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Assay Detail

CHEMBL5733141

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Binding
Electrophysiological Assay: Current record was obtained by an automated patch clamp system “IonWorks Quattro (Molecular Devices Corporation)” in Population Patch Clamp mode. The operation was conducted in accordance with the operating procedure of the system. A Dulbecco's phosphate buffer containing calcium and magnesium (Sigma) was used as an extracellular fluid, and a low C1-buffer (100 mM K-gluconate, 40 mM KCl, 3.2 mM MgCl2, 5 mM EGTA, 5 mM Hepes, pH 7.3) was used as an intracellular fluid. A test compound was dissolved in dimethylsulfoxide (DMSO) to prepare a 30 mM stock solution, so as to produce 4-fold serial dilutions with the extracellular fluid for attaining a DMSO concentration of 0.3% in measurement.The hNav 1.7/β1/β2 cells cultured to a 70-80% confluent state in a T150 flask (Sumilon) were washed with PBS and subsequently with versene (Invitrogen Corp.), and collected by allowing to react with 0.05% trypsin (Invitrogen Corp.) at 37° C. for 3 minutes. After washing with a culture medium, the resultant cells were suspended in an extracellular fluid at a concentration of 2×10−6 cells/ml so as to be used for the measurement. The cell membrane was perforated by using an intracellular fluid including 100 μg/ml amphotericin B (Sigma).
501
Total Activities
151
Compounds Tested
3
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Confidence 0 — Uncurated / Unknown
Curated By Autocuration

Target

Unchecked (CHEMBL612545)
Type UNCHECKED

Publication

Cycloalkane derivatives
(2017)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 167 6.84 8.59
kon 167 - -
k_off 167 - -

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL3341987 3 8.59
CHEMBL5951163 3 8.00
CHEMBL4642571 3 7.92
CHEMBL5997729 3 7.85
CHEMBL5766420 3 7.85
CHEMBL4633566 DS-1971 2.0 9 7.80
CHEMBL4632675 3 7.77
CHEMBL5919308 3 7.77
CHEMBL6042460 3 7.77
CHEMBL6032717 6 7.75
CHEMBL5885552 6 7.70
CHEMBL6065862 6 7.68
CHEMBL6047665 6 7.68
CHEMBL5920808 3 7.64
CHEMBL5797265 3 7.62
CHEMBL4637488 3 7.62
CHEMBL4633573 3 7.55
CHEMBL4642940 3 7.55
CHEMBL5820558 3 7.55
CHEMBL5809919 3 7.55
CHEMBL5859742 3 7.52
CHEMBL4648397 3 7.52
CHEMBL5906846 6 7.52
CHEMBL5759294 3 7.52
CHEMBL6051900 3 7.51
CHEMBL4639987 3 7.51
CHEMBL5850211 6 7.47
CHEMBL5828168 3 7.47
CHEMBL5782845 3 7.47
CHEMBL5954809 3 7.46

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL3341987 IC50 = 2.6 nM 8.59
CHEMBL5951163 IC50 = 10.0 nM 8.00
CHEMBL4642571 IC50 = 12.0 nM 7.92
CHEMBL5997729 IC50 = 14.0 nM 7.85
CHEMBL5766420 IC50 = 14.0 nM 7.85
CHEMBL4633566 DS-1971 IC50 = 16.0 nM 7.80
CHEMBL4632675 IC50 = 17.0 nM 7.77
CHEMBL6042460 IC50 = 17.0 nM 7.77
CHEMBL4633566 DS-1971 IC50 = 17.0 nM 7.77
CHEMBL5919308 IC50 = 17.0 nM 7.77
CHEMBL6032717 IC50 = 18.0 nM 7.75
CHEMBL5885552 IC50 = 20.0 nM 7.70
CHEMBL4633566 DS-1971 IC50 = 20.0 nM 7.70
CHEMBL6065862 IC50 = 21.0 nM 7.68
CHEMBL6047665 IC50 = 21.0 nM 7.68
CHEMBL5920808 IC50 = 23.0 nM 7.64
CHEMBL6032717 IC50 = 24.0 nM 7.62
CHEMBL4637488 IC50 = 24.0 nM 7.62
CHEMBL5797265 IC50 = 24.0 nM 7.62
CHEMBL5809919 IC50 = 28.0 nM 7.55
CHEMBL4633573 IC50 = 28.0 nM 7.55
CHEMBL5820558 IC50 = 28.0 nM 7.55
CHEMBL4642940 IC50 = 28.0 nM 7.55
CHEMBL5759294 IC50 = 30.0 nM 7.52
CHEMBL5859742 IC50 = 30.0 nM 7.52
CHEMBL4648397 IC50 = 30.0 nM 7.52
CHEMBL5906846 IC50 = 30.0 nM 7.52
CHEMBL6051900 IC50 = 31.0 nM 7.51
CHEMBL4639987 IC50 = 31.0 nM 7.51
CHEMBL6047665 IC50 = 34.0 nM 7.47
CHEMBL5850211 IC50 = 34.0 nM 7.47
CHEMBL5828168 IC50 = 34.0 nM 7.47
CHEMBL5782845 IC50 = 34.0 nM 7.47
CHEMBL5954809 IC50 = 35.0 nM 7.46
CHEMBL5942489 IC50 = 36.0 nM 7.44
CHEMBL5982581 IC50 = 36.0 nM 7.44
CHEMBL5832501 IC50 = 36.0 nM 7.44
CHEMBL5908326 IC50 = 36.0 nM 7.44
CHEMBL5874813 IC50 = 37.0 nM 7.43
CHEMBL5893254 IC50 = 39.0 nM 7.41
CHEMBL5814622 IC50 = 39.0 nM 7.41
CHEMBL6007178 IC50 = 40.0 nM 7.40
CHEMBL6022416 IC50 = 41.0 nM 7.39
CHEMBL5828972 IC50 = 42.0 nM 7.38
CHEMBL4645788 IC50 = 43.0 nM 7.37
CHEMBL5885536 IC50 = 43.0 nM 7.37
CHEMBL5914751 IC50 = 43.0 nM 7.37
CHEMBL4637909 IC50 = 45.0 nM 7.35
CHEMBL5795567 IC50 = 46.0 nM 7.34
CHEMBL5773554 IC50 = 46.0 nM 7.34