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Assay Detail

CHEMBL5731333

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Binding
P70S6K Enzyme Assay: P70S6K inhibitor compounds were diluted and plated in 96 well plates. A reaction mixture including the following components was then added to the compound plate to initiate the enzyme reaction; P70S6K (3 nM, T412E mutant, Millipore) was mixed with 24 μM ATP in an assay buffer containing 100 mM Hepes (pH 7.5), 5 mM MgCl2, 1 mM DTT, 0.015% Brij and 1 μM of the substrate peptide FITC-AHA-AKRRRLSSLRA-OH (derived from the S6 ribosomal protein sequence, FITC=fluorescein isothiocyanate, AHA=6-aminohexanoic acid). The reaction was incubated for 90 min at 25° C., before the addition of 10 mM EDTA to stop the reaction. The proportion of substrate and product (phosphorylated) peptide was analysed on a Caliper Life Sciences Lab Chip 3000, using a pressure of −1.4 psi, and upstream and downstream voltages of −3000 and −700 respectively. Product peaks were resolved before substrate peaks on the resulting chromatograms.
729
Total Activities
243
Compounds Tested
3
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Confidence 0 — Uncurated / Unknown
Curated By Autocuration

Target

Unchecked (CHEMBL612545)
Type UNCHECKED

Publication

Aminopyrimidine derivatives for use as modulators of kinase activity
(2018)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 243 6.93 9.10
kon 243 - -
k_off 243 - -

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL4106847 3 9.10
CHEMBL3929756 3 9.05
CHEMBL3942270 3 8.89
CHEMBL3896291 3 8.85
CHEMBL3896704 3 8.77
CHEMBL3957511 3 8.70
CHEMBL3982464 3 8.66
CHEMBL3964354 3 8.60
CHEMBL4110986 3 8.59
CHEMBL3964273 3 8.59
CHEMBL3934983 3 8.59
CHEMBL3936890 3 8.55
CHEMBL4114630 3 8.49
CHEMBL3911701 3 8.48
CHEMBL3917646 3 8.48
CHEMBL4110173 3 8.47
CHEMBL3906331 3 8.47
CHEMBL3932608 3 8.47
CHEMBL3915352 3 8.40
CHEMBL3972358 3 8.39
CHEMBL3948645 3 8.38
CHEMBL3920854 3 8.36
CHEMBL3903649 3 8.35
CHEMBL3935973 3 8.35
CHEMBL3930957 3 8.34
CHEMBL3905652 3 8.33
CHEMBL3929477 3 8.32
CHEMBL3928625 3 8.31
CHEMBL4111671 3 8.31
CHEMBL3947951 3 8.28

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL4106847 IC50 = 0.8 nM 9.10
CHEMBL3929756 IC50 = 0.9 nM 9.05
CHEMBL3942270 IC50 = 1.3 nM 8.89
CHEMBL3896291 IC50 = 1.4 nM 8.85
CHEMBL3896704 IC50 = 1.7 nM 8.77
CHEMBL3957511 IC50 = 2.0 nM 8.70
CHEMBL3982464 IC50 = 2.2 nM 8.66
CHEMBL3964354 IC50 = 2.5 nM 8.60
CHEMBL4110986 IC50 = 2.6 nM 8.59
CHEMBL3964273 IC50 = 2.6 nM 8.59
CHEMBL3934983 IC50 = 2.6 nM 8.59
CHEMBL3936890 IC50 = 2.8 nM 8.55
CHEMBL4114630 IC50 = 3.2 nM 8.49
CHEMBL3911701 IC50 = 3.3 nM 8.48
CHEMBL3917646 IC50 = 3.3 nM 8.48
CHEMBL3932608 IC50 = 3.4 nM 8.47
CHEMBL3906331 IC50 = 3.4 nM 8.47
CHEMBL4110173 IC50 = 3.4 nM 8.47
CHEMBL3915352 IC50 = 4.0 nM 8.40
CHEMBL3972358 IC50 = 4.1 nM 8.39
CHEMBL3948645 IC50 = 4.2 nM 8.38
CHEMBL3920854 IC50 = 4.4 nM 8.36
CHEMBL3903649 IC50 = 4.5 nM 8.35
CHEMBL3935973 IC50 = 4.5 nM 8.35
CHEMBL3930957 IC50 = 4.6 nM 8.34
CHEMBL3905652 IC50 = 4.7 nM 8.33
CHEMBL3929477 IC50 = 4.8 nM 8.32
CHEMBL4111671 IC50 = 4.9 nM 8.31
CHEMBL3928625 IC50 = 4.9 nM 8.31
CHEMBL3947951 IC50 = 5.3 nM 8.28
CHEMBL3913380 IC50 = 5.3 nM 8.28
CHEMBL3933677 IC50 = 5.2 nM 8.28
CHEMBL3918502 IC50 = 5.8 nM 8.24
CHEMBL3957113 IC50 = 5.8 nM 8.24
CHEMBL3892901 IC50 = 5.7 nM 8.24
CHEMBL3906780 IC50 = 5.9 nM 8.23
CHEMBL3928221 IC50 = 6.0 nM 8.22
CHEMBL3929706 IC50 = 6.0 nM 8.22
CHEMBL3955537 IC50 = 6.1 nM 8.21
CHEMBL3890900 IC50 = 6.3 nM 8.20
CHEMBL3916166 IC50 = 7.2 nM 8.14
CHEMBL3933781 IC50 = 8.5 nM 8.07
CHEMBL3897935 IC50 = 9.1 nM 8.04
CHEMBL3963726 IC50 = 9.5 nM 8.02
CHEMBL3942101 IC50 = 9.8 nM 8.01
CHEMBL3978726 IC50 = 11.0 nM 7.96
CHEMBL3986206 IC50 = 11.0 nM 7.96
CHEMBL3940443 IC50 = 11.0 nM 7.96
CHEMBL3909882 IC50 = 11.0 nM 7.96
CHEMBL3980046 IC50 = 12.0 nM 7.92