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Assay Detail

CHEMBL5734704

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
In Vitro Assay: Briefly, bulk histones, histone peptides or nucleosomes are incubated with purified human recombinant KDM1A, in the histone demethylase activity (HDM) assay buffer 1 (50 mM Tris pH 8.5, 50 mM KCl, 5 mM MgCl, 0.5% BSA, and 5% glycerol) from 30 minutes to 4 hours at 37° C. A typical reaction is conducted in 100 microliters in which either 20 micrograms of purified bulk histones or 3 micrograms of modified histone peptides are used as substrates. Different amounts of KDM1A ranging from 1-20 micrograms are used in the reaction along with, as necessary, other co-factors such as FAD or CoREST, depending on the chosen substrate. The reaction mixture is analyzed by SDS-PAGE and Western blotting using histone methyl-specific antibodies or by formaldehyde formation assay to examine the removal and conversion of the methyl group to formaldehyde, or by mass spectrometry in the case of peptide substrates to identify the demethylated histone peptide.
501
Total Activities
165
Compounds Tested
3
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Lysine-specific histone demethylase 1A (CHEMBL6136)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

KDM1A inhibitors for the treatment of disease
(2019)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 167 4.92 6.10
kon 167 - -
k_off 167 - -

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL5905859 3 6.10
CHEMBL5880420 3 6.00
CHEMBL5765675 3 5.70
CHEMBL5742196 3 5.70
CHEMBL6028916 3 5.70
CHEMBL5778938 3 5.70
CHEMBL6056865 3 5.52
CHEMBL5981736 3 5.52
CHEMBL5847512 3 5.52
CHEMBL6014549 3 5.52
CHEMBL5807766 3 5.52
CHEMBL6045682 3 5.52
CHEMBL5967558 3 5.52
CHEMBL5812475 3 5.40
CHEMBL5847735 3 5.40
CHEMBL5908210 3 5.40
CHEMBL5928525 3 5.40
CHEMBL5787891 3 5.40
CHEMBL5866999 3 5.40
CHEMBL6032044 3 5.40
CHEMBL5972560 3 5.40
CHEMBL5933746 3 5.30
CHEMBL5843903 3 5.30
CHEMBL5793521 3 5.30
CHEMBL5755146 3 5.30
CHEMBL5861547 6 5.30
CHEMBL5958240 3 5.30
CHEMBL6016529 3 5.30
CHEMBL5973342 3 5.30
CHEMBL5873519 3 5.30

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL5905859 IC50 = 800.0 nM 6.10
CHEMBL5880420 IC50 = 1000.0 nM 6.00
CHEMBL5742196 IC50 = 2000.0 nM 5.70
CHEMBL5765675 IC50 = 2000.0 nM 5.70
CHEMBL5778938 IC50 = 2000.0 nM 5.70
CHEMBL6028916 IC50 = 2000.0 nM 5.70
CHEMBL6014549 IC50 = 3000.0 nM 5.52
CHEMBL5981736 IC50 = 3000.0 nM 5.52
CHEMBL5967558 IC50 = 3000.0 nM 5.52
CHEMBL5847512 IC50 = 3000.0 nM 5.52
CHEMBL6045682 IC50 = 3000.0 nM 5.52
CHEMBL6056865 IC50 = 3000.0 nM 5.52
CHEMBL5807766 IC50 = 3000.0 nM 5.52
CHEMBL5812475 IC50 = 4000.0 nM 5.40
CHEMBL5928525 IC50 = 4000.0 nM 5.40
CHEMBL5908210 IC50 = 4000.0 nM 5.40
CHEMBL5972560 IC50 = 4000.0 nM 5.40
CHEMBL5866999 IC50 = 4000.0 nM 5.40
CHEMBL5787891 IC50 = 4000.0 nM 5.40
CHEMBL6032044 IC50 = 4000.0 nM 5.40
CHEMBL5847735 IC50 = 4000.0 nM 5.40
CHEMBL5755146 IC50 = 5000.0 nM 5.30
CHEMBL5861547 IC50 = 5000.0 nM 5.30
CHEMBL5808062 IC50 = 5000.0 nM 5.30
CHEMBL5897078 IC50 = 5000.0 nM 5.30
CHEMBL5843903 IC50 = 5000.0 nM 5.30
CHEMBL6016529 IC50 = 5000.0 nM 5.30
CHEMBL5973342 IC50 = 5000.0 nM 5.30
CHEMBL5873519 IC50 = 5000.0 nM 5.30
CHEMBL5958240 IC50 = 5000.0 nM 5.30
CHEMBL5933746 IC50 = 5000.0 nM 5.30
CHEMBL5977278 IC50 = 5000.0 nM 5.30
CHEMBL5793521 IC50 = 5000.0 nM 5.30
CHEMBL5993297 IC50 = 6000.0 nM 5.22
CHEMBL5865418 IC50 = 6000.0 nM 5.22
CHEMBL5812127 IC50 = 6000.0 nM 5.22
CHEMBL5764138 IC50 = 6000.0 nM 5.22
CHEMBL6012498 IC50 = 6000.0 nM 5.22
CHEMBL5789806 IC50 = 6000.0 nM 5.22
CHEMBL5940519 IC50 = 7000.0 nM 5.16
CHEMBL5856358 IC50 = 7000.0 nM 5.16
CHEMBL6015167 IC50 = 7000.0 nM 5.16
CHEMBL5924410 IC50 = 7000.0 nM 5.16
CHEMBL6003294 IC50 = 7000.0 nM 5.16
CHEMBL5815096 IC50 = 8000.0 nM 5.10
CHEMBL5937117 IC50 = 8000.0 nM 5.10
CHEMBL5978958 IC50 = 8000.0 nM 5.10
CHEMBL5782797 IC50 = 8000.0 nM 5.10
CHEMBL5782825 IC50 = 8000.0 nM 5.10
CHEMBL5806907 IC50 = 9000.0 nM 5.05