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Assay Detail

CHEMBL5730474

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Binding
Caliper Assay: Selected compounds disclosed herein were tested in CDK4/cyclinD1, CDK2/CycA and CDK2/cyclinE kinase assays by Nanosyn (Santa Clara, Calif.) to determine their inhibitory effect on these CDKs. The assays were performed using microfluidic kinase detection technology (Caliper Assay Platform). The compounds were tested in 12-point dose-response format in singlicate at Km for ATP. Phosphoacceptor substrate peptide concentration used was 1 μM for all assays and Staurosporine was used as the reference compound for all assays. Specifics of each assay are as described below:CDK2/CyclinA: Enzyme concentration: 0.2 nM; ATP concentration: 50 μM; Incubation time: 3 hr.CDK2/CyclinE: Enzyme concentration: 0.28 nM; ATP concentration: 100 μM; Incubation time: 1 hr.CDK4/CyclinD1: Enzyme concentration: 1 nM; ATP concentration: 200 μM; Incubation time: 10 hr.
177
Total Activities
58
Compounds Tested
3
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 0 — Uncurated / Unknown
Curated By Autocuration

Target

Unchecked (CHEMBL612545)
Type UNCHECKED

Publication

HSPC-sparing treatments for RB-positive abnormal cellular proliferation
(2016)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 59 6.02 7.21
kon 59 - -
k_off 59 - -

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3967592 3 7.21
CHEMBL3972676 3 7.07
CHEMBL3955818 3 7.06
CHEMBL3895782 3 6.97
CHEMBL3967732 3 6.72
CHEMBL3942483 3 6.69
CHEMBL3943554 3 6.69
CHEMBL3913590 3 6.62
CHEMBL3986852 3 6.58
CHEMBL4115060 3 6.47
CHEMBL3956661 3 6.42
CHEMBL3961663 3 6.34
CHEMBL3947713 3 6.30
CHEMBL3925377 3 6.27
CHEMBL3896827 3 6.24
CHEMBL3975020 3 6.22
CHEMBL4114182 3 6.22
CHEMBL3955667 3 6.21
CHEMBL3938919 3 6.19
CHEMBL3934575 3 6.19
CHEMBL3890659 3 6.16
CHEMBL3920205 3 6.13
CHEMBL3916385 3 6.12
CHEMBL3897592 3 6.10
CHEMBL3919361 3 6.07
CHEMBL3918318 3 6.04
CHEMBL3896841 3 6.03
CHEMBL3906916 3 6.00
CHEMBL3961115 3 6.00
CHEMBL3972093 3 6.00

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3967592 IC50 = 61.0 nM 7.21
CHEMBL3972676 IC50 = 85.0 nM 7.07
CHEMBL3955818 IC50 = 87.3 nM 7.06
CHEMBL3895782 IC50 = 108.0 nM 6.97
CHEMBL3967732 IC50 = 190.0 nM 6.72
CHEMBL3943554 IC50 = 204.0 nM 6.69
CHEMBL3942483 IC50 = 203.0 nM 6.69
CHEMBL3913590 IC50 = 239.0 nM 6.62
CHEMBL3986852 IC50 = 265.0 nM 6.58
CHEMBL4115060 IC50 = 342.0 nM 6.47
CHEMBL3956661 IC50 = 377.0 nM 6.42
CHEMBL3961663 IC50 = 457.0 nM 6.34
CHEMBL3947713 IC50 = 502.0 nM 6.30
CHEMBL3925377 IC50 = 539.0 nM 6.27
CHEMBL3896827 IC50 = 570.0 nM 6.24
CHEMBL4114182 IC50 = 597.0 nM 6.22
CHEMBL3975020 IC50 = 596.0 nM 6.22
CHEMBL3955667 IC50 = 616.0 nM 6.21
CHEMBL3938919 IC50 = 647.0 nM 6.19
CHEMBL3934575 IC50 = 646.0 nM 6.19
CHEMBL3890659 IC50 = 693.0 nM 6.16
CHEMBL3920205 IC50 = 738.0 nM 6.13
CHEMBL3916385 IC50 = 755.0 nM 6.12
CHEMBL3897592 IC50 = 789.0 nM 6.10
CHEMBL3919361 IC50 = 857.0 nM 6.07
CHEMBL3918318 IC50 = 915.0 nM 6.04
CHEMBL3896841 IC50 = 943.0 nM 6.03
CHEMBL3972093 IC50 = 1010.0 nM 6.00
CHEMBL3961115 IC50 = 990.0 nM 6.00
CHEMBL3906916 IC50 = 1010.0 nM 6.00
CHEMBL3891784 IC50 = 1110.0 nM 5.96
CHEMBL3929122 IC50 = 1130.0 nM 5.95
CHEMBL3901454 IC50 = 1360.0 nM 5.87
CHEMBL3894204 IC50 = 1390.0 nM 5.86
CHEMBL3980597 IC50 = 1370.0 nM 5.86
CHEMBL3981462 IC50 = 1410.0 nM 5.85
CHEMBL3975426 IC50 = 1400.0 nM 5.85
CHEMBL4109276 IC50 = 1490.0 nM 5.83
CHEMBL3904602 LEROCICLIB IC50 = 1510.0 nM 5.82
CHEMBL3973056 IC50 = 1500.0 nM 5.82
CHEMBL4112645 IC50 = 1560.0 nM 5.81
CHEMBL3894860 TRILACICLIB IC50 = 1670.0 nM 5.78
CHEMBL3892888 IC50 = 1840.0 nM 5.74
CHEMBL3920345 IC50 = 1880.0 nM 5.73
CHEMBL3917699 IC50 = 1890.0 nM 5.72
CHEMBL4111196 IC50 = 2130.0 nM 5.67
CHEMBL3980597 IC50 = 2130.0 nM 5.67
CHEMBL3899618 IC50 = 2570.0 nM 5.59
CHEMBL6009736 IC50 = 2640.0 nM 5.58
CHEMBL3984435 IC50 = 2830.0 nM 5.55