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Assay Detail

CHEMBL5732093

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Binding
Enzymatic Assay: PARP-2 and PARP-3 enzymatic assays were conducted using commercial PARP-2/PARP-3 Chemiluminescent Assay Kit (BPS Biosciences) and the protocols with the kits. Briefly, histones were coated in a high binding plate first, and incubated with PARP-2 or PARP-3, and increasing concentrations of compounds for 0.5 h. Then, biotinylated NAD and activated DNA were added to the wells. The biotinylated PARylation product was measured by adding streptavidin-HRP and HRP substrates which produce chemiluminescence. The IC50s were calculated based on residual enzyme activity in presence of increasing concentrations of compounds.
30
Total Activities
10
Compounds Tested
3
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Confidence 0 — Uncurated / Unknown
Curated By Autocuration

Target

Unchecked (CHEMBL612545)
Type UNCHECKED

Publication

Fused tetra or penta-cyclic dihydrodiazepinocarbazolones as PARP inhibitors
(2017)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 10 4.75 4.75
kon 10 - -
k_off 10 - -

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3970252 3 4.75
CHEMBL3891329 3 -
CHEMBL3911687 3 -
CHEMBL3984980 3 -
CHEMBL3926240 3 -
CHEMBL3940569 3 -
CHEMBL3907535 3 -
CHEMBL3922789 3 -
CHEMBL3978989 3 -
CHEMBL4112930 PAMIPARIB 3.0 3 -

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3970252 IC50 = 18000.0 nM 4.75
CHEMBL3891329 IC50 = 199000.0 nM -
CHEMBL3891329 kon = - -
CHEMBL3891329 k_off = - s-1 -
CHEMBL3911687 IC50 = 136000.0 nM -
CHEMBL3911687 kon = - -
CHEMBL3911687 k_off = - s-1 -
CHEMBL3984980 IC50 > 20000000.0 nM -
CHEMBL3984980 kon = - -
CHEMBL3984980 k_off = - s-1 -
CHEMBL3926240 IC50 = 11000000.0 nM -
CHEMBL3926240 kon = - -
CHEMBL3926240 k_off = - s-1 -
CHEMBL3940569 IC50 = 1000000.0 nM -
CHEMBL3940569 kon = - -
CHEMBL3940569 k_off = - s-1 -
CHEMBL3907535 kon = - -
CHEMBL3907535 k_off = - s-1 -
CHEMBL3922789 IC50 = 180000.0 nM -
CHEMBL3922789 kon = - -
CHEMBL3922789 k_off = - s-1 -
CHEMBL3978989 IC50 = 660000.0 nM -
CHEMBL3978989 kon = - -
CHEMBL3978989 k_off = - s-1 -
CHEMBL3970252 kon = - -
CHEMBL3970252 k_off = - s-1 -
CHEMBL4112930 PAMIPARIB IC50 = 185000.0 nM -
CHEMBL4112930 PAMIPARIB kon = - -
CHEMBL4112930 PAMIPARIB k_off = - s-1 -
CHEMBL3907535 IC50 = 760000.0 nM -