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Assay Detail

CHEMBL5734691

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Interleukin 6 Induction Assay: Compounds diluted in DMSO were transferred to individual wells of a Matrix Technologies clear, V-bottom 384-well plate using ECHO acoustic liquid handling technology (25 nL per well). Human whole-blood samples (25 uL) were added to each well using a CyBio FeliX liquid handling instrument. The plate was shaken on a plate shaker for three min before incubating the reaction mixtures at 37° C. for 20 h. Basel RPMI 1640 medium (supplemented with L-glutamine) was then added to each well (25 uL per well) prior to liberating plasma from each sample by centrifugation (450×g, 5 min, ambient temperature). Treated plasma samples (3 uL) were subsequently transferred to individual wells of a white, shallow, 384-well ProxiPlate (Perkin Elmer) using the FeliX liquid handling instrument and their interleukin 6 levels were measured using AlphaLISA technology as described by the manufacturer, PerkinElmer. Data analyses software was used to determine compound EC50 values where the baseline was established using average DMSO values and 100% induction established using reference compound values at the highest concentration tested. EC50's can be determined with software such as Graphpad Prism.
171
Total Activities
54
Compounds Tested
3
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Confidence 8 — Homologous single protein target
Curated By Autocuration

Target

Interleukin-6 (CHEMBL1795129)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Toll-like receptor 7 (TLR7) agonists having heteroatom-linked aromatic moieties, conjugates thereof, and methods and uses therefor
(2019)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
EC50 57 7.60 8.60
kon 57 - -
k_off 57 - -

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL5967615 3 8.60
CHEMBL5757665 3 8.42
CHEMBL5993886 3 8.42
CHEMBL5977638 6 8.29
CHEMBL5790478 3 8.24
CHEMBL5992328 3 8.23
CHEMBL6041191 3 8.18
CHEMBL5948820 3 8.12
CHEMBL5778223 3 8.12
CHEMBL5950488 3 8.11
CHEMBL5865451 3 8.09
CHEMBL5863568 3 8.02
CHEMBL5757312 3 8.00
CHEMBL6057462 3 7.98
CHEMBL5935960 3 7.97
CHEMBL5801959 3 7.92
CHEMBL6040007 3 7.89
CHEMBL5972079 3 7.85
CHEMBL5769037 3 7.85
CHEMBL5926850 3 7.84
CHEMBL5849962 3 7.82
CHEMBL5947975 3 7.79
CHEMBL5845465 3 7.77
CHEMBL5949769 3 7.76
CHEMBL5936570 3 7.75
CHEMBL5943152 3 7.72
CHEMBL5745822 3 7.72
CHEMBL5985963 3 7.72
CHEMBL5778189 3 7.68
CHEMBL5813554 3 7.68

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL5967615 EC50 = 2.5 nM 8.60
CHEMBL5757665 EC50 = 3.8 nM 8.42
CHEMBL5993886 EC50 = 3.77 nM 8.42
CHEMBL5977638 EC50 = 5.11 nM 8.29
CHEMBL5790478 EC50 = 5.81 nM 8.24
CHEMBL5992328 EC50 = 5.91 nM 8.23
CHEMBL6041191 EC50 = 6.62 nM 8.18
CHEMBL5948820 EC50 = 7.5 nM 8.12
CHEMBL5778223 EC50 = 7.6 nM 8.12
CHEMBL5950488 EC50 = 7.8 nM 8.11
CHEMBL5865451 EC50 = 8.14 nM 8.09
CHEMBL5863568 EC50 = 9.57 nM 8.02
CHEMBL5757312 EC50 = 10.1 nM 8.00
CHEMBL6057462 EC50 = 10.4 nM 7.98
CHEMBL5935960 EC50 = 10.7 nM 7.97
CHEMBL5801959 EC50 = 12.0 nM 7.92
CHEMBL6040007 EC50 = 13.0 nM 7.89
CHEMBL5769037 EC50 = 14.0 nM 7.85
CHEMBL5972079 EC50 = 14.0 nM 7.85
CHEMBL5926850 EC50 = 14.3 nM 7.84
CHEMBL5849962 EC50 = 15.0 nM 7.82
CHEMBL5947975 EC50 = 16.1 nM 7.79
CHEMBL5845465 EC50 = 17.0 nM 7.77
CHEMBL5949769 EC50 = 17.3 nM 7.76
CHEMBL5936570 EC50 = 17.6 nM 7.75
CHEMBL5985963 EC50 = 19.0 nM 7.72
CHEMBL5943152 EC50 = 18.9 nM 7.72
CHEMBL5745822 EC50 = 19.0 nM 7.72
CHEMBL5813554 EC50 = 21.0 nM 7.68
CHEMBL5778189 EC50 = 20.7 nM 7.68
CHEMBL5788562 EC50 = 24.0 nM 7.62
CHEMBL5960544 EC50 = 24.0 nM 7.62
CHEMBL5831527 EC50 = 24.3 nM 7.61
CHEMBL6049946 EC50 = 25.0 nM 7.60
CHEMBL5757520 EC50 = 26.0 nM 7.58
CHEMBL5747710 EC50 = 28.0 nM 7.55
CHEMBL5986883 EC50 = 28.0 nM 7.55
CHEMBL6040035 EC50 = 29.0 nM 7.54
CHEMBL5772844 EC50 = 29.6 nM 7.53
CHEMBL5817643 EC50 = 30.9 nM 7.51
CHEMBL5872235 EC50 = 31.0 nM 7.51
CHEMBL6046238 EC50 = 44.2 nM 7.36
CHEMBL5977638 EC50 = 64.7 nM 7.19
CHEMBL5885144 EC50 = 68.0 nM 7.17
CHEMBL5862695 EC50 = 72.0 nM 7.14
CHEMBL5849169 EC50 = 75.0 nM 7.12
CHEMBL6049858 EC50 = 78.0 nM 7.11
CHEMBL5787885 EC50 = 84.8 nM 7.07
CHEMBL5823588 EC50 = 100.0 nM 7.00
CHEMBL5765280 EC50 = 104.0 nM 6.98