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Assay Detail

CHEMBL4013171

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Inhibition of recombinant human His-tagged KGA (L123 to L669 residues) expressed in Escherichia coli BL21(DE3)pLysS using glutamine substrate preincubated for 10 mins followed by substrate addition measured after 60 mins by glutamate dehydrogenase coupled enzyme assay
17
Total Activities
17
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Glutaminase kidney isoform, mitochondrial (CHEMBL2146302)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Design, Synthesis, and Evaluation of Thiazolidine-2,4-dione Derivatives as a Novel Class of Glutaminase Inhibitors.
Yeh TK, Kuo CC, Lee YZ, Ke YY, Chu KF, Hsu HY, Chang HY, Liu YW, Song JS, Yang CW, Lin LM, Sun M, Wu SH, Kuo PC, Shih C, Chen CT, Tsou LK, Lee SJ.
J Med Chem (2017) 60 : 5599 -5612
PubMed 28609101 · DOI

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 17 6.90 7.46

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL4082885 1 7.46
CHEMBL4072390 1 7.41
CHEMBL4090687 1 7.35
CHEMBL4061000 1 7.32
CHEMBL4080388 1 7.30
CHEMBL4099331 1 7.27
CHEMBL4087349 1 7.25
CHEMBL4074218 1 7.24
CHEMBL4065595 1 7.23
CHEMBL4065936 1 7.18
CHEMBL2177757 1 7.09
CHEMBL4098413 1 6.99
CHEMBL4069677 1 6.61
CHEMBL4087025 1 6.61
CHEMBL4100814 1 6.12
CHEMBL4070276 1 5.51
CHEMBL4074051 1 5.31

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL4082885 IC50 = 35.0 nM 7.46
CHEMBL4072390 IC50 = 39.0 nM 7.41
CHEMBL4090687 IC50 = 45.0 nM 7.35
CHEMBL4061000 IC50 = 48.0 nM 7.32
CHEMBL4080388 IC50 = 50.0 nM 7.30
CHEMBL4099331 IC50 = 54.0 nM 7.27
CHEMBL4087349 IC50 = 56.0 nM 7.25
CHEMBL4074218 IC50 = 57.0 nM 7.24
CHEMBL4065595 IC50 = 59.0 nM 7.23
CHEMBL4065936 IC50 = 66.0 nM 7.18
CHEMBL2177757 IC50 = 81.0 nM 7.09
CHEMBL4098413 IC50 = 102.0 nM 6.99
CHEMBL4069677 IC50 = 243.0 nM 6.61
CHEMBL4087025 IC50 = 247.0 nM 6.61
CHEMBL4100814 IC50 = 754.0 nM 6.12
CHEMBL4070276 IC50 = 3097.0 nM 5.51
CHEMBL4074051 IC50 = 4896.0 nM 5.31