = 2.1 nM 8.68
CHEMBL3978542 IC50 = 2.1 nM 8.68
CHEMBL3892828 IC50 = 2.1 nM 8.68
CHEMBL3944776 IC50 = 2.2 nM 8.66
CHEMBL3916219 IC50 = 2.2 nM 8.66
CHEMBL3905576 IC50 = 2.2 nM 8.66
CHEMBL3956781 IC50 = 2.2 nM 8.66
CHEMBL3971242 IC50 = 2.2 nM 8.66
CHEMBL3946017 IC50 = 2.2 nM 8.66
CHEMBL3968106 IC50 = 2.3 nM 8.64
CHEMBL3982221 IC50 = 2.3 nM 8.64
CHEMBL3979841 IC50 = 2.3 nM 8.64
CHEMBL3905713 IC50 = 2.4 nM 8.62
CHEMBL3892379 IC50 = 2.4 nM 8.62
CHEMBL3934354 IC50 = 2.4 nM 8.62
CHEMBL3951818 IC50 = 2.4 nM 8.62
CHEMBL3972569 IC50 = 2.4 nM 8.62
CHEMBL3957324 IC50 = 2.4 nM 8.62
CHEMBL3947223 IC50 = 2.4 nM 8.62
CHEMBL3953901 IC50 = 2.6 nM 8.59