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Assay Detail

CHEMBL4353689

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Inhibition of N-terminal GST-tagged recombinant human KDM4B (1 to 500 residues) expressed in baculovirus infected Sf9 insect cells assessed as decrease in demethylation of substrate using peptide (ARTKQTARK(Me3)STGGKAPRKQLA-GGKbiotin) as substrate and 2OG as cosubstrate pre-incubated for 10 mins before substrate addition followed by centrifugation for 1 min and measured after 20 mins by AlphaScreen assay
33
Total Activities
33
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Cell Type Sf9
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Lysine-specific demethylase 4B (CHEMBL3313832)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

C8-substituted pyrido[3,4-d]pyrimidin-4(3H)-ones: Studies towards the identification of potent, cell penetrant Jumonji C domain containing histone lysine demethylase 4 subfamily (KDM4) inhibitors, compound profiling in cell-based target engagement assays.
Le Bihan YV, Lanigan RM, Atrash B, McLaughlin MG, Velupillai S, Malcolm AG, England KS, Ruda GF, Mok NY, Tumber A, Tomlin K, Saville H, Shehu E, McAndrew C, Carmichael L, Bennett JM, Jeganathan F, Eve P, Donovan A, Hayes A, Wood F, Raynaud FI, Fedorov O, Brennan PE, Burke R, van Montfort RLM, Rossanese OW, Blagg J, Bavetsias V.
Eur J Med Chem (2019) 177 : 316 -337
PubMed 31158747 · DOI

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 33 7.15 8.10

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL4438830 1 8.10
CHEMBL4440395 1 7.82
CHEMBL4466130 1 7.75
CHEMBL4592908 1 7.72
CHEMBL4585876 1 7.70
CHEMBL4590283 1 7.70
CHEMBL4559561 1 7.62
CHEMBL4567766 1 7.57
CHEMBL4573390 1 7.54
CHEMBL4447515 1 7.50
CHEMBL4438034 1 7.50
CHEMBL4561958 1 7.48
CHEMBL4516101 1 7.48
CHEMBL4449500 1 7.37
CHEMBL4435185 1 7.35
CHEMBL4558689 1 7.33
CHEMBL4520178 1 7.31
CHEMBL4464471 1 7.24
CHEMBL4549505 1 7.20
CHEMBL4538741 1 7.17
CHEMBL4522584 1 7.10
CHEMBL4476629 1 7.00
CHEMBL4553540 1 6.99
CHEMBL4473678 1 6.84
CHEMBL4572027 1 6.82
CHEMBL4525269 1 6.61
CHEMBL4529932 1 6.52
CHEMBL4532069 1 6.43
CHEMBL4560811 1 6.34
CHEMBL4445652 1 6.30

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL4438830 IC50 = 8.0 nM 8.10
CHEMBL4440395 IC50 = 15.0 nM 7.82
CHEMBL4466130 IC50 = 18.0 nM 7.75
CHEMBL4592908 IC50 = 19.0 nM 7.72
CHEMBL4585876 IC50 = 20.0 nM 7.70
CHEMBL4590283 IC50 = 20.0 nM 7.70
CHEMBL4559561 IC50 = 24.0 nM 7.62
CHEMBL4567766 IC50 = 27.0 nM 7.57
CHEMBL4573390 IC50 = 29.0 nM 7.54
CHEMBL4447515 IC50 = 32.0 nM 7.50
CHEMBL4438034 IC50 = 32.0 nM 7.50
CHEMBL4561958 IC50 = 33.0 nM 7.48
CHEMBL4516101 IC50 = 33.0 nM 7.48
CHEMBL4449500 IC50 = 43.0 nM 7.37
CHEMBL4435185 IC50 = 45.0 nM 7.35
CHEMBL4558689 IC50 = 47.0 nM 7.33
CHEMBL4520178 IC50 = 49.0 nM 7.31
CHEMBL4464471 IC50 = 57.0 nM 7.24
CHEMBL4549505 IC50 = 63.0 nM 7.20
CHEMBL4538741 IC50 = 67.0 nM 7.17
CHEMBL4522584 IC50 = 79.0 nM 7.10
CHEMBL4476629 IC50 = 101.0 nM 7.00
CHEMBL4553540 IC50 = 102.0 nM 6.99
CHEMBL4473678 IC50 = 145.0 nM 6.84
CHEMBL4572027 IC50 = 153.0 nM 6.82
CHEMBL4525269 IC50 = 248.0 nM 6.61
CHEMBL4529932 IC50 = 302.0 nM 6.52
CHEMBL4532069 IC50 = 372.0 nM 6.43
CHEMBL4560811 IC50 = 455.0 nM 6.34
CHEMBL4445652 IC50 = 497.0 nM 6.30
CHEMBL4455283 IC50 = 504.0 nM 6.30
CHEMBL4483792 IC50 = 573.0 nM 6.24
CHEMBL4483780 IC50 = 820.0 nM 6.09