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Assay Detail

CHEMBL5736723

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
Scintillation Proximity Assay (SPA: The scintillation proximity assay (SPA) was run in white polystyrene flat-bottom 384-well plates (Greiner, cat. No. 781075). Assays were carried out in 40 i1 reaction volumes. Various concentrations of test ligands in 0.4 microlitres of DMSO were added to assay plates using an acoustic liquid dispenser. 4 nM purified N—(HN)6-GST-TCS-hRORγ (258-518) was mixed with 40 micrograms Yttrium oxide (YOx) glutathione SPA imaging beads in assay buffer (20 mM Tris, 150 mM NaCl, 10% Glycerol, 0.25% CHAPS, 1 mM TCEP) prior to adding 30 microlitres to test ligands. Assay plates were incubated for one hour at room temperature before adding 10 microlitres tritiated 2-(4-(ethylsulfonyl)phenyl)-N-(4-(2-(methoxymethyl)phenyl)thiophen-2-yl)acetamide to test plates in assay buffer (final concentration, 25 nM). Test plates were incubated for 16 hours and read using a LEADseeker Multimodality imaging instrument.
465
Total Activities
136
Compounds Tested
3
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Organism Homo sapiens
Confidence 9 — Direct single protein target
Curated By Autocuration

Target

Nuclear receptor ROR-gamma (CHEMBL1741186)
Type SINGLE PROTEIN
Organism Homo sapiens

Publication

Compounds
(2021)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 155 6.75 7.50
kon 155 - -
k_off 155 - -

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL5938751 3 7.50
CHEMBL4857395 3 7.50
CHEMBL4877500 9 7.40
CHEMBL4857284 3 7.40
CHEMBL5996139 3 7.40
CHEMBL4864990 3 7.30
CHEMBL4868864 3 7.30
CHEMBL5812242 3 7.30
CHEMBL4855387 3 7.30
CHEMBL6026656 3 7.30
CHEMBL5865301 3 7.30
CHEMBL4847761 3 7.30
CHEMBL4865776 3 7.20
CHEMBL4878173 3 7.20
CHEMBL6056242 3 7.20
CHEMBL5960515 3 7.20
CHEMBL4856430 3 7.20
CHEMBL5819478 3 7.20
CHEMBL5828228 3 7.20
CHEMBL6056459 3 7.20
CHEMBL5921331 3 7.20
CHEMBL4869175 3 7.20
CHEMBL4870856 3 7.20
CHEMBL4876902 3 7.20
CHEMBL5835688 3 7.20
CHEMBL4865352 9 7.20
CHEMBL5745189 3 7.20
CHEMBL4872141 3 7.10
CHEMBL5739946 3 7.10
CHEMBL5800395 3 7.10

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL4857395 IC50 = 31.6 nM 7.50
CHEMBL5938751 IC50 = 31.6 nM 7.50
CHEMBL5996139 IC50 = 39.8 nM 7.40
CHEMBL4877500 IC50 = 39.8 nM 7.40
CHEMBL4877500 IC50 = 39.8 nM 7.40
CHEMBL4857284 IC50 = 39.8 nM 7.40
CHEMBL4855387 IC50 = 50.1 nM 7.30
CHEMBL4868864 IC50 = 50.1 nM 7.30
CHEMBL5812242 IC50 = 50.1 nM 7.30
CHEMBL6026656 IC50 = 50.1 nM 7.30
CHEMBL5865301 IC50 = 50.1 nM 7.30
CHEMBL4847761 IC50 = 50.1 nM 7.30
CHEMBL4864990 IC50 = 50.1 nM 7.30
CHEMBL4878173 IC50 = 63.1 nM 7.20
CHEMBL4865352 IC50 = 63.1 nM 7.20
CHEMBL4870856 IC50 = 63.1 nM 7.20
CHEMBL4865776 IC50 = 63.1 nM 7.20
CHEMBL4856430 IC50 = 63.1 nM 7.20
CHEMBL6056242 IC50 = 63.1 nM 7.20
CHEMBL5960515 IC50 = 63.1 nM 7.20
CHEMBL5921331 IC50 = 63.1 nM 7.20
CHEMBL5819478 IC50 = 63.1 nM 7.20
CHEMBL4869175 IC50 = 63.1 nM 7.20
CHEMBL4876902 IC50 = 63.1 nM 7.20
CHEMBL6056459 IC50 = 63.1 nM 7.20
CHEMBL5745189 IC50 = 63.1 nM 7.20
CHEMBL5835688 IC50 = 63.1 nM 7.20
CHEMBL4877500 IC50 = 63.1 nM 7.20
CHEMBL5828228 IC50 = 63.1 nM 7.20
CHEMBL4846059 IC50 = 79.4 nM 7.10
CHEMBL5800395 IC50 = 79.4 nM 7.10
CHEMBL4848388 IC50 = 79.4 nM 7.10
CHEMBL4850359 IC50 = 79.4 nM 7.10
CHEMBL5987712 IC50 = 79.4 nM 7.10
CHEMBL6008825 IC50 = 79.4 nM 7.10
CHEMBL5827930 IC50 = 79.4 nM 7.10
CHEMBL4872141 IC50 = 79.4 nM 7.10
CHEMBL5983750 IC50 = 79.4 nM 7.10
CHEMBL6008577 IC50 = 79.4 nM 7.10
CHEMBL6018849 IC50 = 79.4 nM 7.10
CHEMBL5739946 IC50 = 79.4 nM 7.10
CHEMBL5776829 IC50 = 79.4 nM 7.10
CHEMBL6026771 IC50 = 100.0 nM 7.00
CHEMBL6018927 IC50 = 100.0 nM 7.00
CHEMBL5878673 IC50 = 100.0 nM 7.00
CHEMBL6000337 IC50 = 100.0 nM 7.00
CHEMBL5766992 IC50 = 100.0 nM 7.00
CHEMBL5967906 IC50 = 100.0 nM 7.00
CHEMBL5880723 IC50 = 100.0 nM 7.00
CHEMBL6005326 IC50 = 100.0 nM 7.00