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Assay Detail

CHEMBL4729979

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Inhibition of CD73 in human NCI-H1568 cells assessed as reduction in AMP-induced ADO expression preincubated for 15 mins followed by AMP addition and measured after 1 hr by LC-MS/MS analysis
5
Total Activities
5
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Cell Type NCI-H1568
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

5'-nucleotidase (CHEMBL5957)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Orally Bioavailable Small-Molecule CD73 Inhibitor (OP-5244) Reverses Immunosuppression through Blockade of Adenosine Production.
Du X,Moore J,Blank BR,Eksterowicz J,Sutimantanapi D,Yuen N,Metzger T,Chan B,Huang T,Chen X,Chen Y,Duong F,Kong W,Chang JH,Sun J,Zavorotinskaya T,Ye Q,Junttila MR,Ndubaku C,Friedman LS,Fantin VR,Sun D
J Med Chem (2020) 63 : 10433 -10459
PubMed 32865411 · DOI

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
EC50 5 7.79 9.10

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL4764985 1 9.10
CHEMBL4471306 QUEMLICLUSTAT 2.0 1 8.48
CHEMBL4786598 1 8.43
CHEMBL4752114 1 8.16
CHEMBL583969 PHOSPHOMETHYLPHOSPHONIC ACID ADENOSYL ESTER 1 4.79

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL4764985 EC50 = 0.79 nM 9.10
CHEMBL4471306 QUEMLICLUSTAT EC50 = 3.3 nM 8.48
CHEMBL4786598 EC50 = 3.7 nM 8.43
CHEMBL4752114 EC50 = 6.9 nM 8.16
CHEMBL583969 PHOSPHOMETHYLPHOSPHONIC ACID ADENOSYL ESTER EC50 = 16268.0 nM 4.79