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Assay Detail

CHEMBL4425320

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Inhibition of human His-tagged PDE4D catalytic domain expressed in Escherichia coli BL21-CodonPlus(DE3) cells using [3H]cAMP or [3H]cGMP as substrate incubated for 30 mins by scintillation counting method
10
Total Activities
10
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

3',5'-cyclic-AMP phosphodiesterase 4D (CHEMBL288)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

PDEStrIAn: A Phosphodiesterase Structure and Ligand Interaction Annotated Database As a Tool for Structure-Based Drug Design.
Jansen C, Kooistra AJ, Kanev GK, Leurs R, de Esch IJ, de Graaf C.
J Med Chem (2016) 59 : 7029 -7065
PubMed 26908025 · DOI

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 10 7.13 10.68

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL42126 PICLAMILAST 2.0 1 10.68
CHEMBL193240 ROFLUMILAST 4.0 1 9.17
CHEMBL511115 CILOMILAST 3.0 1 7.96
CHEMBL1230564 1 7.68
CHEMBL1230397 1 6.80
CHEMBL1794670 1 6.57
CHEMBL313842 ZARDAVERINE 2.0 1 6.41
CHEMBL63 ROLIPRAM 2.0 1 6.26
CHEMBL1230268 1 5.70
CHEMBL506972 1 4.09

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL42126 PICLAMILAST IC50 = 0.021 nM 10.68
CHEMBL193240 ROFLUMILAST IC50 = 0.68 nM 9.17
CHEMBL511115 CILOMILAST IC50 = 11.0 nM 7.96
CHEMBL1230564 IC50 = 21.0 nM 7.68
CHEMBL1230397 IC50 = 160.0 nM 6.80
CHEMBL1794670 IC50 = 270.0 nM 6.57
CHEMBL313842 ZARDAVERINE IC50 = 390.0 nM 6.41
CHEMBL63 ROLIPRAM IC50 = 550.0 nM 6.26
CHEMBL1230268 IC50 = 2000.0 nM 5.70
CHEMBL506972 IC50 = 82000.0 nM 4.09