Skip to main content
Free research Free research Free assay review with research home and workspace preview
Quick search ChEMBL 36
Assay Detail

CHEMBL5731492

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Inhibition of ALK WT Anaplastic Lymphoma Kinase Activity: The following experiment was performed in order to measure the activity of the N2-(2-methoxyphenyl)pyrimidine derivative represented by formula 1 of the present invention to inhibit anaplastic lymphoma kinase (ALK) activity at enzyme level. To measure the activity to inhibit ALK, each of the compounds prepared in examples listed in table 2 (2 μl) was loaded in a 384 well plate. Then, each of the compounds was mixed with anaplastic lymphoma kinase (ALK) enzyme (1 μl) and biotin conjugated peptide substrate (2 μl), followed by culture for 15 minutes. ATP solution (5 μl) was added thereto, followed by kinase reaction at room temperature for 30 minutes. Streptavidin conjugated XL 665 (5 μl) dissolved in ethylenediaminetetraacetic acid solution and europium (Eu3+) conjugated anti-phosphotyrosine antibody (5 μl) were added to the reaction solution to terminate the reaction. Upon completion of the reaction, one hour culture was performed, followed by analysis using homogeneous time-resolved fluorescence (HTRF, Cisbio). OD615/665 was measured with Wallac Envision 2103. IC50 of each compound was determined by using prism software (Version 5.01, Graphpad).
216
Total Activities
72
Compounds Tested
3
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

ALK tyrosine kinase receptor (CHEMBL4247)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

N2-(2-methoxyphenyl)pyrimidine derivative, method for preparing same, and pharmaceutical composition for cancer prevention or treatment containing same as active ingredient
(2018)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 72 7.89 9.36
kon 72 - -
k_off 72 - -

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL5907234 3 9.36
CHEMBL5957476 3 9.08
CHEMBL5757765 3 9.06
CHEMBL5908825 3 9.00
CHEMBL5812517 3 9.00
CHEMBL4078406 3 8.92
CHEMBL4099660 3 8.85
CHEMBL4091928 3 8.82
CHEMBL4089672 3 8.82
CHEMBL4080869 3 8.82
CHEMBL4067503 3 8.76
CHEMBL6030742 3 8.72
CHEMBL4070217 3 8.71
CHEMBL6006760 3 8.70
CHEMBL5764344 3 8.70
CHEMBL4096452 3 8.68
CHEMBL4084168 3 8.66
CHEMBL5835139 3 8.59
CHEMBL4081656 3 8.57
CHEMBL4105099 3 8.55
CHEMBL5990800 3 8.51
CHEMBL5782444 3 8.47
CHEMBL4097392 3 8.47
CHEMBL5831597 3 8.46
CHEMBL5916115 3 8.43
CHEMBL5804159 3 8.42
CHEMBL6047646 3 8.40
CHEMBL4071105 3 8.40
CHEMBL5947897 3 8.40
CHEMBL6003895 3 8.38

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL5907234 IC50 = 0.44 nM 9.36
CHEMBL5957476 IC50 = 0.84 nM 9.08
CHEMBL5757765 IC50 = 0.88 nM 9.06
CHEMBL5812517 IC50 = 1.0 nM 9.00
CHEMBL5908825 IC50 = 1.0 nM 9.00
CHEMBL4078406 IC50 = 1.2 nM 8.92
CHEMBL4099660 IC50 = 1.4 nM 8.85
CHEMBL4080869 IC50 = 1.5 nM 8.82
CHEMBL4089672 IC50 = 1.5 nM 8.82
CHEMBL4091928 IC50 = 1.5 nM 8.82
CHEMBL4067503 IC50 = 1.74 nM 8.76
CHEMBL6030742 IC50 = 1.9 nM 8.72
CHEMBL4070217 IC50 = 1.93 nM 8.71
CHEMBL5764344 IC50 = 2.0 nM 8.70
CHEMBL6006760 IC50 = 2.0 nM 8.70
CHEMBL4096452 IC50 = 2.1 nM 8.68
CHEMBL4084168 IC50 = 2.2 nM 8.66
CHEMBL5835139 IC50 = 2.6 nM 8.59
CHEMBL4081656 IC50 = 2.7 nM 8.57
CHEMBL4105099 IC50 = 2.8 nM 8.55
CHEMBL5990800 IC50 = 3.1 nM 8.51
CHEMBL4097392 IC50 = 3.37 nM 8.47
CHEMBL5782444 IC50 = 3.4 nM 8.47
CHEMBL5831597 IC50 = 3.5 nM 8.46
CHEMBL5916115 IC50 = 3.7 nM 8.43
CHEMBL5804159 IC50 = 3.8 nM 8.42
CHEMBL6047646 IC50 = 4.0 nM 8.40
CHEMBL4071105 IC50 = 4.0 nM 8.40
CHEMBL5947897 IC50 = 4.0 nM 8.40
CHEMBL6003895 IC50 = 4.2 nM 8.38
CHEMBL4088751 IC50 = 4.72 nM 8.33
CHEMBL5793829 IC50 = 4.8 nM 8.32
CHEMBL4062466 IC50 = 4.9 nM 8.31
CHEMBL4061549 IC50 = 7.8 nM 8.11
CHEMBL5872198 IC50 = 9.5 nM 8.02
CHEMBL5864674 IC50 = 10.0 nM 8.00
CHEMBL5895722 IC50 = 10.0 nM 8.00
CHEMBL5983550 IC50 = 10.0 nM 8.00
CHEMBL5877236 IC50 = 10.0 nM 8.00
CHEMBL5748068 IC50 = 10.0 nM 8.00
CHEMBL5780443 IC50 = 10.0 nM 8.00
CHEMBL5742478 IC50 = 10.0 nM 8.00
CHEMBL5790566 IC50 = 10.0 nM 8.00
CHEMBL5751408 IC50 = 12.0 nM 7.92
CHEMBL5985163 IC50 = 12.0 nM 7.92
CHEMBL6011332 IC50 = 20.0 nM 7.70
CHEMBL4089527 IC50 = 21.0 nM 7.68
CHEMBL5746465 IC50 = 26.0 nM 7.58
CHEMBL6014384 IC50 = 30.0 nM 7.52
CHEMBL6052776 IC50 = 30.0 nM 7.52