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Assay Detail

CHEMBL4234643

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Activation of full-length recombinant N-terminal His-tagged human AMPKalpha2beta1gamma1 expressed in Escherichia coli BL21 cells using Cy-5 SAMS peptide as substrate preincubated for 60 mins followed by substrate addition and measured after 60 mins in presence of PP2a by TR-FRET assay
6
Total Activities
6
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 7 — Homologous single protein target
Curated By Intermediate

Target

AMPK alpha2/beta1/gamma1 (CHEMBL3038455)
Type PROTEIN COMPLEX
Organism Homo sapiens

Publication

Acyl Glucuronide Metabolites of 6-Chloro-5-[4-(1-hydroxycyclobutyl)phenyl]-1 H-indole-3-carboxylic Acid (PF-06409577) and Related Indole-3-carboxylic Acid Derivatives are Direct Activators of Adenosine Monophosphate-Activated Protein Kinase (AMPK).
Ryder TF, Calabrese MF, Walker GS, Cameron KO, Reyes AR, Borzilleri KA, Delmore J, Miller R, Kurumbail RG, Ward J, Kung DW, Brown JA, Edmonds DJ, Eng H, Wolford AC, Kalgutkar AS.
J Med Chem (2018) 61 : 7273 -7288
PubMed 30036059 · DOI

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
EC50 6 7.21 8.22

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL4105032 1 8.22
CHEMBL3891221 1 7.95
CHEMBL3986871 1 7.57
CHEMBL4249790 1 6.56
CHEMBL4246000 1 6.48
CHEMBL4250253 1 6.45

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL4105032 EC50 = 6.0 nM 8.22
CHEMBL3891221 EC50 = 11.3 nM 7.95
CHEMBL3986871 EC50 = 27.0 nM 7.57
CHEMBL4249790 EC50 = 275.0 nM 6.56
CHEMBL4246000 EC50 = 332.0 nM 6.48
CHEMBL4250253 EC50 = 353.0 nM 6.45