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Assay Detail

CHEMBL5734703

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Binding
Enzymatic Assay: Compounds were tested in an enzymatic assay using human ERK-2 (Mitogen Activated Kinase 1), recombinantly expressed as an n-terminal 6-His fusion protein in E. coli and corresponding to a 8-360. The substrate used was the fluorescent Omnia peptide S/T17 (Invitrogen of Carlsbad, Calif.; Cat. KNZ 171C). Test compounds were diluted in DMSO in 3-fold serial dilutions at 100× final concentrations. In addition to compound, the assay contained 50 mM HEPES [pH 7.3], 10 mM MgCl2, 2 mM DTT, 0.005% Triton-X100, 5 nM ERK-2 enzyme, 6.25 μM S/T17 peptide substrate and 25 μM ATP (corresponding to the observed Km) for a total reaction volume of 25 μL. The assay was run at ambient temperature in a white 384-well polypropylene plate (Nunc, Inc of Naperville, Ill.; Cat. 267462) collecting data every 50 seconds for approximately 30 minutes on an Envision plate reader (PerkinElmer, Inc. of Waltham, Mass.); Excitation 340 nm/Emission 495 nm.
330
Total Activities
106
Compounds Tested
3
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Mitogen-activated protein kinase 1 (CHEMBL4040)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Serine/threonine kinase inhibitors
(2019)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 110 9.23 10.70
kon 110 - -
k_off 110 - -

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL6045548 3 10.70
CHEMBL5863069 3 10.70
CHEMBL5999003 3 10.70
CHEMBL5908683 6 10.70
CHEMBL5806164 3 10.70
CHEMBL5927076 3 10.64
CHEMBL5776694 3 10.52
CHEMBL5945294 3 10.52
CHEMBL5887657 3 10.46
CHEMBL5833636 3 10.44
CHEMBL5891541 3 10.41
CHEMBL5744381 6 10.14
CHEMBL5876552 3 10.10
CHEMBL5985409 3 9.99
CHEMBL5914503 3 9.99
CHEMBL5768349 3 9.96
CHEMBL6055966 3 9.95
CHEMBL6050192 3 9.88
CHEMBL5970498 3 9.83
CHEMBL5843088 3 9.83
CHEMBL5959724 3 9.78
CHEMBL5958147 3 9.76
CHEMBL6024181 3 9.67
CHEMBL5932850 3 9.56
CHEMBL5904247 3 9.51
CHEMBL5952404 3 9.50
CHEMBL5929992 3 9.50
CHEMBL5765337 3 9.42
CHEMBL5988077 3 9.41
CHEMBL6056771 3 9.29

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL6045548 IC50 = 0.02 nM 10.70
CHEMBL5863069 IC50 = 0.02 nM 10.70
CHEMBL5806164 IC50 = 0.02 nM 10.70
CHEMBL5908683 IC50 = 0.02 nM 10.70
CHEMBL5999003 IC50 = 0.02 nM 10.70
CHEMBL5927076 IC50 = 0.023 nM 10.64
CHEMBL5776694 IC50 = 0.03 nM 10.52
CHEMBL5945294 IC50 = 0.03 nM 10.52
CHEMBL5887657 IC50 = 0.035 nM 10.46
CHEMBL5833636 IC50 = 0.036 nM 10.44
CHEMBL5891541 IC50 = 0.039 nM 10.41
CHEMBL5744381 IC50 = 0.073 nM 10.14
CHEMBL5876552 IC50 = 0.079 nM 10.10
CHEMBL5914503 IC50 = 0.103 nM 9.99
CHEMBL5985409 IC50 = 0.102 nM 9.99
CHEMBL5768349 IC50 = 0.111 nM 9.96
CHEMBL6055966 IC50 = 0.113 nM 9.95
CHEMBL6050192 IC50 = 0.132 nM 9.88
CHEMBL5970498 IC50 = 0.149 nM 9.83
CHEMBL5843088 IC50 = 0.149 nM 9.83
CHEMBL5959724 IC50 = 0.168 nM 9.78
CHEMBL5958147 IC50 = 0.173 nM 9.76
CHEMBL6024181 IC50 = 0.215 nM 9.67
CHEMBL5932850 IC50 = 0.273 nM 9.56
CHEMBL5904247 IC50 = 0.311 nM 9.51
CHEMBL5952404 IC50 = 0.316 nM 9.50
CHEMBL5929992 IC50 = 0.316 nM 9.50
CHEMBL5765337 IC50 = 0.38 nM 9.42
CHEMBL5988077 IC50 = 0.39 nM 9.41
CHEMBL6056771 IC50 = 0.512 nM 9.29
CHEMBL5877935 IC50 = 0.6 nM 9.22
CHEMBL5987978 IC50 = 0.66 nM 9.18
CHEMBL6044562 IC50 = 0.655 nM 9.18
CHEMBL5744391 IC50 = 0.751 nM 9.12
CHEMBL5891249 IC50 = 1.12 nM 8.95
CHEMBL5992303 IC50 = 1.15 nM 8.94
CHEMBL5764298 IC50 = 1.17 nM 8.93
CHEMBL5768025 IC50 = 1.33 nM 8.88
CHEMBL5834243 IC50 = 1.7 nM 8.77
CHEMBL5827057 IC50 = 1.85 nM 8.73
CHEMBL6039441 IC50 = 2.3 nM 8.64
CHEMBL5927578 IC50 = 2.34 nM 8.63
CHEMBL5798231 IC50 = 2.42 nM 8.62
CHEMBL5879549 IC50 = 2.55 nM 8.59
CHEMBL5879549 IC50 = 2.55 nM 8.59
CHEMBL5871770 IC50 = 2.77 nM 8.56
CHEMBL5908683 IC50 = 2.95 nM 8.53
CHEMBL6052694 IC50 = 3.22 nM 8.49
CHEMBL6011847 IC50 = 4.28 nM 8.37
CHEMBL5821428 IC50 = 4.61 nM 8.34