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Assay Detail

CHEMBL5737547

Review assay metadata, readout intent, target linkage, and publication context from the same page.

Binding
MLL1-WRAD2 Enzyme Assay: Compound potency was assessed through incorporation of 3H-SAM into oligonucleosomes purified from HeLa cells. Specifically, recombinant human MLL1 (aa 3745-3969, GenBank Accession No. NM_005933), WDR5 (aa 22-334, GenBank Accession No. NM 017588), RbBP5 (aa 1-538, GenBank Accession No. NM_005057), Ash2L (aa 2-534, GenBank Accession No. NM_001105214), and DPY-30 (aa 1-99, GenBank Accession No. NM_0325742), all with N-terminal His tag, were expressed in E. coli and mixed at a molar ratio of 1:1:1:1:2. 10 nM of the assembled MLL1-WRAD2 complex was mixed with 100 nM WRAD2 to enhance complex formation before incubation with 0.05 mg/ml nucleosome substrate and compounds (as 10 point duplicate dose response titrations) for 15 min in a buffer consisting of 50 mM Tris (pH 8.5), 5 mM MgCl2, 50 mM NaCl, 1 mM DTT, 0.01% Brij-35, and 1% DMSO. Reaction was initiated with 1 μM 3H-SAM and incubated for 1 hour at 30° C. Reaction mixture was transferred to P81 filter-paper and washed with PBS before detection.
216
Total Activities
69
Compounds Tested
3
Activity Types
0
Assay Parameters

Assay Information

Assay Type Binding
Confidence 0 — Uncurated / Unknown
Curated By Autocuration

Target

Unchecked (CHEMBL612545)
Type UNCHECKED

Publication

Substituted carboxamides as inhibitors of WDR5 protein-protein binding
(2021)

Activity Statistics

Type Count Avg pChEMBL Best pChEMBL
IC50 72 5.72 7.31
kon 72 - -
k_off 72 - -

Compounds Tested

Compound Name Phase Activities Best pChEMBL
CHEMBL6018567 3 7.31
CHEMBL5964471 3 6.71
CHEMBL5758844 3 6.69
CHEMBL5941839 3 6.67
CHEMBL5988233 3 6.54
CHEMBL5751480 3 6.53
CHEMBL5955314 3 6.48
CHEMBL5820916 3 6.29
CHEMBL5769064 3 6.28
CHEMBL5989434 3 6.26
CHEMBL5984557 6 6.23
CHEMBL5764557 3 6.22
CHEMBL5999701 3 6.12
CHEMBL5806937 3 6.11
CHEMBL5959550 3 6.04
CHEMBL5765286 9 6.03
CHEMBL5819994 3 6.01
CHEMBL5777404 3 5.96
CHEMBL5775482 3 5.96
CHEMBL5965571 3 5.96
CHEMBL6015959 3 5.94
CHEMBL5770014 3 5.89
CHEMBL5972754 3 5.85
CHEMBL5773992 3 5.83
CHEMBL5921931 3 5.83
CHEMBL5948754 3 5.80
CHEMBL5740516 3 5.76
CHEMBL5896100 3 5.76
CHEMBL5922903 3 5.75
CHEMBL5803196 3 5.72

Activity Data

Compound Name Type Rel. Value Units pChEMBL
CHEMBL6018567 IC50 = 49.0 nM 7.31
CHEMBL5964471 IC50 = 197.0 nM 6.71
CHEMBL5758844 IC50 = 203.0 nM 6.69
CHEMBL5941839 IC50 = 216.0 nM 6.67
CHEMBL5988233 IC50 = 290.0 nM 6.54
CHEMBL5751480 IC50 = 293.0 nM 6.53
CHEMBL5955314 IC50 = 332.0 nM 6.48
CHEMBL5820916 IC50 = 514.0 nM 6.29
CHEMBL5769064 IC50 = 529.0 nM 6.28
CHEMBL5989434 IC50 = 549.0 nM 6.26
CHEMBL5984557 IC50 = 592.0 nM 6.23
CHEMBL5984557 IC50 = 592.0 nM 6.23
CHEMBL5764557 IC50 = 607.0 nM 6.22
CHEMBL5999701 IC50 = 764.0 nM 6.12
CHEMBL5806937 IC50 = 779.0 nM 6.11
CHEMBL5959550 IC50 = 907.0 nM 6.04
CHEMBL5765286 IC50 = 939.0 nM 6.03
CHEMBL5765286 IC50 = 939.0 nM 6.03
CHEMBL5765286 IC50 = 939.0 nM 6.03
CHEMBL5819994 IC50 = 966.0 nM 6.01
CHEMBL5965571 IC50 = 1100.0 nM 5.96
CHEMBL5777404 IC50 = 1093.0 nM 5.96
CHEMBL5775482 IC50 = 1110.0 nM 5.96
CHEMBL6015959 IC50 = 1150.0 nM 5.94
CHEMBL5770014 IC50 = 1300.0 nM 5.89
CHEMBL5972754 IC50 = 1410.0 nM 5.85
CHEMBL5773992 IC50 = 1470.0 nM 5.83
CHEMBL5921931 IC50 = 1480.0 nM 5.83
CHEMBL5948754 IC50 = 1570.0 nM 5.80
CHEMBL5740516 IC50 = 1740.0 nM 5.76
CHEMBL5896100 IC50 = 1750.0 nM 5.76
CHEMBL5922903 IC50 = 1790.0 nM 5.75
CHEMBL5803196 IC50 = 1900.0 nM 5.72
CHEMBL5816421 IC50 = 1900.0 nM 5.72
CHEMBL5756767 IC50 = 1890.0 nM 5.72
CHEMBL5936269 IC50 = 2090.0 nM 5.68
CHEMBL5992323 IC50 = 2070.0 nM 5.68
CHEMBL6017945 IC50 = 2100.0 nM 5.68
CHEMBL6004276 IC50 = 2250.0 nM 5.65
CHEMBL5979000 IC50 = 2280.0 nM 5.64
CHEMBL6012221 IC50 = 2390.0 nM 5.62
CHEMBL6037844 IC50 = 2390.0 nM 5.62
CHEMBL6060568 IC50 = 2534.0 nM 5.60
CHEMBL5964629 IC50 = 2510.0 nM 5.60
CHEMBL5874695 IC50 = 2510.0 nM 5.60
CHEMBL5974041 IC50 = 2890.0 nM 5.54
CHEMBL5834019 IC50 = 3250.0 nM 5.49
CHEMBL5987537 IC50 = 3890.0 nM 5.41
CHEMBL5986659 IC50 = 3985.0 nM 5.40
CHEMBL5956068 IC50 = 3990.0 nM 5.40