Skip to main content
Free research Free research Free assay review with research home and workspace preview
Quick search ChEMBL 36
Assay Detail

CHEMBL5736166

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
FLIPR and cAMP Inhibition Assay: hADORA1/CHO (hA1 expressing) cells (Genscript) were plated at 1×104 cells/well into 384-well polystyrene plates one day before starting the experiment. On the day of experiment, the supernatant was discard and replaced with 40 L of dye (FLIPR calcium 5 Assay Kit) per well and the plates were incubated for 60 mins at 37° C. plus 5% CO2. Then testing compounds were added at different concentrations for FLIPR™ inhibition assay. After a 400 s incubation with compound, 10 M adenosine was added into the cells, and the signal was captured by FLIPR.hA2a/CHO, hA2b/CHO and mA2a/CHO (Genscript) were plated at 5×103 cells/well into 384-well polystyrene plates at the day of experiment. Compounds were pre-incubated with cells for 30 min at 37° C., 5% CO2. Then 10 M adenosine was added to the cells and incubated for 30 min at 37° C., 5% CO2. Detection reagent (CISBIO) was added and the plates were incubated for 60 min at room temperature. The signal was captured by Envision.
318
Total Activities
106
Compounds Tested
3
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Adenosine receptor A2b (CHEMBL255)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Triazolo-pyrimidine compounds and uses thereof
(2020)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 106 6.65 8.36
kon 106 - -
k_off 106 - -

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL5827075 3 8.36
CHEMBL5999728 3 8.33
CHEMBL5928153 3 8.32
CHEMBL5867675 3 7.92
CHEMBL5986561 3 7.92
CHEMBL6007478 3 7.91
CHEMBL5800386 3 7.85
CHEMBL5917926 3 7.85
CHEMBL6057843 3 7.79
CHEMBL5880072 3 7.77
CHEMBL5841873 3 7.72
CHEMBL6057896 3 7.68
CHEMBL5747460 3 7.63
CHEMBL5765395 3 7.42
CHEMBL5833725 3 7.42
CHEMBL5829088 3 7.42
CHEMBL5825227 3 7.39
CHEMBL6003948 3 7.35
CHEMBL5913092 3 7.35
CHEMBL5974806 3 7.33
CHEMBL5795044 3 7.32
CHEMBL5882133 3 7.32
CHEMBL5940119 3 7.32
CHEMBL6030840 3 7.29
CHEMBL5756623 3 7.25
CHEMBL5966778 3 7.24
CHEMBL5919017 3 7.19
CHEMBL6043653 3 7.17
CHEMBL6022992 3 7.14
CHEMBL5875672 3 7.14

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL5827075 IC50 = 4.4 nM 8.36
CHEMBL5999728 IC50 = 4.69 nM 8.33
CHEMBL5928153 IC50 = 4.8 nM 8.32
CHEMBL5986561 IC50 = 12.0 nM 7.92
CHEMBL5867675 IC50 = 12.0 nM 7.92
CHEMBL6007478 IC50 = 12.2 nM 7.91
CHEMBL5917926 IC50 = 14.0 nM 7.85
CHEMBL5800386 IC50 = 14.0 nM 7.85
CHEMBL6057843 IC50 = 16.4 nM 7.79
CHEMBL5880072 IC50 = 17.0 nM 7.77
CHEMBL5841873 IC50 = 19.0 nM 7.72
CHEMBL6057896 IC50 = 21.0 nM 7.68
CHEMBL5747460 IC50 = 23.3 nM 7.63
CHEMBL5829088 IC50 = 38.0 nM 7.42
CHEMBL5765395 IC50 = 38.0 nM 7.42
CHEMBL5833725 IC50 = 38.0 nM 7.42
CHEMBL5825227 IC50 = 40.9 nM 7.39
CHEMBL5913092 IC50 = 44.5 nM 7.35
CHEMBL6003948 IC50 = 45.0 nM 7.35
CHEMBL5974806 IC50 = 47.0 nM 7.33
CHEMBL5882133 IC50 = 48.0 nM 7.32
CHEMBL5795044 IC50 = 48.0 nM 7.32
CHEMBL5940119 IC50 = 47.5 nM 7.32
CHEMBL6030840 IC50 = 51.0 nM 7.29
CHEMBL5756623 IC50 = 56.0 nM 7.25
CHEMBL5966778 IC50 = 58.0 nM 7.24
CHEMBL5919017 IC50 = 65.0 nM 7.19
CHEMBL6043653 IC50 = 68.0 nM 7.17
CHEMBL6022992 IC50 = 73.0 nM 7.14
CHEMBL5875672 IC50 = 72.0 nM 7.14
CHEMBL5836704 IC50 = 71.6 nM 7.14
CHEMBL6063197 IC50 = 80.0 nM 7.10
CHEMBL5847956 IC50 = 82.0 nM 7.09
CHEMBL6055525 IC50 = 80.5 nM 7.09
CHEMBL5990931 IC50 = 81.0 nM 7.09
CHEMBL5810207 IC50 = 83.0 nM 7.08
CHEMBL5956015 IC50 = 84.0 nM 7.08
CHEMBL5817464 IC50 = 91.0 nM 7.04
CHEMBL6016827 IC50 = 93.5 nM 7.03
CHEMBL6062538 IC50 = 94.0 nM 7.03
CHEMBL5787943 IC50 = 97.0 nM 7.01
CHEMBL5957422 IC50 = 101.0 nM 7.00
CHEMBL6041892 IC50 = 102.0 nM 6.99
CHEMBL5896698 IC50 = 102.0 nM 6.99
CHEMBL6044836 IC50 = 109.0 nM 6.96
CHEMBL5993458 IC50 = 117.0 nM 6.93
CHEMBL5857008 IC50 = 121.0 nM 6.92
CHEMBL5988628 IC50 = 122.0 nM 6.91
CHEMBL5813457 IC50 = 125.0 nM 6.90
CHEMBL5774791 IC50 = 142.0 nM 6.85