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Assay Detail

CHEMBL5734849

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Binding
Z-lyte Assay : The DYRK1A kinase assay was run using the Ser/Thr 18 peptide Z-lyte assay kit according to manufacturer's instructions. This is a non-radioactive assay using fluorescence resonance energy transfer (FRET) between coumarin and fluorescein to detect kinase activity which is represented as a ratio of coumarin emission/fluorescein emission.Briefly, recombinant DYRK1A kinase, ATP and Ser/Thr peptide 18 were prepared in 1x Kinase buffer to final concentrations of 0.19 uMg/mL, 30 uM, and 4 uM respectively. The mixture was allowed to incubate with the representative compounds for one hour at room temperature. All reactions were performed in duplicate. Additionally, an 11-point dose-response curve of Staurosporine (1 μM top) was run to serve as a positive compound control.After incubation, Development Reagent A was diluted in Development Buffer then added to the reaction and allowed to further incubate for one hour at room temperature. The plate was read at Ex 400 Em 455 to detect the coumarin signal and Ex 400 Em 520 to measure the signal (EnVision Multilabel Plate Reader, PerkinElmer).
951
Total Activities
302
Compounds Tested
3
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Publication

Isoquinolin-3-YL carboxamides and preparation and use thereof
(2020)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
EC50 317 8.16 9.40
kon 317 - -
k_off 317 - -

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL5973318 3 9.40
CHEMBL5945495 3 9.22
CHEMBL6063676 3 9.10
CHEMBL6021234 6 9.05
CHEMBL5825110 3 9.05
CHEMBL5812865 3 9.05
CHEMBL5949017 3 9.05
CHEMBL5796895 3 9.00
CHEMBL5791577 3 9.00
CHEMBL6006860 3 8.96
CHEMBL5963096 3 8.92
CHEMBL6051950 3 8.92
CHEMBL6047852 3 8.92
CHEMBL5878488 3 8.92
CHEMBL5954396 3 8.89
CHEMBL5879982 3 8.89
CHEMBL5817052 3 8.89
CHEMBL6041318 3 8.89
CHEMBL5889343 3 8.89
CHEMBL5910604 3 8.89
CHEMBL5786788 3 8.85
CHEMBL6040393 3 8.85
CHEMBL6063445 3 8.85
CHEMBL5795403 3 8.85
CHEMBL5788174 3 8.85
CHEMBL5893128 3 8.82
CHEMBL6000877 3 8.82
CHEMBL5885382 3 8.82
CHEMBL5779760 3 8.82
CHEMBL6028032 3 8.82

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL5973318 EC50 = 0.4 nM 9.40
CHEMBL5945495 EC50 = 0.6 nM 9.22
CHEMBL6063676 EC50 = 0.8 nM 9.10
CHEMBL5825110 EC50 = 0.9 nM 9.05
CHEMBL5812865 EC50 = 0.9 nM 9.05
CHEMBL6021234 EC50 = 0.9 nM 9.05
CHEMBL5949017 EC50 = 0.9 nM 9.05
CHEMBL5796895 EC50 = 1.0 nM 9.00
CHEMBL5791577 EC50 = 1.0 nM 9.00
CHEMBL6006860 EC50 = 1.1 nM 8.96
CHEMBL6047852 EC50 = 1.2 nM 8.92
CHEMBL5878488 EC50 = 1.2 nM 8.92
CHEMBL5963096 EC50 = 1.2 nM 8.92
CHEMBL6051950 EC50 = 1.2 nM 8.92
CHEMBL6041318 EC50 = 1.3 nM 8.89
CHEMBL5879982 EC50 = 1.3 nM 8.89
CHEMBL5817052 EC50 = 1.3 nM 8.89
CHEMBL5889343 EC50 = 1.3 nM 8.89
CHEMBL5954396 EC50 = 1.3 nM 8.89
CHEMBL5910604 EC50 = 1.3 nM 8.89
CHEMBL6040393 EC50 = 1.4 nM 8.85
CHEMBL5788174 EC50 = 1.4 nM 8.85
CHEMBL5786788 EC50 = 1.4 nM 8.85
CHEMBL5795403 EC50 = 1.4 nM 8.85
CHEMBL6063445 EC50 = 1.4 nM 8.85
CHEMBL6028032 EC50 = 1.5 nM 8.82
CHEMBL5893128 EC50 = 1.5 nM 8.82
CHEMBL6000877 EC50 = 1.5 nM 8.82
CHEMBL5885382 EC50 = 1.5 nM 8.82
CHEMBL5779760 EC50 = 1.5 nM 8.82
CHEMBL5877648 EC50 = 1.6 nM 8.80
CHEMBL5898255 EC50 = 1.6 nM 8.80
CHEMBL5289681 EC50 = 1.6 nM 8.80
CHEMBL5285332 EC50 = 1.6 nM 8.80
CHEMBL6064270 EC50 = 1.7 nM 8.77
CHEMBL6054569 EC50 = 1.7 nM 8.77
CHEMBL5939127 EC50 = 1.7 nM 8.77
CHEMBL6034964 EC50 = 1.8 nM 8.74
CHEMBL5884403 EC50 = 1.8 nM 8.74
CHEMBL5858691 EC50 = 1.8 nM 8.74
CHEMBL5922426 EC50 = 1.9 nM 8.72
CHEMBL5856875 EC50 = 1.9 nM 8.72
CHEMBL5842812 EC50 = 1.9 nM 8.72
CHEMBL5905693 EC50 = 1.9 nM 8.72
CHEMBL5893743 EC50 = 1.9 nM 8.72
CHEMBL6012317 EC50 = 1.9 nM 8.72
CHEMBL5802776 EC50 = 1.9 nM 8.72
CHEMBL5965762 EC50 = 1.9 nM 8.72
CHEMBL5761418 EC50 = 2.0 nM 8.70
CHEMBL5881768 EC50 = 2.0 nM 8.70