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Assay Detail

CHEMBL5509526

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Binding
Antagonist activity at N-terminal his6-tagged human recombinant NUDT5 (1 to 208 residues) expressed in Escherichia coli Rosetta (DE3) using ADP as substrate incubated for 1 hr by luminescence based microplate reader analysis
10
Total Activities
10
Compounds Tested
1
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

ADP-sugar pyrophosphatase (CHEMBL4105713)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Unexpected Noncovalent Off-Target Activity of Clinical BTK Inhibitors Leads to Discovery of a Dual NUDT5/14 Antagonist.
Balıkçı E, Marques AMC, Bauer LG, Seupel R, Bennett J, Raux B, Buchan K, Simelis K, Singh U, Rogers C, Ward J, Cheng C, Szommer T, Schützenhofer K, Elkins JM, Sloman DL, Ahel I, Fedorov O, Brennan PE, Huber KVM.
J Med Chem (2024) 67 : 7245 -7259
PubMed 38635563 · DOI

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 10 5.58 6.57

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL5527860 1 6.57
CHEMBL5549952 1 6.31
CHEMBL1873475 IBRUTINIB 4.0 1 6.08
CHEMBL1242204 1 5.69
CHEMBL4072833 EVOBRUTINIB 3.0 1 4.86
CHEMBL5549782 1 4.86
CHEMBL4449342 1 4.67
CHEMBL5560485 1 -
CHEMBL5561533 1 -
CHEMBL5565823 1 -

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL5527860 IC50 = 270.0 nM 6.57
CHEMBL5549952 IC50 = 487.0 nM 6.31
CHEMBL1873475 IBRUTINIB IC50 = 837.0 nM 6.08
CHEMBL1242204 IC50 = 2040.0 nM 5.69
CHEMBL4072833 EVOBRUTINIB IC50 = 13900.0 nM 4.86
CHEMBL5549782 IC50 = 13800.0 nM 4.86
CHEMBL4449342 IC50 = 21200.0 nM 4.67
CHEMBL5560485 IC50 > 50000.0 nM -
CHEMBL5561533 IC50 - -
CHEMBL5565823 IC50 - -