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Assay Detail

CHEMBL4843878

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Inhibition of N-terminal GST-tagged ITK (2 to 620 residues) (unknown origin) expressed in Sf21 insect cells using NH2-ETVYSEVRK-biotin as substrate preincubated for 1 hr followed by ATP addition and measured after 2 hrs by ELISA
13
Total Activities
13
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Cell Type Sf21
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Tyrosine-protein kinase ITK/TSK (CHEMBL2959)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Structure-activity relationship investigation for imidazopyrazole-3-carboxamide derivatives as novel selective inhibitors of Bruton's tyrosine kinase.
Zhang D, Xu G, Zhao J, Wang Y, Wu X, He X, Li W, Zhang S, Yang S, Ma C, Jiang Y, Ding Q.
Eur J Med Chem (2021) 225 : 113724 -113724
PubMed 34391034 · DOI

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 13 6.03 8.05

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3647964 1 8.05
CHEMBL3936761 ZANUBRUTINIB 4.0 1 6.69
CHEMBL4852264 1 6.42
CHEMBL4863088 1 6.33
CHEMBL4878090 1 6.26
CHEMBL4875332 1 6.13
CHEMBL4863078 1 5.96
CHEMBL4856592 1 5.85
CHEMBL4867893 1 5.79
CHEMBL4873984 1 5.72
CHEMBL4871192 1 5.69
CHEMBL4869409 1 5.05
CHEMBL4857353 1 4.43

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3647964 IC50 = 8.9 nM 8.05
CHEMBL3936761 ZANUBRUTINIB IC50 = 202.9 nM 6.69
CHEMBL4852264 IC50 = 385.0 nM 6.42
CHEMBL4863088 IC50 = 465.0 nM 6.33
CHEMBL4878090 IC50 = 549.0 nM 6.26
CHEMBL4875332 IC50 = 734.0 nM 6.13
CHEMBL4863078 IC50 = 1109.0 nM 5.96
CHEMBL4856592 IC50 = 1415.0 nM 5.85
CHEMBL4867893 IC50 = 1619.0 nM 5.79
CHEMBL4873984 IC50 = 1916.0 nM 5.72
CHEMBL4871192 IC50 = 2033.0 nM 5.69
CHEMBL4869409 IC50 = 8940.0 nM 5.05
CHEMBL4857353 IC50 = 37225.0 nM 4.43