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Assay Detail

CHEMBL4050074

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Inhibition of wild-type BRAF (unknown origin) using human His6-tagged MEK1 K97R mutant as substrate pretreated for 20 mins followed by [33P]-ATP addition measured after 2 hrs by filter binding method
12
Total Activities
12
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Serine/threonine-protein kinase B-raf (CHEMBL5145)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Design, synthesis and evaluation of derivatives based on pyrimidine scaffold as potent Pan-Raf inhibitors to overcome resistance.
Wang L, Zhang Q, Zhu G, Zhang Z, Zhi Y, Zhang L, Mao T, Zhou X, Chen Y, Lu T, Tang W.
Eur J Med Chem (2017) 130 : 86 -106
PubMed 28242553 · DOI

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 12 7.54 8.16

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL1229517 VEMURAFENIB 4.0 1 8.16
CHEMBL4080362 1 7.98
CHEMBL4066939 1 7.85
CHEMBL4060057 1 7.76
CHEMBL4104590 1 7.67
CHEMBL1336 SORAFENIB 4.0 1 7.65
CHEMBL4075036 1 7.53
CHEMBL4087837 1 7.47
CHEMBL4085294 1 7.40
CHEMBL4082425 1 7.28
CHEMBL4060531 1 7.22
CHEMBL4101882 1 6.54

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL1229517 VEMURAFENIB IC50 = 6.9 nM 8.16
CHEMBL4080362 IC50 = 10.5 nM 7.98
CHEMBL4066939 IC50 = 14.2 nM 7.85
CHEMBL4060057 IC50 = 17.2 nM 7.76
CHEMBL4104590 IC50 = 21.2 nM 7.67
CHEMBL1336 SORAFENIB IC50 = 22.6 nM 7.65
CHEMBL4075036 IC50 = 29.7 nM 7.53
CHEMBL4087837 IC50 = 33.8 nM 7.47
CHEMBL4085294 IC50 = 39.8 nM 7.40
CHEMBL4082425 IC50 = 52.1 nM 7.28
CHEMBL4060531 IC50 = 60.0 nM 7.22
CHEMBL4101882 IC50 = 287.0 nM 6.54