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Assay Detail

CHEMBL4158661

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Binding
Binding affinity to human His-thioredoxin-tagged HDAC8 expressed in Escherichia coli BL21 (DE3) cells by ITC method
12
Total Activities
3
Compounds Tested
4
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Histone deacetylase 8 (CHEMBL3192)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Characterization of Histone Deacetylase 8 (HDAC8) Selective Inhibition Reveals Specific Active Site Structural and Functional Determinants.
Marek M, Shaik TB, Heimburg T, Chakrabarti A, Lancelot J, Ramos-Morales E, Da Veiga C, Kalinin D, Melesina J, Robaa D, Schmidtkunz K, Suzuki T, Holl R, Ennifar E, Pierce RJ, Jung M, Sippl W, Romier C.
J Med Chem (2018) 61 : 10000 -10016
PubMed 30347148 · DOI

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
Kd 3 7.27 7.64
deltaG 3 - -
deltaH 3 - -
-TdeltaS 3 - -

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL2105763 QUISINOSTAT 2.0 4 7.64
CHEMBL2170177 4 7.12
CHEMBL2178342 4 7.05

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL2105763 QUISINOSTAT Kd = 22.7 nM 7.64
CHEMBL2170177 Kd = 75.1 nM 7.12
CHEMBL2178342 Kd = 89.6 nM 7.05
CHEMBL2170177 deltaG = -9.7 kcal/mol -
CHEMBL2170177 deltaH = -11.0 kcal/mol -
CHEMBL2170177 -TdeltaS = 1.3 kcal/mol -
CHEMBL2178342 deltaG = -9.6 kcal/mol -
CHEMBL2178342 deltaH = -10.3 kcal/mol -
CHEMBL2178342 -TdeltaS = 0.7 kcal/mol -
CHEMBL2105763 QUISINOSTAT deltaG = -10.4 kcal/mol -
CHEMBL2105763 QUISINOSTAT deltaH = -12.7 kcal/mol -
CHEMBL2105763 QUISINOSTAT -TdeltaS = 2.3 kcal/mol -