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Assay Detail

CHEMBL5151697

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Inhibition of human 20S immunoproteasome beta-1i subunit using (Ac-PAL)2R110 as substrate preincubated for 2 hrs followed by substrate addition and measured after 1 hr by fluorescence intensity assay
5
Total Activities
5
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Proteasome subunit beta type-9 (CHEMBL1944495)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Structure-Based Optimization and Discovery of M3258, a Specific Inhibitor of the Immunoproteasome Subunit LMP7 (β5i).
Klein M, Busch M, Friese-Hamim M, Crosignani S, Fuchss T, Musil D, Rohdich F, Sanderson MP, Seenisamy J, Walter-Bausch G, Zanelli U, Hewitt P, Esdar C, Schadt O.
J Med Chem (2021) 64 : 10230 -10245
PubMed 34228444 · DOI

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 5 8.06 8.57

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL5171825 1 8.57
CHEMBL325041 BORTEZOMIB 3.0 1 8.54
CHEMBL5188533 1 7.96
CHEMBL451887 CARFILZOMIB 4.0 1 7.16
CHEMBL5184466 1 -

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL5171825 IC50 = 2.7 nM 8.57
CHEMBL325041 BORTEZOMIB IC50 = 2.9 nM 8.54
CHEMBL5188533 IC50 = 11.0 nM 7.96
CHEMBL451887 CARFILZOMIB IC50 = 69.0 nM 7.16
CHEMBL5184466 IC50 > 30000.0 nM -