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Assay Detail

CHEMBL5731448

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Binding
Biacore Assay: The test compounds were dissolved in 1% acetic acid and further complemented with an equal volume of DMSO. The resulting stock solutions were serially diluted in 0.5% acetic acid/50% DMSO. 1 μL aliquots of these solutions were placed into 384 well microplates (Greiner, black, transparent bottom), followed by 30 μL of diluted human citrated plasma (platelet-poor, final concentration: 5%; supplemented with fibrinogen, final concentration: 3 μM; dilution buffer: 20 mM HEPES, 150 mM NaCl, 0.01% Brij (pH 7)). The reactions were started by addition of 20 L of CaCl2 (final concentration: 10 mM), and tPA (tissue plasminogen activator, final concentration: 0.2 nM) in dilution buffer, followed by an additional volume of 20 μL dilution buffer for improved mixing. The reactions were incubated at 37° C. Clot formation and degradation was monitored spectrophotometrically by kinetic optical density measurements at 405 nm.
315
Total Activities
100
Compounds Tested
3
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Confidence 0 — Uncurated / Unknown
Curated By Autocuration

Target

Unchecked (CHEMBL612545)
Type UNCHECKED

Publication

(Aza)pyridopyrazolopyrimidinones and indazolopyrimidinones and their use
(2018)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 105 7.56 8.00
kon 105 - -
k_off 105 - -

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL5897890 6 8.00
CHEMBL4536269 3 7.96
CHEMBL4578240 3 7.96
CHEMBL6062318 3 7.89
CHEMBL5928912 3 7.89
CHEMBL6011509 3 7.89
CHEMBL5980444 3 7.89
CHEMBL5933220 6 7.89
CHEMBL5872096 3 7.85
CHEMBL5896722 6 7.85
CHEMBL5774413 3 7.85
CHEMBL6031955 3 7.85
CHEMBL5977403 3 7.85
CHEMBL5901899 3 7.82
CHEMBL5976620 3 7.82
CHEMBL5791398 3 7.82
CHEMBL5803225 3 7.82
CHEMBL5315598 6 7.82
CHEMBL5838352 3 7.82
CHEMBL5957884 3 7.82
CHEMBL6040865 3 7.82
CHEMBL5754051 3 7.82
CHEMBL5818228 3 7.80
CHEMBL6020010 3 7.80
CHEMBL5756524 3 7.80
CHEMBL5908431 3 7.77
CHEMBL5765780 3 7.75
CHEMBL5853281 3 7.75
CHEMBL5998204 3 7.75
CHEMBL5826177 3 7.75

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL5897890 IC50 = 10.0 nM 8.00
CHEMBL4578240 IC50 = 11.0 nM 7.96
CHEMBL4536269 IC50 = 11.0 nM 7.96
CHEMBL5980444 IC50 = 13.0 nM 7.89
CHEMBL6062318 IC50 = 13.0 nM 7.89
CHEMBL6011509 IC50 = 13.0 nM 7.89
CHEMBL5933220 IC50 = 13.0 nM 7.89
CHEMBL5928912 IC50 = 13.0 nM 7.89
CHEMBL5977403 IC50 = 14.0 nM 7.85
CHEMBL6031955 IC50 = 14.0 nM 7.85
CHEMBL5774413 IC50 = 14.0 nM 7.85
CHEMBL5872096 IC50 = 14.0 nM 7.85
CHEMBL5896722 IC50 = 14.0 nM 7.85
CHEMBL5957884 IC50 = 15.0 nM 7.82
CHEMBL5838352 IC50 = 15.0 nM 7.82
CHEMBL5754051 IC50 = 15.0 nM 7.82
CHEMBL5791398 IC50 = 15.0 nM 7.82
CHEMBL5901899 IC50 = 15.0 nM 7.82
CHEMBL5976620 IC50 = 15.0 nM 7.82
CHEMBL5803225 IC50 = 15.0 nM 7.82
CHEMBL6040865 IC50 = 15.0 nM 7.82
CHEMBL5315598 IC50 = 15.0 nM 7.82
CHEMBL5756524 IC50 = 16.0 nM 7.80
CHEMBL5818228 IC50 = 16.0 nM 7.80
CHEMBL6020010 IC50 = 16.0 nM 7.80
CHEMBL5908431 IC50 = 17.0 nM 7.77
CHEMBL5998204 IC50 = 18.0 nM 7.75
CHEMBL5933220 IC50 = 18.0 nM 7.75
CHEMBL5765780 IC50 = 18.0 nM 7.75
CHEMBL5853281 IC50 = 18.0 nM 7.75
CHEMBL5826177 IC50 = 18.0 nM 7.75
CHEMBL5774198 IC50 = 19.0 nM 7.72
CHEMBL5987508 IC50 = 20.0 nM 7.70
CHEMBL6002758 IC50 = 20.0 nM 7.70
CHEMBL5966749 IC50 = 21.0 nM 7.68
CHEMBL5897890 IC50 = 21.0 nM 7.68
CHEMBL5989259 IC50 = 22.0 nM 7.66
CHEMBL5928184 IC50 = 22.0 nM 7.66
CHEMBL5777260 IC50 = 23.0 nM 7.64
CHEMBL5745904 IC50 = 23.0 nM 7.64
CHEMBL5886142 IC50 = 23.0 nM 7.64
CHEMBL5787752 IC50 = 24.0 nM 7.62
CHEMBL5753283 IC50 = 24.0 nM 7.62
CHEMBL5976342 IC50 = 24.0 nM 7.62
CHEMBL5822208 IC50 = 24.0 nM 7.62
CHEMBL5930231 IC50 = 25.0 nM 7.60
CHEMBL5766019 IC50 = 25.0 nM 7.60
CHEMBL5989533 IC50 = 25.0 nM 7.60
CHEMBL5778636 IC50 = 26.0 nM 7.58
CHEMBL5847667 IC50 = 26.0 nM 7.58