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Assay Detail

CHEMBL3889232

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Time Resolved-Fluorescence Resonance Energy Transfer (TR-FRET) Assay: Representative compounds were serially diluted in dimethyl sulfoxide (DMSO) starting at 50 uM (2x starting concentration; 10% DMSO) and 10 uL were transferred into a 384-well plate. Then 10 uL of a protein/probe/antibody mix was added to each well at final concentrations listed in TABLE 1. The samples are then mixed on a shaker for 1 minute and incubated for an additional 3 hours at room temperature. For each assay, the probe/antibody and protein/probe/antibody were included on each assay plate as negative and positive controls, respectively. Fluorescence was measured on the ENVISION plate reader (Perkin Elmer) using a 340/35 nm excitation filter and 520/525 (F-Bak peptide) and 495/510 nm (Tb-labeled anti-Histidine antibody) emission filters Inhibition constants (Ki) are shown in TABLE 2 below and were determined using Wang's equation (Wang Z.-X. An Exact Mathematical Expression For Describing Competitive Binding Of Two Different Ligands To A Protein Molecule. FEBS Lett. 1995, 360:111-4).
44
Total Activities
44
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

Apoptosis regulator Bcl-2 (CHEMBL4860)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Apoptosis-inducing agent for the treatment of cancer and immune and autoimmune diseases
(2016)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
Ki 44 7.46 10.41

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3926447 1 10.41
CHEMBL3950005 1 10.28
CHEMBL3964082 1 10.19
CHEMBL3914582 1 10.08
CHEMBL3923607 1 9.51
CHEMBL3935424 1 9.39
CHEMBL3948854 1 9.19
CHEMBL3903384 1 8.79
CHEMBL3935806 1 8.76
CHEMBL3921048 1 8.75
CHEMBL3973825 1 8.69
CHEMBL3911407 1 8.17
CHEMBL3912602 1 7.69
CHEMBL3962876 1 7.69
CHEMBL3954629 1 7.61
CHEMBL3978310 1 7.42
CHEMBL3926997 1 7.33
CHEMBL3965688 1 7.32
CHEMBL3930124 1 7.29
CHEMBL3905577 1 7.29
CHEMBL3893173 1 7.08
CHEMBL3941074 1 6.89
CHEMBL3910451 1 6.86
CHEMBL3902143 1 6.75
CHEMBL3905254 1 6.75
CHEMBL3897719 1 6.72
CHEMBL3913077 1 6.63
CHEMBL3905470 1 6.57
CHEMBL3919771 1 6.55
CHEMBL3947773 1 6.53

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3926447 Ki = 0.039 nM 10.41
CHEMBL3950005 Ki = 0.053 nM 10.28
CHEMBL3964082 Ki = 0.064 nM 10.19
CHEMBL3914582 Ki = 0.084 nM 10.08
CHEMBL3923607 Ki = 0.307 nM 9.51
CHEMBL3935424 Ki = 0.407 nM 9.39
CHEMBL3948854 Ki = 0.649 nM 9.19
CHEMBL3903384 Ki = 1.637 nM 8.79
CHEMBL3935806 Ki = 1.75 nM 8.76
CHEMBL3921048 Ki = 1.791 nM 8.75
CHEMBL3973825 Ki = 2.067 nM 8.69
CHEMBL3911407 Ki = 6.735 nM 8.17
CHEMBL3912602 Ki = 20.42 nM 7.69
CHEMBL3962876 Ki = 20.24 nM 7.69
CHEMBL3954629 Ki = 24.78 nM 7.61
CHEMBL3978310 Ki = 37.86 nM 7.42
CHEMBL3926997 Ki = 46.5 nM 7.33
CHEMBL3965688 Ki = 48.08 nM 7.32
CHEMBL3930124 Ki = 51.7 nM 7.29
CHEMBL3905577 Ki = 51.45 nM 7.29
CHEMBL3893173 Ki = 82.92 nM 7.08
CHEMBL3941074 Ki = 128.53 nM 6.89
CHEMBL3910451 Ki = 138.75 nM 6.86
CHEMBL3905254 Ki = 177.06 nM 6.75
CHEMBL3902143 Ki = 176.18 nM 6.75
CHEMBL3897719 Ki = 188.23 nM 6.72
CHEMBL3913077 Ki = 234.12 nM 6.63
CHEMBL3905470 Ki = 269.18 nM 6.57
CHEMBL3919771 Ki = 282.11 nM 6.55
CHEMBL3947773 Ki = 293.81 nM 6.53
CHEMBL3973043 Ki = 339.99 nM 6.47
CHEMBL3936044 Ki = 342.1 nM 6.47
CHEMBL3904077 Ki = 356.26 nM 6.45
CHEMBL3956645 Ki = 372.11 nM 6.43
CHEMBL3910827 Ki = 387.69 nM 6.41
CHEMBL3942247 Ki = 392.53 nM 6.41
CHEMBL3982046 Ki = 393.36 nM 6.41
CHEMBL3947557 Ki = 408.57 nM 6.39
CHEMBL3903210 Ki = 417.29 nM 6.38
CHEMBL3974157 Ki = 434.0 nM 6.36
CHEMBL3926506 Ki = 437.92 nM 6.36
CHEMBL3957851 Ki = 447.13 nM 6.35
CHEMBL3939121 Ki = 703.74 nM 6.15
CHEMBL3933269 Ki = 743.18 nM 6.13