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Assay Detail

CHEMBL5377217

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Inhibition of CaMKK2 (161 to 449 residues) (unknown origin) expressed in Escherichia coli BL21 (DE3) star cells incubated for 20 mins in presence of kinase tracer 236 by TR-FRET
9
Total Activities
9
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Calcium/calmodulin-dependent protein kinase kinase 2 (CHEMBL5284)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Identification of Small Molecule Inhibitors and Ligand Directed Degraders of Calcium/Calmodulin Dependent Protein Kinase Kinase 1 and 2 (CaMKK1/2).
Chen Y, Whitefield B, Nevius E, Hill M, DelRosario J, Sinitsyna N, Shanmugasundaram V, Mukherjee D, Shi L, Mayne CG, Rousseau AM, Bernard SM, Buenviaje J, Khambatta G, El Samin M, Wallace M, Nie Z, Sivakumar P, Hamann LG, McDonnell DP, D'Agostino LA.
J Med Chem (2023) 66 : 15750 -15760
PubMed 38009718 · DOI

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 9 8.12 8.85

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL5421767 1 8.85
CHEMBL558642 GSK-650394 1 8.64
CHEMBL5439578 1 8.60
CHEMBL5431962 1 8.40
CHEMBL5426746 1 8.15
CHEMBL5396413 1 8.15
CHEMBL5422255 1 8.05
CHEMBL5397685 1 7.30
CHEMBL1182777 1 6.92

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL5421767 IC50 = 1.4 nM 8.85
CHEMBL558642 GSK-650394 IC50 = 2.3 nM 8.64
CHEMBL5439578 IC50 = 2.5 nM 8.60
CHEMBL5431962 IC50 = 4.0 nM 8.40
CHEMBL5426746 IC50 = 7.0 nM 8.15
CHEMBL5396413 IC50 = 7.0 nM 8.15
CHEMBL5422255 IC50 = 9.0 nM 8.05
CHEMBL5397685 IC50 = 50.0 nM 7.30
CHEMBL1182777 IC50 = 120.0 nM 6.92