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Assay Detail

CHEMBL5732092

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Binding
Enzymatic Assay: PARP-2 and PARP-3 enzymatic assays were conducted using commercial PARP-2/PARP-3 Chemiluminescent Assay Kit (BPS Biosciences) and the protocols with the kits. Briefly, histones were coated in a high binding plate first, and incubated with PARP-2 or PARP-3, and increasing concentrations of compounds for 0.5 h. Then, biotinylated NAD and activated DNA were added to the wells. The biotinylated PARylation product was measured by adding streptavidin-HRP and HRP substrates which produce chemiluminescence. The IC50s were calculated based on residual enzyme activity in presence of increasing concentrations of compounds.
66
Total Activities
21
Compounds Tested
3
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Confidence 0 — Uncurated / Unknown
Curated By Autocuration

Target

Unchecked (CHEMBL612545)
Type UNCHECKED

Publication

Fused tetra or penta-cyclic dihydrodiazepinocarbazolones as PARP inhibitors
(2017)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 22 6.09 6.70
kon 22 - -
k_off 22 - -

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3984980 3 6.70
CHEMBL3922789 3 6.52
CHEMBL3926240 3 6.52
CHEMBL3933450 3 6.52
CHEMBL4107982 3 6.40
CHEMBL4112930 PAMIPARIB 3.0 3 6.30
CHEMBL3955609 3 6.30
CHEMBL3972156 3 6.22
CHEMBL3901034 3 6.16
CHEMBL3914932 6 6.16
CHEMBL3929705 3 6.10
CHEMBL3907535 3 6.10
CHEMBL3961684 3 6.05
CHEMBL3970252 3 6.00
CHEMBL3907218 3 5.96
CHEMBL3969742 3 5.96
CHEMBL3978989 3 5.89
CHEMBL3892363 3 5.80
CHEMBL3915929 3 5.77
CHEMBL3891329 3 5.72
CHEMBL3940569 3 4.68

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3984980 IC50 = 200.0 nM 6.70
CHEMBL3922789 IC50 = 300.0 nM 6.52
CHEMBL3926240 IC50 = 300.0 nM 6.52
CHEMBL3933450 IC50 = 300.0 nM 6.52
CHEMBL4107982 IC50 = 400.0 nM 6.40
CHEMBL3955609 IC50 = 500.0 nM 6.30
CHEMBL4112930 PAMIPARIB IC50 = 500.0 nM 6.30
CHEMBL3972156 IC50 = 600.0 nM 6.22
CHEMBL3914932 IC50 = 700.0 nM 6.16
CHEMBL3901034 IC50 = 700.0 nM 6.16
CHEMBL3914932 IC50 = 700.0 nM 6.16
CHEMBL3907535 IC50 = 800.0 nM 6.10
CHEMBL3929705 IC50 = 800.0 nM 6.10
CHEMBL3961684 IC50 = 900.0 nM 6.05
CHEMBL3970252 IC50 = 1000.0 nM 6.00
CHEMBL3969742 IC50 = 1100.0 nM 5.96
CHEMBL3907218 IC50 = 1100.0 nM 5.96
CHEMBL3978989 IC50 = 1300.0 nM 5.89
CHEMBL3892363 IC50 = 1600.0 nM 5.80
CHEMBL3915929 IC50 = 1700.0 nM 5.77
CHEMBL3891329 IC50 = 1900.0 nM 5.72
CHEMBL3940569 IC50 = 21000.0 nM 4.68
CHEMBL3907535 kon = - -
CHEMBL3978989 kon = - -
CHEMBL3907535 k_off = - s-1 -
CHEMBL3922789 k_off = - s-1 -
CHEMBL3914932 kon = - -
CHEMBL3891329 kon = - -
CHEMBL3891329 k_off = - s-1 -
CHEMBL3969742 kon = - -
CHEMBL3969742 k_off = - s-1 -
CHEMBL3915929 kon = - -
CHEMBL3915929 k_off = - s-1 -
CHEMBL3892363 kon = - -
CHEMBL3892363 k_off = - s-1 -
CHEMBL3907218 kon = - -
CHEMBL3978989 k_off = - s-1 -
CHEMBL3970252 kon = - -
CHEMBL3940569 k_off = - s-1 -
CHEMBL3940569 kon = - -
CHEMBL3922789 kon = - -
CHEMBL3926240 k_off = - s-1 -
CHEMBL4107982 kon = - -
CHEMBL3926240 kon = - -
CHEMBL4107982 k_off = - s-1 -
CHEMBL4112930 PAMIPARIB kon = - -
CHEMBL3984980 k_off = - s-1 -
CHEMBL3984980 kon = - -
CHEMBL4112930 PAMIPARIB k_off = - s-1 -
CHEMBL3970252 k_off = - s-1 -